System for purifying argon by cryogenic distillation, comprising a single column surmounted by a top-end condenser, a fluid inlet in the lower part of the column, a fluid outlet in the upper part of the column, and N distillation sections where N≥4, of which at least the two uppermost sections of the column are equipped respectively with a first liquid distributor and with a second liquid distributor, the second distributor being capable of performing a function of mixing together liquids that fall onto the distributor, each of the first and second distributors being positioned above the respective section and of which the two lowermost sections of the column are respectively equipped with a (N−1)th and an Nth liquid distributor capable of performing a function of mixing together liquids that fall onto the distributor, and which is arranged above the respective section, the first, second, (N−1)th and Nth distributors each being dimensioned to contain a maximum height of liquid head, that (those) of the first and second distributors being greater than that (those) of the (N−1)th and Nth distributors.

Embodiments of false downcomers are described having a lip extending inwardly from a bottom portion of the wall of the false downcomer. The lip has a length sufficient to deflect downward vapor from exiting through the bottom opening.

A double liquid distribution device (1) suitable for use in in a fractionating or wash column (10) including a high collector tray (2) connected to a manifold support (7) via at least two longitudinal liquid downflow ducts (5, 6), the manifold support (7) supporting at least two series of transverse tubular manifolds (8, 8a 8b) and serving to feed liquid respectively to the first series of manifolds (8a) via a first longitudinal duct (5) and to the second series of manifolds (8b) via a second longitudinal duct (6), each manifold (8, 8a 8b) including distribution orifices (8c) in its under face that are suitable for distributing the liquid onto the top face of the packing bed (9). The two longitudinal liquid downflow ducts (5, 6) are connected together in a low portion (5b, 6b) by a communication device (11) fitted with a valve (12) having controlled opening that is suitable for allowing the liquid to be transferred between the two longitudinal ducts in a controlled manner.

Plant for the production of argon by cryogenic distillation, comprising an argon separation column, means for sending a gas containing argon and oxygen to the argon separation column, means for extracting a fluid enriched in argon at the top of the argon separation column, means for extracting a liquid enriched in oxygen at the bottom of the argon separation column and at least two storage tanks, positioned one above the other, each storage tank being connected to two different intermediate levels of the argon separation column by two pipes, the two storage tanks being contiguous.

The invention relates to a fluid collection device (8), in particular a support collector unit, for collecting fluid flowing through a packing (4) of a material exchange column (1). The fluid collection device (8) includes a support ring (11), a plurality of support profiles (12-16) secured to the support ring (11) for supporting the at least one packing (4), and a plurality of collection channels (19-21) secured to the support ring (11) for collecting the fluid. The collection channels (19-21) are positioned in parallel to the support profiles (12-16) and the support profiles (12-16) are arranged in such a way that they are each arranged in a no-flow area (40, 41) of one of the collection channels (19-21).

A two-stage liquid distribution device for use within an internal region of a mass transfer column to distribute liquid to an underlying mass transfer bed. The two-stage liquid distribution device includes a lower distributor with a lower parting box and lower troughs and an upper distributor with an upper parting box and upper troughs. The lower and upper parting boxes and troughs are enclosed to allow a liquid head in a lower downpipe section and an upper downpipe section that feed liquid to the lower distributor and the upper distributor to cause pressurization of liquid within the lower and upper parting boxes and troughs. The pressurization makes the lower and upper distributors less susceptible to rocking motion of the mass transfer column and reduces any maldistribution of liquid discharged from the lower and upper troughs to the mass transfer bed.

Apparatus for separating air comprising a device for breaking up a jet of cryogenic liquid in a gas flow, comprising a supply pipeline for the cryogenic liquid having an inside diameter greater than or equal to 10 mm, and a gas pipe of circular section, with a diameter d, the gas pipe comprising a portion having a reduction in diameter by a ratio of 20 to 50% at the point of injection of liquid and over a distance y wherein:

y=nd

and wherein the supply pipeline penetrates the gas pipe such that its end is in the portion of the pipe having the reduction in diameter and n is between 7 and 9.

An annular divided wall column for the cryogenic rectification of air or constituents of air is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall to define an annulus column region and an interior core column region. The present annular divided wall column further includes structured packing elements disposed within at least the annulus column region as well as a ring-shaped cantilevered collector; and a ring-shaped distributor disposed in the annulus column region above or below the plurality of structured packing elements. The thermal expansion and contraction of the second annular column wall in a radial direction and in an axial direction is independent of the thermal expansion and contraction of the first annular column wall in the radial and axial directions.

An annular divided wall column is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall and radially spaced therefrom to define an annulus column region as the space between the first annular column wall and the second annular column wall. An interior core column region is also defined by the interior space of the second annular column wall. The present annular divided wall column further includes a plurality of packing elements, disposed within the interior core column region within the annulus column region having different surface area densities and optionally, also have different geometries.

An annular divided wall column for the cryogenic rectification of air or constituents of air is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall to define an annulus column region and an interior core column region. The present annular divided wall column further includes structured packing elements disposed within at least the annulus column region as well as a ring-shaped cantilevered collector; and a ring-shaped distributor disposed in the annulus column region above or below the plurality of structured packing elements. The thermal expansion and contraction of the second annular column wall in a radial direction and in an axial direction is independent of the thermal expansion and contraction of the first annular column wall in the radial and axial directions.