A system and method for improving the performance of an oxygen, nitrogen, and argon producing air separation unit configured to produce a gaseous nitrogen product stream is provided. By recycling the argon condenser boil-off vapor stream to the main air compression train, the argon recovery and oxygen recovery while maintaining the production level of a medium or high pressure gaseous nitrogen product stream. In addition, some operational cost savings in terms of lower power costs can also be realized compared to some prior art oxygen, nitrogen, and argon producing air separation units.

A method for obtaining one or more air products by means of an air separation unit comprising a first booster, a second booster, a first decompression machine, and a rectification column system which has a high-pressure column operated at a first pressure level and a low-pressure column operated at a second pressure level below the first pressure level. All of the air supplied to the rectification column system is first compressed to a third pressure level, which lies at least 3 bar above the first pressure level, as a feed air quantity. A first fraction of the feed air quantity is supplied to a first booster at the third pressure level and at a temperature level of −140 to −70 ° C. and is compressed to a fourth pressure level using the first booster.

Enhancements to a dual column, nitrogen producing cryogenic air separation unit with waste expansion are provided. Such enhancements include an improved air separation cycle that uses: (i) three condenser-reboilers; (ii) a reverse reflux stream from the condenser-reboiler associated with the lower pressure column to the higher pressure column; and (iii) a recycle stream of a portion of the vapor from one or more of the condenser-reboilers that is recycled back to the incoming feed stream and or the compressed purified air streams to yield improvements in the performance of such dual column, nitrogen producing cryogenic air separation units in terms of overall nitrogen recovery as well as power consumption compared to conventional dual column, nitrogen producing cryogenic air separation units employing waste expansion.

A method for obtaining one or more air products, in which method an air fractionation plant is used which has a column system with a pressure column, wherein air is fedto the column system and is fractionated in the column system, wherein at least 90% of the total amount of air supplied to the column system is compressed, wherein nitrogen-rich gas is extracted from the pressure column, and wherein, at least in a first operating mode, further air is compressed to a pressure level above the base pressure level, is expanded, and is warmed without fractionation in the column system. It is provided that, at least in the first operating mode, a proportion of the nitrogen-rich gas extracted from the pressure column is fed to the further air upstream of the expansion.

Xenon and/or krypton is separated from a liquid oxygen stream comprising oxygen and xenon and/or krypton in a process comprising providing at least a portion of the liquid oxygen stream as a reflux liquid to the top of a rare gas recovery column operated at a pressure of between 5 to 25 bara, vaporizing a reboiler liquid in the reboiling zone in the bottom of the rare gas recovery column to produce a mixture of a rising vapor and a xenon and/or krypton-enriched liquid stream; and contacting the rising vapor with the reflux liquid in at least one distillation zone of the column to effect stripping xenon and/or krypton from the rising vapor to the reflux liquid. The process provides a recovery of xenon of greater than 90% and a krypton recovery of 15% to 90%.

The invention proposes a process and an air separation plant comprising a rectification column system comprising a high-pressure column, a low-pressure column, a main heat exchanger, and a main air compressor. The total air supplied to the rectification column system is compressed in the main air compressor to a first pressure level. The high-pressure column is operated at a second pressure level, at least 3 bar below the first pressure level. A gaseous, nitrogen-rich fluid is removed from the high-pressure column and warmed up in the gaseous state without prior liquefaction. A first partial quantity of the gaseous, nitrogen-rich fluid is warmed to a first temperature level of −150 to −100° C., supplied at this first temperature level to a booster and compressed further to a third pressure level. The first partial quantity is then warmed to a second temperature level and discharged from the air separation plant.

Xenon and/or krypton is separated from a liquid oxygen stream comprising oxygen and xenon and/or krypton in a process comprising providing at least a portion of the liquid oxygen stream as a reflux liquid to the top of a rare gas recovery column operated at a pressure of between 5 to 25 bara, vaporizing a reboiler liquid in the reboiling zone in the bottom of the rare gas recovery column to produce a mixture of a rising vapor and a xenon and/or krypton-enriched liquid stream; and contacting the rising vapor with the reflux liquid in at least one distillation zone of the column to effect stripping xenon and/or krypton from the rising vapor to the reflux liquid. The process provides a recovery of xenon of greater than 90% and a krypton recovery of 15% to 90%.

Provided are a method and apparatus for producing nitrogen and oxygen by means of cryogenic distillation of air. Nitrogen products are extracted only from the top of a tower. If a customer needs nitrogen with lower pressure, part of pure nitrogen that is partially located at a first nitrogen product pressure is reheated in a main heat exchanger, then decompressed to a second nitrogen product pressure by means of a nitrogen expander, further reheated by means of the main heat exchanger, and output as a low-pressure nitrogen product. The nitrogen expander can be braked by an expander booster for compressing air. By means of the method, nitrogen with different pressures can be suitably produced, and the energy consumption for producing the pressurized air can be reduced by utilizing the expansion work of nitrogen.

Various embodiments include an apparatus for liquefying gas comprising: an inlet for a pressurized gas; a countercurrent heat exchanger with a first channel for the pressurized gas to flow in a first direction; an expansion nozzle, such that the pressurized gas flows from the first channel into the nozzle, and flows out to form an aerosol comprising a gaseous phase and liquid droplets; an aerosol breaker separating at least some of the droplets out of the gaseous phase; a collecting region for gathering and collecting droplets dripping off the aerosol breaker; and a second channel of the countercurrent heat exchanger surrounding the first channel. The flow of the gaseous phase out of the expansion nozzle is colder compared to the gas flowing through the second channel in a second direction opposite to the first direction. The second channel surrounds the first channel. The apparatus comprises a monolithic structure.

A system and method for improving the performance of an oxygen, nitrogen, and argon producing air separation unit configured to produce a gaseous nitrogen product stream is provided. By recycling the argon condenser boil-off vapor stream to the main air compression train, the argon recovery and oxygen recovery while maintaining the production level of a medium or high pressure gaseous nitrogen product stream. In addition, some operational cost savings in terms of lower power costs can also be realized compared to some prior art oxygen, nitrogen, and argon producing air separation units.