Patent classifications
F25J3/04703
FULL LIQUID-PRODUCT AIR SEPARATION EQUIPMENT AND PROCESS THEREFOR
A full liquid-product air separation equipment is disclosed. The equipment comprises an air filtration system, a compression system, a precooling system, a purification system, a high-temperature expander having a first pressurizing part and a first expanding part, a low-temperature expander having a second pressurizing part and a second expanding part, a main heat exchanger having a first heat exchange pipeline, a second heat exchange pipeline, a third heat exchange pipeline, a fourth heat exchange pipeline and a fifth heat exchange pipeline, and a rectification system for rectifying air. The equipment has a simple configuration, is easy to implement, and has high gas separation efficiency and low energy consumption.
SYSTEM FOR PURIFYING ARGON BY CRYOGENIC DISTILLATION
System for purifying argon by cryogenic distillation, comprising a single column surmounted by a top-end condenser, a fluid inlet in the lower part of the column, a fluid outlet in the upper part of the column, and N distillation sections where N≥4, of which at least the two uppermost sections of the column are equipped respectively with a first liquid distributor and with a second liquid distributor, the second distributor being capable of performing a function of mixing together liquids that fall onto the distributor, each of the first and second distributors being positioned above the respective section and of which the two lowermost sections of the column are respectively equipped with a (N−1)th and an Nth liquid distributor capable of performing a function of mixing together liquids that fall onto the distributor, and which is arranged above the respective section, the first, second, (N−1)th and Nth distributors each being dimensioned to contain a maximum height of liquid head, that (those) of the first and second distributors being greater than that (those) of the (N−1)th and Nth distributors.
System and method for flexible recovery of argon from a cryogenic air separation unit
A system and method for flexible production of argon from a cryogenic air separation unit is provided. The cryogenic air separation unit is capable of operating in a ‘no-argon’ or ‘low-argon’ mode when argon demand is low or non-existent and then switching to operating in a ‘high-argon’ mode when argon is needed. The recovery of the argon products from the air separation unit is adjusted by varying the percentages of dirty shelf nitrogen and clean shelf nitrogen in the reflux stream directed to the lower pressure column. The cryogenic air separation unit and associated method also provides an efficient argon production/rejection process that minimizes the power consumption when the cryogenic air separation unit is operating in a ‘no-argon’ or ‘low-argon’ mode yet maintains the capability to produce higher volumes of argon products at full design capacity to meet argon product demands.
METHOD AND DEVICE FOR VARIABLY OBTAINING ARGON BY MEANS OF LOW-TEMPERATURE SEPARATION
A method and device to variably obtain argon by means of low-temperature separation. Feed air is cooled in a main heat exchanger and then conducted into a distillation column system with a high-pressure column and a low-pressure column. Argon is obtained using a crud argon column and a purified argon column. A purified liquid argon product flow is generated from an argon-enriched flow from the low-pressure column. In a first operating mode, a first quantity of purified argon product is discharged, and in a second operating mode, a reduced quantity of purified argon product is discharged. In the second operating mode, a gaseous argon return flow is drawn from the crude argon column or the purified argon column and heated in a separate passage of the main heat exchanger.
SYSTEM AND METHOD FOR FLEXIBLE RECOVERY OF ARGON FROM A CRYOGENIC AIR SEPARATION UNIT
A system and method for flexible production of argon from a cryogenic air separation unit is provided. The cryogenic air separation unit is capable of operating in a ‘no-argon’ or ‘low-argon’ mode when argon demand is low or non-existent and then switching to operating in a ‘high-argon’ mode when argon is needed. The recovery of the argon products from the air separation unit is adjusted by varying the percentages of dirty shelf nitrogen and clean shelf nitrogen in the reflux stream directed to the lower pressure column. The cryogenic air separation unit and associated method also provides an efficient argon production/rejection process that minimizes the power consumption when the cryogenic air separation unit is operating in a ‘no-argon’ or ‘low-argon’ mode yet maintains the capability to produce higher volumes of argon products at full design capacity to meet argon product demands.
