Patent classifications
C22B7/008
METHOD FOR REUSING ACTIVE MATERIAL USING POSITIVE ELECTRODE SCRAP
There is provided a method for collecting and reusing an active material from positive electrode scrap. The method of reusing a positive electrode active material of the present disclosure includes (a-1) immersing a positive electrode scrap comprising an active material layer on a current collector into a basic solution to separate the active material layer from the current collector, (a-2) thermally treating the active material layer in air for thermal decomposition of a binder and a conductive material in the active material layer, and collecting an active material in the active material layer, (b) washing the active material collected from the step (a-2) with a lithium compound solution which is basic in an aqueous solution and drying, and (c) annealing the active material washed from the step (b) with a lithium precursor to obtain a reusable active material.
DESULFURISATION OF LEAD-CONTAINING WASTE
The present invention relates to the desulfurisation of lead-containing waste. In particular, the present invention relates to a method in which lead-containing waste is desulfurised to form a desulfurised lead-containing waste material which is suitable for recycling into lead or leady oxide. The method is particularly suitable for desulfurising lead-acid battery paste.
RECOVERY OF VANADIUM FROM ALKALINE SLAG MATERIALS
A method for the recovery of vanadium from a vanadium containing feed stream, the method comprising the steps of: subjecting the vanadium feed stream to a leach step, the leach step comprising contacting the vanadium feed stream with an alkaline carbonate leach solution to form a leach slurry comprising a pregnant leach solution containing vanadium and a solid residue; passing the leach slurry to a solid/liquid separation step to produce a pregnant leach solution containing vanadium; and recovering a vanadium product from the pregnant leach solution.
OBTAINING VALUABLE SOLIDS AND COMBUSTIBLE GAS FROM ALUMINUM REMELTING WASTE
Methods for obtaining solid products and combustible gas using aluminum waste are disclosed. In some embodiments, a method for obtaining solid products and combustible gas using aluminum waste may comprise: obtaining a reactive mass, the reactive mass comprising aluminum remelting waste or a derivative thereof; applying a solvent to the reactive mass to generate a solution and a first solid product; separating the solution from the first solid product; applying a reactant to at least a portion of the first solid product to initiate a reaction, the reactant being different from the solvent, the reaction generating a combustible gas and a second solid product; and separating the reactant from the second solid product.
METHOD FOR RECOVERING PRECIOUS METAL FROM PRECIOUS METAL-CONTAINING WASTE CATALYST
A method for recovering a precious metal from a precious metal-containing waste catalyst includes the following steps: i) at least partially dissolving a precious metal-containing waste catalyst in an alkaline aqueous solution; ii) performing filtering to obtain a precious metal-containing filtrate and a precious metal; iii) treating the filtrate with a reducing agent; and iv) separating the precious metal from the filtrate after treatment, wherein step iii) is performed under a pressure of 8-12 bar at a temperature of 190-210° C. for 2-4 h. The method provided in the present invention has a simple process and a high recovery rate. The filtrate obtained from separation comprises a precious metal of 1 ppm or less by weight.
BINDER COMPOSITION FOR SECONDARY BATTERY
Provides an aqueous binder composition for a secondary battery electrode, comprising a copolymer and a dispersion medium, wherein the copolymer comprises a structural unit (a), a structural unit (b), and a structural unit (c). The binder composition disclosed herein has improved binding capability. In addition, battery cells comprising electrodes prepared using the binder composition disclosed herein exhibits exceptional electrochemical performance.
METHOD FOR THERMAL BARRIER COATING PRODUCTION BY RECYCLING THERMAL BARRIER COATING MATERIALS
Disclosed are methods to produce Thermal Barrier Coating (TBC) products using materials recycled from TBC waste. These methods include ways to produce zirconium and rare earth chemicals and raw materials appropriate for producing TBC materials.
METHOD AND APPARATUS FOR PRODUCING VANADIUM COMPOUND, AND METHOD AND APPARATUS FOR PRODUCING REDOX-FLOW BATTERY ELECTROLYTE
A production method includes: an alkali extraction step of adding an alkali and water, or an alkali solution, to raw material ash containing an ammonium sulfate component, sulfuric acid, vanadium, and at least one other metal selected from nickel, iron, and magnesium, wherein a pH of 13 or higher is achieved, to obtain an alkali leachate; a solid-liquid separation step on the alkali leachate to obtain a leach filtrate containing vanadium; an evaporation concentration step of evaporating and concentrating the leach filtrate to obtain a concentrated liquid; and a crystallization/solid-liquid separation step of cooling and crystalizing the concentrated liquid and recovering a precipitate containing a vanadium compound. Another production method includes an alkali extraction step, a solid-liquid separation step, an evaporation concentration step, an alkali concentration adjustment step of further adding an alkali or alkali solution to a concentrated liquid to obtain a concentration-adjusted liquid, and a crystallization/solid-liquid separation step.
METHOD OF SELECTIVELY REMOVING ALUMINUM FROM WASTE ELECTRODE AND A METHOD OF REMOVING METAL COMPONENTS FROM THE WASTE ELECTRODE USING THE METHOD
A method of removing aluminum from a waste electrode. The method includes comminuting the waste electrode containing a waste current collector and an electrode active material. The method further includes screening the comminuted waste electrode to collect the electrode active material. The method further includes mixing the electrode active material and an alkaline solution to remove aluminum impurities in the electrode active material.
PROCESS FOR THE RECOVERY OF LITHIUM AND OTHER METALS FROM WASTE LITHIUM ION BATTERIES
A process for the recovery of one or more transition metals and lithium from waste lithium ion batteries or parts thereof is disclosed. The process comprising the steps of (a) providing a particulate material containing a transition metal compound and/or transition metal, wherein the transition metal is selected from the group consisting of Ni and Co, and wherein further at least a fraction of said Ni and/or Co, if present, are in an oxidation state lower than +2, e.g. in the metallic state; which particulate material further contains a lithium salt; (b) treating the material provided in step (a) with a polar solvent and optionally an alkaline earth hydroxide; (c) separating the solids from the liquid, optionally followed by a solid-solid separation step; and (d) treating the solids containing the transition metal in a smelting furnace to obtain a metal melt containing Ni and/or Co provides good separation of transition metal as alloy and of lithium in high purity.