A pure copper powder with a Si coating formed thereon, wherein a Si adhesion amount is 5 wtppm or more and 200 wtppm or less, a C adhesion amount is 15 wtppm or more, and a weight ratio C/Si is 3 or less. An object of the present invention is to provide a pure copper powder with a Si coating formed thereon and a production method thereof, as well as an additive manufactured object using such pure copper powder capable of suppressing the partial sintering of the pure copper powder caused by the preheating thereof in additive manufacturing based on the electron beam (EB) method, and suppressing the loss of the degree of vacuum caused by carbon (C) during the molding process.

Method of manufacturing zirconium alloy tubular products containing (wt. %): niobium—0.9-1.7; iron—0.04-0.10; oxygen—0.03-0.10; silicon—less than 0.02, carbon—less than 0.02, and zirconium—as the base of the alloy. This includes an ingot melting by multiple vacuum arc remelting, mechanical processing of the ingot, heating, hot working of the ingot, subsequent mechanical processing for the production of tubular billets, heat treatment of the tubular billets, application of a protective coating and heating to a hot pressing temperature, hot pressing, removal of the protective coating, multi-stage cold radial forging, vacuum thermal treatment, multiple cold rolling runs with a total deformation degree of 50-80-% per run and a tubular coefficient of Q=1.0-2.7 with intermediate vacuum thermal treatment after each cold rolling operation, and final vacuum thermal treatment of the resulting tubular products carried out at the final size with subsequent final finishing operations.

Manufacturing method for tubular products made of zirconium-based alloy includes melting an ingot by multiple vacuum arc remelting, mechanical processing of the ingot, heating, multi-stage hot forging of the ingot for production of a forged piece, subsequent mechanical processing of the forged piece for production of the a round-profile blank, manufacturing of tubular billets, their quenching and tempering, application of a protective coating, heating to a hot pressing temperature, hot pressing, removal of the protective coating, vacuum thermal treatment, multiple cold rolling steps in order to produce tubular products, with intermediate vacuum thermal treatment after each cold rolling, and a final vacuum thermal treatment being carried out at a final size with subsequent final finishing operations. The tubular products can be used as the structural components of a core in water-cooled nuclear reactors. The method can provide increased processibility, high strength, and corrosion resistance of tubular products.

Manufacturing method for zirconium alloy tubular products containing (% wt.): niobium—0.9-1.7; iron—0.10-0.20; oxygen—0.10-0.20; silicon—less than 0.02, carbon—less than 0.02, zirconium—the alloy base. The method includes melting an ingot by multiple vacuum arc remelting, mechanical processing of the ingot, heating, multi-stage hot forging for production of the forged piece, subsequent mechanical processing of the forged piece for production of tubular billets with vacuum thermal treatment, application of a protective coating, heating to a hot pressing temperature, hot pressing, removal of the protective coating, vacuum thermal treatment, multiple cold rolling steps with a total deformation degree of 58-74% per run and a tubular coefficient of Q=1.18-2.01, with intermediate vacuum thermal treatment in order to produce tubular products, and final vacuum thermal treatment being carried out at the final size with subsequent final finishing operations.

Producing a Ni superalloy component in which the superalloy has a γ phase matrix containing intermetallic γ′ precipitates. Providing a Ni superalloy casting of the component; solutioning the component by heat treating the casting under vacuum and/or in an inert atmosphere at a temperature above the γ′ solvus to homogenize the γ phase; quenching and ageing the solutioned component to grow intermetallic γ′ precipitates in the homogenized γ phase. Before the solutioning step: heat treating the casting to produce a thermally grown oxide on the surface, oxide adherent to supress volatilization of Ni from the surface of the casting during the solutioning heat treatment. Performing the solutioning step under a Ni vapor pressure which is sufficient to supress volatilization of Ni from the surface of the casting during the solutioning heat treatment. During the solutioning heat treatment the component is encapsulated in a container protecting the casting from Si-doped contaminants.

A method for protecting a metal during an annealing process, the metal being in the form of a coil or sheets, including placing a protective film between adjacent surfaces of the wraps of the coil or of the sheets, such that the protective film separates the adjacent surfaces of the metal. The metal is subjected with the protective film to the annealing process, the protective film being resistant to temperatures between 200° C. and 360° C. A metal product is obtained by this method.

Medical instruments, particularly, endodontic instruments with unique limited memory characteristics, and methods for making such instruments. One embodiment includes heat treating a finished endodontic instrument. A related embodiment includes electropolishing a finished endodontic instrument and then heat treating the endodontic instrument.

A method for manufacturing a balance spring intended to equip a balance of a horological movement, including a step of producing a blank made of a Nb—Zr alloy including between 10 and 30 wt % Zr, a step of annealing and cooling the blank, at least one step of deforming the annealed blank in order to form a wire, wherein, before the deformation step, a step of depositing, on the blank, a layer of a ductile material chosen from copper, nickel, cupronickel, cupro-manganese, gold, silver, nickel-phosphorus Ni—P and nickel-boron Ni—B, in order to facilitate the wire shaping operation, the thickness of the ductile material layer deposited being chosen such that the ratio of the area of ductile material to the area of the alloy for a given wire cross-section is less than 1, preferably less than 0.5, and more preferably lies in the range 0.01 to 0.4.

An insert fixture for use in the manufacture of a single crystal component by a hot isostatic pressing process. The insert fixture comprising: at least a lower plate separated from an upper plate by interconnecting members. The upper plate comprises at least a slot for the insertion of the single crystal component. The lower plate features a related engagement feature for engaging with the single crystal component. The insert fixture may be cast from a ceramic material. The insert fixture may be cast from an alumina ceramic or molybdenum alloy. The interconnecting members may be made from a molybdenum alloy.

A surface of a metal substrate formed from a metal is heated, an oxide film is formed on the surface of the metal substrate, at least a portion of the oxide film is heated so as to increase a joining strength of the oxide film to the metal substrate, subsequently a synthetic resin substrate formed from a synthetic resin is joined to the oxide film, and thus a metal-resin joined body is obtained. Thereby, a metal-resin joined body having high joining strength is obtained.