Air separation unit by cryogenic distillation
An air separation unit using cryogenic distillation comprises a first column, a second column thermally linked to the first column, a first argon column, a second argon column, means for sending cooled, compressed and purified air to at least the first column, means for sending at least one fluid enriched in nitrogen from the first column to the second column and at least one fluid enriched in oxygen from the first column to the second column, means for sending a gas enriched in argon from the second column to a first end of the first argon column, means for sending gas from a second end of the first argon column to a first end of the second argon column, means for removing argon rich fluid from a second end of the second argon column, a pump, means for removing argon enriched liquid from the first end of the second argon column and sending it to the second end of the first argon column via the pump, the first end of the first argon column being raised above the ground by a first supporting structure, the pump being positioned within the first supporting structure, such that the pump is at least partially underneath the first end of the first argon column.
AIR SEPARATION UNIT BY CRYOGENIC DISTILLATION
An air separation unit using cryogenic distillation comprises a first column, a second column thermally linked to the first column, a first argon column, a second argon column, means for sending cooled, compressed and purified air to at least the first column, means for sending at least one fluid enriched in nitrogen from the first column to the second column and at least one fluid enriched in oxygen from the first column to the second column, means for sending a gas enriched in argon from the second column to a first end of the first argon column, means for sending gas from a second end of the first argon column to a first end of the second argon column, means for removing argon rich fluid from a second end of the second argon column, a pump, means for removing argon enriched liquid from the first end of the second argon column and sending it to the second end of the first argon column via the pump, the first end of the first argon column being raised above the ground by a first supporting structure, the pump being positioned within the first supporting structure, such that the pump is at least partially underneath the first end of the first argon column.
METHOD FOR FLEXIBLE RECOVERY OF ARGON FROM A CRYOGENIC AIR SEPARATION UNIT
A method for flexible production of argon from a cryogenic air separation unit is provided. The disclosed cryogenic air separation unit is capable of operating in a ‘no-argon’ or ‘low-argon’ mode when argon demand is low or non-existent and then switching to operating in a ‘high-argon’ mode when argon is needed. The recovery of the argon products from the air separation unit is adjusted by varying the percentages of dirty shelf nitrogen and clean shelf nitrogen in the reflux stream directed to the lower pressure column. The cryogenic air separation unit and associated method also provides an efficient argon production/rejection process that minimizes the power consumption when the cryogenic air separation unit is operating in a ‘no-argon’ or ‘low-argon’ mode yet maintains the capability to produce higher volumes of argon products at full design capacity to meet argon product demands.
METHOD FOR STARTING UP AN ARGON SEPARATION COLUMN OF AN APPARATUS FOR AIR SEPARATION BY CRYOGENIC DISTILLATION AND UNIT FOR IMPLEMENTING THE METHOD
A unit for producing argon by cryogenic distillation, suitable for connection to a double air separation column consisting of first and second columns interconnected thermally, comprises an argon separation column surmounted with a top condenser and a denitrogenation column, means for withdrawing an argon-rich and nitrogen-depleted product (LAR) at the bottom of the denitrogenation column, means for connecting the top of the argon separation column to the denitrogenation column, means for sending a top gas from the argon separation column to the atmosphere, means for withdrawing a nitrogen-rich fluid from the top of the denitrogenation column, an analyser for measuring the nitrogen content at the top of the argon separation column, and means for opening and closing the means for connecting the top of the argon separation column to the denitrogenation column depending on the nitrogen content detected by the analyser.
AIR SEPARATION UNIT BY CRYOGENIC DISTILLATION
An air separation unit using cryogenic distillation comprises a first column, a second column thermally linked to the first column, a first argon column, a second argon column, means for sending cooled, compressed and purified air to at least the first column, means for sending at least one fluid enriched in nitrogen from the first column to the second column and at least one fluid enriched in oxygen from the first column to the second column, means for sending a gas enriched in argon from the second column to a first end of the first argon column, means for sending gas from a second end of the first argon column to a first end of the second argon column, means for removing argon rich fluid from a second end of the second argon column, a pump, means for removing argon enriched liquid from the first end of the second argon column and sending it to the second end of the first argon column via the pump, the first end of the first argon column being raised above the ground by a first supporting structure, the pump being positioned within the first supporting structure, such that the pump is at least partially underneath the first end of the first argon column.