F25J2200/06

CRYOGENIC AIR SEPARATION UNIT WITH ARGON CONDENSER VAPOR RECYCLE
20230050296 · 2023-02-16 ·

A system and method for producing two or more nitrogen product streams and a crude argon stream from a nitrogen and argon producing air separation unit is provided. The disclosed embodiments of the cryogenic-based nitrogen and argon producing air separation units and associated air separation cycles include the means for directing a first portion of a boil-off stream from an argon condenser of the air separation unit to a waste expansion refrigeration circuit and concurrently recycling a second portion of the boil-off stream from the argon condenser to the main air compression system of the air separation unit to be mixed or blended with the incoming feed air. Optionally, a third portion of the boil-off stream from the argon condenser may be further compressed in a cold compressor and returned to the lower pressure column.

APPARATUS FOR OPERATING AN AIR SEPARATION PLANT

An apparatus for the production of air gases with variable liquid production by the cryogenic separation of air can include a cold box having a heat exchanger, and a system of columns; a pressure monitoring device; and a controller. The cold box can be configured to receive a purified and compressed air stream under conditions effective for cryogenically separating the air stream to form an air gas product. The apparatus may also include means for transferring the air gas product from the cold box to an air gas pipeline. The pressure monitoring device is configured to monitor the pipeline pressure, and the controller is configured to adjust the product pressure of the air gas product coming out of the cold box based upon the pipeline pressure and to further adjust liquid production from the cold box based on the adjusted product pressure.

System and Method for Separating Methane and Nitrogen with Reduced Horsepower Demands
20230235955 · 2023-07-27 ·

A system and method for removing nitrogen from natural gas using two fractionating columns, that may be stacked, and a plurality of separators and heat exchangers, with horsepower requirements that are 50-80% of requirements for prior art systems. The fractionating columns operate at different pressures. A feed stream is separated with a vapor portion feeding the first column to produce a first column bottoms stream that is split into multiple portions at different pressures and first column overhead stream that is split or separated into two portions at least one of which is subcooled prior to feeding the top of the second column. Optional heat exchange between first column and second column streams provides first column reflux and reboil heat for a second column ascending vapor stream. Three sales gas streams are produced, each at a different pressure.

PROCESS TO SEPARATE NITROGEN FROM METHANE BY PERMEATION AND CRYOGENIC DISTILLATION

A process for the separation of nitrogen from a feed stream containing at least methane and nitrogen, with a methane content between 4 and 12% mol. consists of at least the following steps: separation of the feed stream by means of a rubbery-type membrane to produce a permeate enriched in methane at a pressure greater than 2 bara and a non-permeate which is a nitrogen-enriched residue gas at a pressure greater than 2 bara and processing of the high-pressure residue gas in a cryogenic separation unit to produce a methane rich liquid and a nitrogen-enriched gas wherein the pressure of the membrane permeate is controlled as a function of the nitrogen concentration in the nitrogen-enriched gas.

Cryogenic air separation apparatus

A cryogenic air separation apparatus comprises: a heat exchanger, a first rectification column, a first condenser, a second rectification column, a third rectification column, a second condenser, a high-purity oxygen rectification column, a third condenser, a nitrogen compressor, and a compressed recycled gas line L52 for introducing product nitrogen gas compressed by the first nitrogen compressor into a warm end (heat source) of an ultra-high-purity oxygen vaporizer as a compressed recycled gas.

Producing LNG from Methane Containing Synthetic Gas

Described herein are methods and systems for producing liquefied natural gas (LNG) from a methane-containing synthetic gas (MCSG). An MCSG feed stream may be cooled and partially liquefied using one or more heat exchanger units. A first phase separator and a second phase separator in downstream fluid flow communication with the first phase separator may be used to separate the partially liquefied MCSG stream into a first residue gas stream and first and second feed streams, the first and second feed streams then being fed into a distillation column to produce an LNG stream and a second residue gas stream.

FACILITY FOR THE SEPARATION AND LIQUEFACTION OF METHANE AND CO2 COMPRISING A VAPO/CONDENSER PLACED IN AN INTERMEDIATE STAGE OF THE DISTILLATION COLUMN
20220397343 · 2022-12-15 ·

A combined plant for cryogenic separation and liquefaction of methane and carbon dioxide in a biogas stream, including a mixing means, a compressor, a first exchanger, a distillation column, a second exchanger, a separating means, an expanding means, and a separator vessel. Wherein, the mixing means is configured such that the recycle gas is the overhead vapour stream, and the first exchanger and the expanding means are combined.

NITROGEN PRODUCING CRYOGENIC AIR SEPARATION UNIT WITH EXCESS AIR CIRCUIT
20230055205 · 2023-02-23 ·

A nitrogen producing cryogenic air separation unit with an excess air circuit is provided. The nitrogen producing cryogenic air separation unit is capable of producing high pressure gaseous nitrogen without the use of a nitrogen product compressors and is also capable of producing high rates of liquid nitrogen without adding additional compression stages in the main air compressor and/or without a nitrogen recycle compressor.

Method for cryogenic separation of air, and air separation plant
11602713 · 2023-03-14 · ·

A method for cryogenic separation of air uses an air separation plant, wherein, in a mass transfer column, a liquid first fluid and a gaseous second fluid are subjected to mass transfer with one another. A gaseous third fluid is removed from the column and is at least partly discharged from the air separation plant. A liquid fourth fluid is removed from the column and is at least partly fed into a low-pressure column. The first fluid is formed using at least a part of an oxygen-rich liquid removed from the low-pressure column. The second fluid is formed using an oxygen-enriched liquid removed from a high-pressure column. The oxygen-enriched liquid removed from the high-pressure column and bottom liquid of the mass transfer column are mixed and partly evaporated in a condenser-evaporator. A liquid fifth fluid is removed from the mass transfer column between a feed point for the first fluid and a feed point for the oxygen-enriched liquid, and is at least partly fed into the low-pressure column. The fifth fluid or a fraction thereof is fed into the low-pressure column below the fourth fluid or a fraction thereof.

METHOD FOR SEPARATING A MIXTURE CONTAINING AT LEAST NITROGEN AND METHANE
20220325951 · 2022-10-13 ·

A method for separating a mixture containing at least nitrogen and methane by cryogenic distillation in a first column operating in a first pressure and a second column operating at a second pressure lower than the first pressure, the mixture being separated in the first column to form a gas enriched in nitrogen and a liquid enriched in methane, at least a portion of the gas enriched in nitrogen being at least partially condensed in a heat exchanger and returned to the first column, the gas enriched in nitrogen is sent into the heat exchanger by the bottom, ascends in a first series of passages of the exchanger and condenses therein at least partially, the liquid formed descending in these passages of the first series and exiting by the bottom of the exchanger.