A nanocomposite comprising crystalline grains in an amorphous matrix, the crystalline grains comprising an iron (Fe)-nickel (Ni) compound and being separated from one another by the amorphous matrix; and one or more barriers between the crystalline grains and the amorphous matrix, the barriers being configured to inhibit growth of the crystalline grains during forming of the crystalline grains, a barrier of the one or more barriers being between a crystalline grain and the amorphous matrix; wherein the amorphous matrix comprises an increased resistivity relative to a resistivity of the crystalline grains; and wherein the amorphous matrix is configured to reduce losses of the crystalline grains caused by a change in a magnetic field applied to the crystalline grains relative to losses of the crystalline grains that occur without the amorphous matrix.

The present disclosure relates to an iron (Fe)-based amorphous soft magnetic alloy and a method for manufacturing the soft magnetic alloy. According to the present disclosure, there is provided an Fe-based soft magnetic alloy including C and S meeting 1≥a+b≥6, wherein a is an atomic % content of C and b is an atomic % content of S, B meeting 4.5≥x≥13.0, wherein x is an atomic % content of B, Cu meeting 0.2≥y≥1.5, wherein y is an atomic % content of Cu, Al meeting 0.5≥z≥2, wherein z is an atomic % content of Al, and a remaining atomic % content of Fe and other inevitable impurities, wherein the Fe-based soft magnetic alloy includes a micro-structure, and wherein the micro-structure includes a crystalline phase with a mean crystalline grain size ranging from 15 nm to 50 nm in an amorphous base.

An Fe-based nano-crystalline alloy formed from an alloy composition of (FeE).sub.(100-X-Y-Z)B.sub.XP.sub.YCu.sub.Z having an amorphous phase as a main phase, wherein 79≦100-X-Y-Z≦86 atomic %, 4≦X≦9 atomic %, 1≦Y≦10 atomic %, and 0.5≦Z<1.2 atomic %, and wherein (FeE) includes Fe and at least one element selected from the group consisting of Ti, Zr, Hf, Nb, Ta, Mo, W, Cr, Al, Mn, Ag, Zn, Sn, As, Sb, Bi, Y, N, O and a rare-earth element, wherein a combined total of said at least one element selected from the group consisting of Ti, Zr, Hf, Nb, Ta, Mo, W, Cr, Al, Mn, Ag, Zn, Sn, As, Sb, Bi, Y, N, O and a rare-earth element is in an amount of 3 atomic % or less relative to the whole composition.

An R—Fe—B base sintered magnet is provided consisting essentially of R (which is at least two rare earth elements and essentially contains Nd and Pr), M.sub.1 which is at least two of Si, Al, Mn, Ni, Cu, Zn, Ga, Ge, Pd, Ag, Cd, In, Sn, Sb, Pt, Au, Hg, Pb, and Bi, M.sub.2 which is at least one of Ti, V, Cr, Zr, Nb, Mo, Hf, Ta, and W, boron, and the balance of Fe, and containing an intermetallic compound R.sub.2(Fe,(Co)).sub.14B as a main phase. The magnet contains an R—Fe(Co)-M.sub.1 phase as a grain boundary phase, the R—Fe(Co)-M.sub.1 phase contains A phase which is crystalline with crystallites of at least 10 nm formed at grain boundary triple junctions, and B phase which is amorphous and/or nanocrystalline with crystallites of less than 10 nm formed at intergranular grain boundaries and optionally grain boundary triple junctions.

The disclosure is directed to a method of forming high-aspect-ratio metallic glass articles that are substantially free of defects and cosmetic flaws by means of rapid capacitive discharge forming. Metallic glass alloys that are stable against crystallization for at least 100 ms at temperatures where the viscosity is in the range of 10.sup.0 to 10.sup.4 Pa-s are considered as suitable for forming such high-aspect-ratio articles.

A magnetic core includes a nanocrystalline alloy ribbon having a composition represented by FeCu.sub.xB.sub.ySi.sub.zA.sub.aX.sub.b, where 0.6≤x<1.2, 10≤y≤20, 0≤(y+z)≤24, and 0≤a≤10, 0≤b≤5, all numbers being in atomic percent, with the balance being Fe and incidental impurities, and where A is an optional inclusion of at least one element selected from Ni, Mn, Co, V, Cr, Ti, Zr, Nb, Mo, Hf, Ta and W, and X is an optional inclusion of at least one element selected from Re, Y, Zn, As, In, Sn, and rare earth elements. The nanocrylstalline alloy ribbon has a local structure such that nanocrystals with average particle sizes of less than 40 nm are dispersed in an amorphous matrix and are occupying more than 30 volume percent of the ribbon.

Manufacturing a cold-rolled steel plate by smelting a steel slab having the chemical composition containing on the basis of percent by mass, C from 0.03 to 0.12%, Si from 0 to 1.0%, Mn from 0.2 to 0.8%, P at 0.03% or less, S at 0.03% or less, Ti from 0.04 to 0.3%, and Al at 0.05% or less, with a residue being formed of Fe and unavoidable impurities, the chemical composition satisfying 5*C%-Si %+Mn %−1.5 *Al %<1, and an average diameter of particles of a Ti-based carbide as a precipitate is from 20 to 100 nm; heating the slab to 1200° C. or more and hot rolling, forming a hot-rolled steel plate; winding the hot-rolled steel plate from 500 to 700° C. to form a hot-rolled coil; and cold rolling or annealing and cold rolling the coil obtaining cross-sectional hardness from 200 to 400 HV.

An apparatus and method of uniformly heating, rheologically softening, and thermoplastically forming metallic glasses rapidly into a net shape using a rapid capacitor discharge forming (RCDF) tool are provided. The RCDF method utilizes the discharge of electrical energy stored in a capacitor to uniformly and rapidly heat a sample or charge of metallic glass alloy to a predetermined “process temperature” between the glass transition temperature of the amorphous material and the equilibrium melting point of the alloy in a time scale of several milliseconds or less. Once the sample is uniformly heated such that the entire sample block has a sufficiently low process viscosity it may be shaped into high quality amorphous bulk articles via any number of techniques including, for example, injection molding, dynamic forging, stamp forging, and blow molding in a time frame of Less than 1 second.

There is provided a method for producing metal foils, capable of easily crystalizing amorphous soft magnetic material of a plurality of metal foils into nano-crystal magnetic by uniformly heating the metal foils. Separating members (magnets) are disposed on the opposite sides of a laminate, which has been obtained by laminating a plurality of metal foils made of amorphous soft magnetic material, in the laminated direction of the laminate, and the metal foils forming the laminate are magnetized with the magnets. Thus, the adjacent metal foils are separated from each other in the laminated direction and a gap is formed between the metal foils. The metal foils are heated with the gap formed therebetween so that the amorphous soft magnetic material of each metal foil is crystalized into nano-crystal magnetic material.

Systems and methods in accordance with embodiments of the invention implement layers of devitrified metallic glass-based materials. In one embodiment, a method of fabricating a layer of devitrified metallic glass includes: applying a coating layer of liquid phase metallic glass to an object, the coating layer being applied in a sufficient quantity such that the surface tension of the liquid phase metallic glass causes the coating layer to have a smooth surface; where the metallic glass has a critical cooling rate less than 10.sup.6 K/s; and cooling the coating layer of liquid phase metallic glass to form a layer of solid phase devitrified metallic glass.