C11B3/06

Preparation method of eicosapentaenoic acid ethyl ester

A preparation method of eicosapentaenoic acid (EPA) ethyl ester is provided and relates to the field of EPA ethyl ester processing technologies. The preparation method includes: performing degumming and deacidification on a sardine crude oil to obtain a semi-refined sardine oil, performing esterification on the semi-refined sardine oil to obtain an esterified sardine oil and then performing winterization on the esterified sardine oil to thereby obtain an semi-refined esterified sardine oil, performing bleaching and deodorization on the semi-refined esterified sardine oil, and performing multi-stage distillation treatment. Finally, the sardine oil is purified by liquid chromatography to obtain the high purity EPA ethyl ester. The preparation method can improve a utilization rate of the sardine oil and obtain the high-purity EPA ethyl ester.

Enzymatic degumming of unrefined triglyceride oil
11505763 · 2022-11-22 · ·

The invention relates to a process for enzymatic degumming of unrefined triglyceride oil, said process comprising the following successive steps: (a) providing an unrefined triglyceride oil having a phosphorus content of at least 100 mg per kg of unrefined triglyceride oil; (b) combining the unrefined triglyceride oil with water, an acid and a phospholipase to produce an oil-in-water emulsion having a pH in the range of 2.5 to 4.5; said phospholipase being selected phospholipase A1, phospholipase A2 and combinations thereof; (c) keeping the emulsion at a temperature of 20-90° C. for at least 10 minutes; (d) introducing a base into the emulsion; and (e) separating degummed triglyceride oil from the emulsion. This enzymatic degumming process is extremely effective in removing phospholipids, including non-hydratable phospholipids (NHP), from unrefined vegetable oils and produces degummed vegetable oil in high yield.

ELECTROLYTIC OIL EXTRACTION SYSTEM AND PROCESS

Systems and methods for use in extracting oil from solid plant-based materials are described. The systems and methods use an electrolyzed carrier fluid made from a hydroxide brine for contacting with plant-based material to thereby separate oil from solid plant particulate. The electrolyzed carrier fluid can have a reductive oxidation-reduction-potential (ORP) of −700 mV or more, such as in the range of from about −900 mV to about −1000 mV.

OILINESS-REDUCING AGENT, EDIBLE OIL AND FAT COMPOSITION, METHOD FOR MANUFACTURING OILINESS-REDUCING AGENT, AND METHOD FOR REDUCING OILINESS OF FOOD PRODUCT
20230089540 · 2023-03-23 ·

There is provided an oiliness-reducing agent that is capable of reducing the oiliness perceived when a person consumes a food product.

The oiliness-reducing agent is characterized by containing, as an active ingredient, a heated oil obtained by implementing a heating treatment at 120° C. or higher on an unrefined crude oil including an expressed oil of an oil and fat raw material or an extracted oil of the oil and fat raw material, or on an oil and fat that has passed through a degumming step, a deacidification step, or a bleaching step in steps for refining the unrefined crude oil.

REMOVAL OF MIU AND METALS FROM FEEDSTOCK
20220333035 · 2022-10-20 ·

MIU and metals are removed from Tallow or Seed based oils (feedstock) utilizing water treated by reverse osmosis and specific operating conditions using a very high RCF centrifuge. A relatively small quantity of the RO water (3% to 20% by weight) is added to the feedstock to attract the MIU and metals. The mixture is then centrifuged at an RCF in excess of approximately 6500. Temperature, flow rate to control Residence time and backpressure in the centrifuge are selected. The process separates the RO water with the MIU and metals from the feedstock.

A PROCESS FOR THE PRODUCTION OF DEGUMMED OIL AND GUMS, AND PRODUCTS PRODUCED BY THE PROCESS

The present disclosure relates to a process for refining crude oils using a combination of a chemical process and mega-sonic treatment to simultaneously and efficiently separate oil and gum phases. In particular, the present disclosure relates to a process for refining crude oils using a combination of chemical processes followed by megasonic treatment to effectively separate and recover entrained oil from a gum phase to increase the oil yield, and to produce an oil of higher quality with reduced gum content. The present disclosure also relates to a process for refining crude oils using a combination of chemical processes followed by megasonic treatment to effectively separate and recover entrained gums from an oil phase to increase the gum yield, and to produce a gum of higher quality with reduced oil content. The present disclosure also relates to obtaining refined oils and refined gums from the process described herein.

A PROCESS FOR THE PRODUCTION OF DEGUMMED OIL AND GUMS, AND PRODUCTS PRODUCED BY THE PROCESS

The present disclosure relates to a process for refining crude oils using a combination of a chemical process and mega-sonic treatment to simultaneously and efficiently separate oil and gum phases. In particular, the present disclosure relates to a process for refining crude oils using a combination of chemical processes followed by megasonic treatment to effectively separate and recover entrained oil from a gum phase to increase the oil yield, and to produce an oil of higher quality with reduced gum content. The present disclosure also relates to a process for refining crude oils using a combination of chemical processes followed by megasonic treatment to effectively separate and recover entrained gums from an oil phase to increase the gum yield, and to produce a gum of higher quality with reduced oil content. The present disclosure also relates to obtaining refined oils and refined gums from the process described herein.

METHOD FOR EXTRACTING HIGH-QUALITY KRILL OIL FROM KRILL

A method for extracting high-quality krill oil from krill includes the following steps: S1. performing extraction on krill with an organic solvent, and collecting an extracting solution; S2. adding alkaline water to the extracting solution to enable a free fatty acid to form a fatty acid salt to be separated from an oil phase, and performing oil-water phase separation and collecting the oil phase; and S3. purifying the oil phase to obtain the high-quality krill oil. In the present application, the preparation process for krill oil is optimized, organic solvent extraction and alkali refining are ingeniously combined, and process parameters are adjusted and optimized, thereby reducing the acid value of krill oil, and also ensuring the content of active ingredients such as phospholipid and astaxanthin in krill oil to the greatest extent, and improving the quality of krill oil.

METHOD FOR EXTRACTING HIGH-QUALITY KRILL OIL FROM KRILL

A method for extracting high-quality krill oil from krill includes the following steps: S1. performing extraction on krill with an organic solvent, and collecting an extracting solution; S2. adding alkaline water to the extracting solution to enable a free fatty acid to form a fatty acid salt to be separated from an oil phase, and performing oil-water phase separation and collecting the oil phase; and S3. purifying the oil phase to obtain the high-quality krill oil. In the present application, the preparation process for krill oil is optimized, organic solvent extraction and alkali refining are ingeniously combined, and process parameters are adjusted and optimized, thereby reducing the acid value of krill oil, and also ensuring the content of active ingredients such as phospholipid and astaxanthin in krill oil to the greatest extent, and improving the quality of krill oil.

Removing organic chlorides from glyceride oils
11466230 · 2022-10-11 · ·

A process is provided for removing organic chlorides from glyceride oil. The process includes the steps of (a) reacting a glyceride oil comprising organic chlorides with a liquid aqueous system at a temperature of at least 80° C. to form a treated glyceride oil and (b) separating the treated glyceride oil from the liquid aqueous system. The treated glyceride oil has a reduced concentration of organic chlorides compared to the glyceride oil reacted in step (a).