Patent classifications
C11D11/02
Powder and granule, process for making such powder and granule, and use thereof
The present invention is directed towards a process for making a powder or granule containing (A) at least one chelating agent selected from methyl glycine diacetic acid (MGDA) and glutamic acid diacetate (GLDA) and iminodisuccinic acid (IDS) and their respective alkali metal salts, (B) at least one homo- or copolymer of (meth)acrylic acid, partially or fully neutralized with alkali,
said process comprising the steps of (a) mixing the at least one chelating agent (A) and the at least one homo- or copolymer (B) in the presence of water, (b) removing most of said water by spray-drying or spray granulation using a gas with an inlet temperature of at least 125° C.
Powder and granule, process for making such powder and granule, and use thereof
The present invention is directed towards a process for making a powder or granule containing (A) at least one chelating agent selected from methyl glycine diacetic acid (MGDA) and glutamic acid diacetate (GLDA) and iminodisuccinic acid (IDS) and their respective alkali metal salts, (B) at least one homo- or copolymer of (meth)acrylic acid, partially or fully neutralized with alkali,
said process comprising the steps of (a) mixing the at least one chelating agent (A) and the at least one homo- or copolymer (B) in the presence of water, (b) removing most of said water by spray-drying or spray granulation using a gas with an inlet temperature of at least 125° C.
GRANULES OF MGDA AND (METH)ACRYLIC ACID HOMO- OR CO-POLYMER; PROCESS FOR MAKING THE SAME
Process for making a granule containing (A) at least one chelating agent selected from alkali metal salts of methyl glycine diacetic acid (MGDA) and of iminodisuccinic acid (IDS), and, optionally, (B) at least one homo- or copolymer of (meth)acrylic acid, partially or fully neutralized with alkali,
said process comprising the steps of (a) providing an aqueous solution or slurry containing chelating agent (A) and, if applicable, (co)polymer (B), (b) removing most of said water by spray granulation in a fluidized bed, (c) treating the resultant granule in a vessel of which at least one part rotates around a horizontal axis and wherein said vessel is selected from paddle mixers, free-fall mixers and plough share mixers.
GRANULES OF MGDA AND (METH)ACRYLIC ACID HOMO- OR CO-POLYMER; PROCESS FOR MAKING THE SAME
Process for making a granule containing (A) at least one chelating agent selected from alkali metal salts of methyl glycine diacetic acid (MGDA) and of iminodisuccinic acid (IDS), and, optionally, (B) at least one homo- or copolymer of (meth)acrylic acid, partially or fully neutralized with alkali,
said process comprising the steps of (a) providing an aqueous solution or slurry containing chelating agent (A) and, if applicable, (co)polymer (B), (b) removing most of said water by spray granulation in a fluidized bed, (c) treating the resultant granule in a vessel of which at least one part rotates around a horizontal axis and wherein said vessel is selected from paddle mixers, free-fall mixers and plough share mixers.
METHOD OF MAKING A SPRAY-DRIED LAUNDRY DETERGENT PARTICLE
A method of making a spray-dried laundry detergent particle, wherein the method includes the steps: (a) forming an aqueous laundry detergent slurry, wherein the slurry includes: (i) from 1 wt% to 40 wt% anionic detersive surfactant; (ii) from 0.1 wt% to 3.5 wt% polyepoxy succinic acid polymer; and (iii) from 10 wt% to 80 wt% water, and (b) spray drying the slurry formed in step (a) to form a spray-dried laundry detergent particle.
METHOD OF MAKING A SPRAY-DRIED LAUNDRY DETERGENT PARTICLE
A method of making a spray-dried laundry detergent particle, wherein the method includes the steps: (a) forming an aqueous laundry detergent slurry, wherein the slurry includes: (i) from 1 wt% to 40 wt% anionic detersive surfactant; (ii) from 0.1 wt% to 3.5 wt% polyepoxy succinic acid polymer; and (iii) from 10 wt% to 80 wt% water, and (b) spray drying the slurry formed in step (a) to form a spray-dried laundry detergent particle.
SOLIDIFYING LIQUID AMINE OXIDE, BETAINE, AND/OR SULTAINE SURFACTANTS WITH A BINDER AND OPTIONAL CARRIER
The invention relates to solidification of liquid amine oxide, betaine, and/or sultaine surfactants with a binder to form a solidified surfactant composition. In particular, the invention relates to solidification of liquid surfactants utilizing drying device(s), wherein the feed composition contains at least one liquid surfactant and a binder and optional carrier to form a solidified surfactant composition. The solidified surfactant compositions can be useful in various cleaning compositions.
SOLIDIFYING LIQUID AMINE OXIDE, BETAINE, AND/OR SULTAINE SURFACTANTS WITH A BINDER AND OPTIONAL CARRIER
The invention relates to solidification of liquid amine oxide, betaine, and/or sultaine surfactants with a binder to form a solidified surfactant composition. In particular, the invention relates to solidification of liquid surfactants utilizing drying device(s), wherein the feed composition contains at least one liquid surfactant and a binder and optional carrier to form a solidified surfactant composition. The solidified surfactant compositions can be useful in various cleaning compositions.
Process for preparing a spray-dried laundry detergent particle
The present invention relates to a process for preparing a spray-dried laundry detergent particle, wherein the process includes the step of contacting water-insoluble silicate salt to monomeric organic carboxylic acid in an aqueous mixture, wherein the aqueous mixture has a pH of 4.2 or less, wherein the aqueous mixture includes detersive surfactant, wherein the aqueous mixture is substantially free of carbonate salt, wherein the water-insoluble silicate salt reacts with the monomeric organic carboxylic acid to form silica, wherein the aqueous mixture is spray-dried to form a spray-dried laundry detergent particle, wherein the particle comprises: detersive surfactant; monomeric organic carboxylic acid; and silica, wherein the particle is substantially free of carbonate salt.
Process for preparing a spray-dried laundry detergent particle
The present invention relates to a process for preparing a spray-dried laundry detergent particle, wherein the process includes the step of contacting water-insoluble silicate salt to monomeric organic carboxylic acid in an aqueous mixture, wherein the aqueous mixture has a pH of 4.2 or less, wherein the aqueous mixture includes detersive surfactant, wherein the aqueous mixture is substantially free of carbonate salt, wherein the water-insoluble silicate salt reacts with the monomeric organic carboxylic acid to form silica, wherein the aqueous mixture is spray-dried to form a spray-dried laundry detergent particle, wherein the particle comprises: detersive surfactant; monomeric organic carboxylic acid; and silica, wherein the particle is substantially free of carbonate salt.