A fine cellulose fiber composite in which a modifying group is bound to a carboxy group of fine cellulose fibers, the fine cellulose fibers having a carboxy group content of 0.1 mmol/g or more, wherein the fine cellulose fiber composite has an average aspect ratio of 1 or more and 150 or less; and a resin composition containing the fine cellulose fiber composite and a resin. The resin composition containing a fine cellulose fiber composite of the present invention has excellent heat resistance, and the molded article of this resin composition has excellent mechanical strength, heat resistance, and dimensional stability. Accordingly, the present invention can be suitably used in various industrial applications such as daily sundries, household electric appliance parts, wrapping materials for household electric appliance parts, and automobile parts.

A fine cellulose fiber composite in which a modifying group is bound to a carboxy group of fine cellulose fibers, the fine cellulose fibers having a carboxy group content of 0.1 mmol/g or more, wherein the fine cellulose fiber composite has an average aspect ratio of 1 or more and 150 or less; and a resin composition containing the fine cellulose fiber composite and a resin. The resin composition containing a fine cellulose fiber composite of the present invention has excellent heat resistance, and the molded article of this resin composition has excellent mechanical strength, heat resistance, and dimensional stability. Accordingly, the present invention can be suitably used in various industrial applications such as daily sundries, household electric appliance parts, wrapping materials for household electric appliance parts, and automobile parts.

Provided by the present invention is a method for simultaneously dyeing and flame-retardant finishing a polyester-based fiber product, which is excellent regarding dyeing reproducibility, the method including immersing and heating a polyester-based fiber product in a processing bath containing a specific yellow disperse dye and a phosphoramidate represented by Formula (V):

##STR00001##

Provided by the present invention is a method for simultaneously dyeing and flame-retardant finishing a polyester-based fiber product, which is excellent regarding dyeing reproducibility, the method including immersing and heating a polyester-based fiber product in a processing bath containing a specific yellow disperse dye and a phosphoramidate represented by Formula (V):

##STR00001##

Method for sulphation and phosphorylation of a cellulose substrate for imparting anti-flame properties to the substrate in which at least one phosphonic acid of formula (I):
PO(OH).sub.2—R—PO(OH).sub.2,   (I)
is used as a catalyst of sulphation and a phosphorylating agent and relative substrate.

Method for sulphation and phosphorylation of a cellulose substrate for imparting anti-flame properties to the substrate in which at least one phosphonic acid of formula (I):
PO(OH).sub.2—R—PO(OH).sub.2,   (I)
is used as a catalyst of sulphation and a phosphorylating agent and relative substrate.

A flame retardant composition containing a phosphorous containing ammonium salt, a crosslinker, and water is provided, and its application to yarn or fabric to provide a flame retardant yarn or fabric. In a preferred embodiment, the yarn or fabric is made from a polyurethane elastomer, such as a spandex. A method to prepare the flame retardant composition and apply it to the fiber or yarn is also provided.

A type of flame-retardant cellulosic fiber and a preparation method thereof are disclosed. The preparation method includes extruding the cellulosic solution through a spinneret, coagulating, stretching, and water-washing to obtain a water-washed filament, which is then treated with a flame-retardant solution, and then rinsed and dried to prepare the flame-retardant cellulosic fiber. The water-washing temperature is 90° C., the temperature of the flame-retardant solution during treatment is 60-90° C., and the rinsing temperature is 20-40° C. The flame retardant contains more than one of a group that forms a covalent bond with a hydroxy group of the cellulosic macromolecule, a group having the ability of self-crosslinking reaction, and a group that forms a hydrogen bond with a hydroxy group of the cellulosic macromolecule. The prepared flame-retardant cellulosic fiber is mainly composed of the cellulosic fiber matrix and the flame retardant dispersed in the matrix.

A type of flame-retardant cellulosic fiber and a preparation method thereof are disclosed. The preparation method includes extruding the cellulosic solution through a spinneret, coagulating, stretching, and water-washing to obtain a water-washed filament, which is then treated with a flame-retardant solution, and then rinsed and dried to prepare the flame-retardant cellulosic fiber. The water-washing temperature is ≤90° C., the temperature of the flame-retardant solution during treatment is 60-90° C., and the rinsing temperature is 20-40° C. The flame retardant contains more than one of a group that forms a covalent bond with a hydroxy group of the cellulosic macromolecule, a group having the ability of self-crosslinking reaction, and a group that forms a hydrogen bond with a hydroxy group of the cellulosic macromolecule. The prepared flame-retardant cellulosic fiber is mainly composed of the cellulosic fiber matrix and the flame retardant dispersed in the matrix.

A flame retardant aid includes an amphoteric polymer compound having at least one of a specific cationic unit such as allylamine, and an anionic unit such as maleic acid, and a flame retarding agent composition including the flame retardant aid. A method of producing a flame-retardant fiber fabric includes treating a polyester fiber fabric using a flame retardant aid including a flame retardant component and the above amphoteric polymer compound, and drying the polyester fiber fabric.