C22B21/0023

METHOD FOR RECYCLING IRON AND ALUMINUM IN NICKEL-COBALT-MANGANESE SOLUTION

The present invention relates to a method for recycling iron and aluminum in a nickel-cobalt-manganese solution. The method comprises the following steps: leaching a battery powder and removing copper therefrom to obtain a copper-removed solution, and adjusting the pH value in stages to remove iron and aluminum, so as to obtain a goethite slag and an iron-aluminum slag separately; mixing the iron-aluminum slag with an alkali liquor, and heating and stirring same to obtain an aluminum-containing solution and alkaline slag; and heating and stirring the aluminum-containing solution, introducing carbon dioxide thereto and controlling the pH value to obtain aluminum hydroxide and an aluminum-removed solution.

OBTAINING VALUABLE SOLIDS AND COMBUSTIBLE GAS FROM ALUMINUM REMELTING WASTE

Methods for obtaining solid products and combustible gas using aluminum waste are disclosed. In some embodiments, a method for obtaining solid products and combustible gas using aluminum waste may comprise: obtaining a reactive mass, the reactive mass comprising aluminum remelting waste or a derivative thereof; applying a solvent to the reactive mass to generate a solution and a first solid product; separating the solution from the first solid product; applying a reactant to at least a portion of the first solid product to initiate a reaction, the reactant being different from the solvent, the reaction generating a combustible gas and a second solid product; and separating the reactant from the second solid product.

BINDER COMPOSITION FOR SECONDARY BATTERY
20230216055 · 2023-07-06 ·

Provides an aqueous binder composition for a secondary battery electrode, comprising a copolymer and a dispersion medium, wherein the copolymer comprises a structural unit (a), a structural unit (b), and a structural unit (c). The binder composition disclosed herein has improved binding capability. In addition, battery cells comprising electrodes prepared using the binder composition disclosed herein exhibits exceptional electrochemical performance.

A METHOD FOR PROCESSING LITHIUM IRON PHOSPHATE BATTERIES

A method of processing a black mass material feed material can include a) receiving a black mass material feed material; b) acid leaching the black mass material at a pH that is less than 4, thereby producing a pregnant leach solution (PLS) comprising at least 80% the lithium from the black mass feed material, and at least a portion of the iron and the phosphorous from the black mass feed material; providing a first intermediary solution after completing step b); and separating at least 90% of the iron and the phosphorous from the first intermediary solution to provide an output solution.

METHOD FOR COMPOSITE DELAMINATION
20230136670 · 2023-05-04 ·

The invention provides a method for delaminating a composite by immersing the composite into a delamination solution; wherein the composite comprises a metal substrate and a coating applied on one side or both sides of the metal substrate, wherein the coating comprises a polymeric binder; and wherein the polymeric binder comprises an aqueous copolymer. The use of delamination solution comprising a weak base allows for complete delamination of the composite in a highly efficient and extremely fast manner. Furthermore, the delamination method disclosed herein circumvents complex separation processes, contamination and corrosion of the metal substrate and enables an excellent materials recovery. An application of the method for delaminating an electrode for a battery is disclosed herein.

METHOD FOR PRODUCING MIXED METAL SOLUTION AND METHOD FOR PRODUCING MIXED METAL SALT

A method for producing a mixed metal solution containing manganese ions and at least one of cobalt ions and nickel ions, the method including: an Al removal step of subjecting an acidic solution containing at least manganese ions and aluminum ions, and at least one of cobalt ions and nickel ions, to removal of the aluminum ions by extracting the aluminum ions into a solvent while leaving at least a part of the manganese ions in the acidic solution in an aqueous phase, the acidic solution being obtained by subjecting battery powder of lithium ion batteries to a leaching step; and a metal extraction step of bringing an extracted residual liquid obtained in the Al removal step to an equilibrium pH of 6.5 to 7.5 using a solvent containing a carboxylic acid-based extracting agent, extracting at least one of the manganese ions and at least one of the cobalt ions and the nickel ions into the solvent, and then back-extracting the manganese ions and at least one of the cobalt ions and nickel ions.

ACID DIGESTION PROCESSES FOR RECOVERY OF RARE EARTH ELEMENTS FROM COAL AND COAL BYPRODUCTS

A system for recovering rare earth elements from coal ash includes a leaching reactor, an ash dryer downstream of the leaching reactor, and a roaster downstream of the ash dryer that is cooperatively connected to both the leaching reactor and the ash dryer. Coal ash is mixed with an acid stream such that rare earth elements present in the coal ash are dissolved in the acid stream, thereby creating (i) a leachate containing the rare earth elements and (ii) leached ash. The leachate is heated to obtain acid vapor and an acid-soluble rare earth concentrate. Mixing of the coal ash with the acid stream can occur in a leaching reactor and heating of the leachate can occur in a roaster. The acid-soluble rare earth concentrate can be fed to a hydrometallurgical process to separate and purify the rare earth elements.

Hydrometallurgical Recycling of Lithium-Ion Battery Electrodes
20230187720 · 2023-06-15 ·

A green chemistry hydrometallurgical process for recovering one or more metals from a metal-containing material includes leaching the metal-containing material with formic acid, obtaining a leachate comprising the one or more metals as one or more metal formates, and precipitating at least one of the one or more metal formates. The metal-containing material may be a lithium-ion battery cathode material, resulting in Li formate remaining in solution and precipitation of salts including one or more of Ni, Co, and Mn formates. Steps may include filtration of the leachate, sulphurization of retained metal formate salts to produce metal sulphate salts, purification of filtered leachate by adding lithium carbonate and filtering, dewatering of the purified leachate, and thermal decomposition of resulting lithium salts to produce battery grade lithium carbonate. Carbon dioxide, water, and formic acid may be recovered and reused, without liquid or solid waste produced.

METHOD FOR COMPOSITE DELAMINATION
20230178820 · 2023-06-08 ·

The invention provides a method for delaminating a composite by immersing the composite into a delamination solution; wherein the composite comprises a metal substrate and a coating applied on one side or both sides of the metal substrate, wherein the coating comprises a polymeric binder; and wherein the polymeric binder comprises an aqueous copolymer. The use of delamination solution comprising an alkali metal phosphate salt allows for complete delamination of the composite in a highly efficient and extremely fast manner. Furthermore, the delamination method disclosed herein circumvents complex separation processes, contamination and corrosion of the metal substrate and enables an excellent materials recovery. An application of the method for delaminating an electrode for a battery is disclosed herein.

Novel Method for Extracting Ultra High Purity Alumina from Wastewater
20170306443 · 2017-10-26 · ·

An object of the present invention is to provide a novel method for extracting ultra high purity alumina from wastewater. Wastewater is recycled, filtered, concentrated and pretreated in order to mix with alkali solution and extraction agent PX-17, undergoing 2 times of purification, adding control agent SX-1 and high temperature heat treatment to finally obtain ultra high purity nano-alumina particles which purity reaches as 99.999% and particle size reaches as 20-200 nm.