A standard sample for measuring rock porosity by helium method is disclosed, which includes a cylinder body open above and a cover body matching the cylinder body. The center of the cover body is provided with a vent hole. The cylinder body is filled and tamped with filled sand body so that theoretical porosity in the cylinder body is 5%-10%. The filled sand body includes mixed sand body and quartz cotton. The mixed sand body includes coarse-grained high-purity quartz sand, medium-grained high-purity quartz sand and fine-grained silicon micropowder. By mixing, filling and tamping high-purity quartz sand with different particle sizes, silicon micropowder and quartz cotton, the porosity and permeability of the standard sample are reduced, so that the standard sample is closer to the physical properties of the actual shale geological samples to verify the method or calibrate the instrument for measuring rock porosity with helium method.

A method can include receiving porosimetry data for a range of pressures that spans a transition zone defined at least in part by a high-pressure end of a first pressure zone and a low-pressure end of a second pressure zone; detecting at least one artifact in the transition zone; computing accuracy information for the highpressure end of a first pressure zone and the low-pressure end of a second pressure zone; computing a pressure-volume adjustment based at least in part on the accuracy information; and outputting a pressure-volume relationship in the transition zone based at least in part on the pressure-volume adjustment.

A standard sample for measuring rock porosity by helium method is disclosed, which includes a cylinder body open above and a cover body matching the cylinder body. The center of the cover body is provided with a vent hole. The cylinder body is filled and tamped with filled sand body so that theoretical porosity in the cylinder body is 5%-10%. The filled sand body includes mixed sand body and quartz cotton. The mixed sand body includes coarse-grained high-purity quartz sand, medium-grained high-purity quartz sand and fine-grained silicon micropowder. By mixing, filling and tamping high-purity quartz sand with different particle sizes, silicon micropowder and quartz cotton, the porosity and permeability of the standard sample are reduced, so that the standard sample is closer to the physical properties of the actual shale geological samples to verify the method or calibrate the instrument for measuring rock porosity with helium method.

A data processing method includes: collecting test data of a target rock sample in different gas adsorption experiments; the test data including pore sizes and pore volumes corresponding to the pore sizes and including at least two selected from the group consisting of the test data with pore sizes less than 3 nm in CO.sub.2 adsorption experiment, the test data with pore sizes in 1.5 nm to 250 nm in N.sub.2 adsorption experiment and the test data with pore sizes in 10 nm to 1000 μm in high-pressure mercury adsorption experiment; and fitting the test data in overlapping ranges of the pore sizes using a least square method, and obtaining target pore volumes corresponding to the pore sizes respectively. The accuracy of joint characterization of shale pore structures can be improved by using mathematical methods to process the data in overlapping ranges of pore sizes among different characterization methods.

A method includes screening heterogeneity of a rock sample using nuclear magnetic resonance testing to determine a composition of the rock sample, drilling at least one smaller rock sample representative of the determined composition, and testing the at least one smaller rock sample with mercury injection capillary pressure to obtain a capillary pressure distribution of the at least one smaller rock sample. The method further includes decomposing a T.sub.2 distribution from the nuclear magnetic resonance testing and the capillary pressure distribution using Gaussian fitting to identify multiple pore systems, where the small ends of the Gaussian fitted T.sub.2 distribution and the Gaussian fitted capillary pressure distribution are overlapped for at least one of the identified pore systems.

Discussed is an apparatus for estimating a rechargeable battery performance according to an electrode structure and a method thereof and the apparatus for estimating the rechargeable battery performance. The apparatus may include a communication unit that receives a cumulative intrusion value that is a summed value of volumes of entire pores per unit area of a positive electrode from an apparatus for measuring volumes of pores formed in the positive electrode, and a processor that estimates an output performance of a rechargeable battery by comparing the cumulative intrusion value and a volume reference value, wherein the volume reference value is the cumulative intrusion value corresponding to an expected output value required for the rechargeable battery when the rechargeable battery is continuously discharged.

A single stage high pressure mercury injection capillary pressure measurement apparatus includes a sample sub-assembly, a transducer sub-assembly a hydraulic intensifier, and a gas cylinder. The sample sub-assembly includes a casing having walls defining an interior volume, a penetrometer arranged in the casing, the penetrometer having walls defining a sample volume, an annular space defined between the walls of the casing and the walls of the penetrometer, and a common chamber fluidly connected to the annular space by a fluid line and to the sample volume of the penetrometer by a tubing. The transducer sub-assembly is fluidly connected to the sample sub-assembly via the common chamber and includes a plurality of high-pressure transducers a plurality of low-pressure transducers. The hydraulic intensifier is fluidly connected to the common chamber and is configured to apply a high pressure to the annular space.

A data processing method includes: collecting test data of a target rock sample in different gas adsorption experiments; the test data including pore sizes and pore volumes corresponding to the pore sizes and including at least two selected from the group consisting of the test data with pore sizes less than 3 nm in CO.sub.2 adsorption experiment, the test data with pore sizes in 1.5 nm to 250 nm in N.sub.2 adsorption experiment and the test data with pore sizes in 10 nm to 1000 μm in high-pressure mercury adsorption experiment; and fitting the test data in overlapping ranges of the pore sizes using a least square method, and obtaining target pore volumes corresponding to the pore sizes respectively. The accuracy of joint characterization of shale pore structures can be improved by using mathematical methods to process the data in overlapping ranges of pore sizes among different characterization methods.

A method includes screening heterogeneity of a rock sample using nuclear magnetic resonance testing to determine a composition of the rock sample, drilling at least one smaller rock sample representative of the determined composition, and testing the at least one smaller rock sample with mercury injection capillary pressure to obtain a capillary pressure distribution of the at least one smaller rock sample. The method further includes decomposing a T.sub.2 distribution from the nuclear magnetic resonance testing and the capillary pressure distribution using Gaussian fitting to identify multiple pore systems, where the small ends of the Gaussian fitted T.sub.2 distribution and the Gaussian fitted capillary pressure distribution are overlapped for at least one of the identified pore systems.

A single stage high pressure mercury injection capillary pressure measurement apparatus includes a sample sub-assembly, a transducer sub-assembly, a hydraulic intensifier, and a gas cylinder. The sample sub-assembly includes a casing having walls defining an interior volume, a penetrometer arranged in the casing, the penetrometer having walls defining a sample volume, an annular space defined between the walls of the casing and the walls of the penetrometer, and a common chamber fluidly connected to the annular space by a fluid line and to the sample volume of the penetrometer by a tubing. The transducer sub-assembly is fluidly connected to the sample sub-assembly via the common chamber and includes a plurality of high-pressure transducers a plurality of low-pressure transducers. The hydraulic intensifier is fluidly connected to the common chamber and is configured to apply a high pressure to the annular space.