F25J3/04793

METHOD FOR THE PRODUCTION OF AIR GASES BY THE CRYOGENIC SEPARATION OF AIR WITH VARIABLE LIQUID PRODUCTION AND POWER USAGE

A method for the production of air gases by the cryogenic separation of air can include the steps of sending a purified and compressed air stream to a cold box under conditions effective for cryogenically separating the air stream into oxygen and nitrogen using a system of columns, wherein the purified and compressed air stream is at a feed pressure when entering the system of columns; withdrawing the oxygen at a product pressure; delivering the oxygen at a delivery pressure to an oxygen pipeline, wherein the oxygen pipeline has a pipeline pressure; and monitoring the pipeline pressure. The method can also include a controller configured to determine whether to operate in a power savings mode or a variable liquid production mode. By operating the method in a dynamic fashion, a power savings and/or additional high value cryogenic liquids can be realized in instances in which the pipeline pressure deviates from its highest value.

Modelling of a distillation column with operating state changes
11698225 · 2023-07-11 · ·

A method is provided for determining a state of a distillation column having multiple column stages for separating a feed fluid stream into individual fluid components. The state is determined by means of a model in a manner dependent on pressure differences prevailing between adjacent column stages. In the model, both gaseous and liquid flows between adjacent column stages are brought about by the pressure differences prevailing between adjacent column stages. A substance quantity flow characterizing gaseous flow between two column stages is given by {dot over (N)}.sub.V.Math.R.sub.V=C.sub.V.Math.Δp.sub.V. A substance quantity flow characterizing liquid flow between two column stages is given by {dot over (N)}.sub.L.Math.R.sub.L=C.sub.L.Math.Δp.sub.L. Δp.sub.V,L is a total pressure difference between two adjacent column stages. R.sub.V,L is a coefficient of resistance between two adjacent column stages and C.sub.V,L is a conductance value of flow between two adjacent column stages.

METHOD AND APPARATUS FOR TRANSFER OF LIQUID

A method and apparatus for transferring a first liquid removed from an outlet of a first distillation column to an inlet of a second distillation column is provided. The second distillation column operates at a higher pressure than the first distillation column, and the inlet of the second distillation column is at higher elevation as compared to the outlet of the first distillation column. The method advantageously transfers the first liquid from the outlet to the inlet by mixing with a sufficient amount of a lower density second liquid that results in a mixed liquid having a reduced density as compared to the first liquid.

PRODUCT GAS SUPPLY QUANTITY ADJUSTMENT DEVICE AND AIR SEPARATION APPARATUS COMPRISING SAME

A supply quantity adjustment device 500 comprises: a total demand quantity calculation unit 502 that calculates a total demand quantity used at a supply destination, based on plant information; an excess/deficit information setting unit 503 that compares the total demand quantity and a flow rate set value and sets a first calculated pressure value; a backup coefficient setting unit that sets a backup coefficient set value based on a reference gasholder pressure, the first calculated pressure value, a reference backup pressure set value, and a measured gasholder pressure value; and a production coefficient setting unit that compares a production pressure set value obtained by adding the reference gasholder pressure and a first pressure output value with the measured gasholder pressure value, and sets a production coefficient so as to modify a variation in the quantity of product gas produced by the air separation apparatus.

METHOD AND APPARATUS FOR IMPROVING EFFICIENCY OF A FRONT-END PURIFICATION UNIT OF AN AIR SEPARATION PLANT

A method and apparatus for reducing heat bumps following regeneration of adsorbers in an air separation unit is provided. Certain embodiments of the current invention utilize the two waste streams available at very different temperatures from the two main exchangers (low-pressure and high-pressure core exchangers) for regeneration of the front-end purification adsorbers in the air separation unit (ASU) to reduce its energy consumption without compromising the stability of process. Certain embodiments help to eliminate/minimize high air temperature disturbance (heat bump) for the process downstream of the front-end purification unit during the transition from offline to online.

Method for utilizing waste air to improve the capacity of an existing air separation unit

A method for improving the capacity of an existing air separation unit employing a lost air turbine is provided in which the capacity is increased by operating the existing air separation unit as previously operated, with the exception of collecting the lost air from the lost air turbine, and instead of venting said lost air to the atmosphere, the lost air is compressed in a supplemental air compressor and returned to the air separation unit at a location downstream a front-end purification unit and upstream a booster. This setup advantageously allows for increased production without having to adjust the sizing of the front-end purification unit or main air compressor.

Apparatus for the distillation of air by cryogenic distillation

An apparatus for the distillation of air by cryogenic distillation is provided. The apparatus can include an enclosure; a first distillation column configured to operate at a first pressure; a second distillation column configured to operate at a second pressure that is lower than the first pressure, the second distillation column being placed above the first distillation column and forming therewith a double column; a subcooling heat exchanger configured to cool at least one liquid from the first distillation column upstream of the second distillation column and configured to warm a gaseous nitrogen stream from the second distillation column; and an argon column configured to separate an argon enriched stream from the second distillation column and configured to produce an argon rich stream. In certain embodiments, the first distillation column, the second distillation column, the argon column and the subcooling heat exchanger are disposed within the enclosure, and/or the subcooling heat exchanger is disposed directly underneath the first distillation column or the argon column.

Method for utilizing waste air to improve the capacity of an existing air separation unit

A method for improving the capacity of an existing air separation unit employing a lost air turbine is provided in which the capacity is increased by operating the existing air separation unit as previously operated, with the exception of collecting the lost air from the lost air turbine, and instead of venting said lost air to the atmosphere, the lost air is compressed in a supplemental air compressor and returned to the air separation unit at a location downstream a front-end purification unit and upstream a booster. This setup advantageously allows for increased production without having to adjust the sizing of the front-end purification unit or main air compressor.

METHOD FOR UTILIZING WASTE AIR TO IMPROVE THE CAPACITY OF AN EXISTING AIR SEPARATION UNIT

A method for improving the capacity of an existing air separation unit employing a lost air turbine is provided in which the capacity is increased by operating the existing air separation unit as previously operated, with the exception of collecting the lost air from the lost air turbine, and instead of venting said lost air to the atmosphere, the lost air is compressed in a supplemental air compressor and returned to the air separation unit at a location downstream a front-end purification unit and upstream a booster. This setup advantageously allows for increased production without having to adjust the sizing of the front-end purification unit or main air compressor.

METHOD FOR UTILIZING WASTE AIR TO IMPROVE THE CAPACITY OF AN EXISTING AIR SEPARATION UNIT

A method for improving the capacity of an existing air separation unit employing a lost air turbine is provided in which the capacity is increased by operating the existing air separation unit as previously operated, with the exception of collecting the lost air from the lost air turbine, and instead of venting said lost air to the atmosphere, the lost air is compressed in a supplemental air compressor and returned to the air separation unit at a location downstream a front-end purification unit and upstream a booster. This setup advantageously allows for increased production without having to adjust the sizing of the front-end purification unit or main air compressor.