VACUUM TREATMENT APPARATUS
20230234094 · 2023-07-27
Inventors
- Rico BENZ (Montlingen, CH)
- Martin DÜTSCHLER (Trübbach, CH)
- Josef STEINKELLER (St. Gallen, CH)
- Daniele ZORZI (Eschenbach, CH)
- Jörg PATSCHEIDER (Meilen, CH)
- Stephan VOSER (Buchs, CH)
- Pierre MATTEACCI (Flums-Hochwiese, CH)
Cpc classification
H01L21/6719
ELECTRICITY
B05D1/60
PERFORMING OPERATIONS; TRANSPORTING
C23C16/46
CHEMISTRY; METALLURGY
B05D3/0218
PERFORMING OPERATIONS; TRANSPORTING
C23C14/568
CHEMISTRY; METALLURGY
C23C16/54
CHEMISTRY; METALLURGY
H01L21/6776
ELECTRICITY
International classification
Abstract
So as to perform a vacuum surface treatment on a workpiece at a predetermined temperature, which is different from a temperature to which the surface is exposed during the vacuum surface treatment, the workpiece is conveyed in a conveyance direction along one or more than one station group including one or more than one tempering station and of a single treatment station.
Claims
1. A vacuum treatment apparatus, comprising a vacuum recipient (1); a workpiece conveyer arrangement (3) in said vacuum recipient, driven by a controlled step-drive arrangement (9) in a conveyance direction (W) and comprising at least two workpiece carriers (17); at least one station-group (11) coupled to said vacuum recipient (1) and consisting of at least one tempering-station (13) and of one single treatment-station (15), said one single treatment-station (15) being located subsequent said at least one tempering-station (13) in said conveyance direction, said at least one tempering-station (13) and said one single treatment-station (15) being mutually spaced by a distance in said conveyance direction (W); said workpiece conveyer arrangement (3) and said step-drive arrangement (9) being constructed to convey said workpiece carriers (17) by one or more than one steps in said conveyance direction (W) simultaneously and thereby simultaneously into alignment with said at least one tempering-station (13) and with said one single treatment-station (15); each of said at least two workpiece carriers (17) being movable by a tempering-station drive (19) into and from a tempering position (TP) relative to said one single tempering-station (13), once aligned with said tempering-station; each of said at least two workpiece carriers (17) being movable by a treatment-station drive (27) into and from a treatment position (DP) relative to said one single treatment-station (15), once aligned with said one single treatment-station, said at least one tempering-station being configured to heat or to cool a workpiece in said tempering-station to such a temperature that said heated or cooled workpiece, once conveyed from said at least one tempering-station into said treatment-station, enters said treatment-station with a surface temperature which is different from the temperature said surface is exposed to in said treatment-station by a desired, selected amount.
2. The vacuum treatment apparatus according to claim 1 wherein said desired, selected amount is at least 50° C.
3. The vacuum treatment apparatus according to claim 1 wherein said desired, selected amount is at least 100° C.
4. The vacuum treatment apparatus according to claim 1 wherein said single treatment-station (15) comprises a gas feed arrangement (35) connectable or connected in gas-flow communication with a gas supply (37) containing a reactive gas.
5. The vacuum treatment apparatus according to claim 1 wherein said single treatment-station (15) is operationally connected to a controllable source of thermal energy or to a controllable sink of thermal energy (39).
6. The vacuum treatment apparatus according to claim 1 wherein a reaction space (29) to which said workpiece carrier (17) is exposed in said single treatment-station (15) is sealed as said workpiece carrier (17) is in said treatment position (DP).
7. The vacuum treatment apparatus of claim 1 said single treatment-station (15) comprising a pumping port (33p) connectable or connected in flow communication to a pump (33).
8. The vacuum treatment apparatus of claim 1 said single treatment-station (15) being a layer deposition station.
9. The vacuum treatment apparatus of claim 1 wherein at least a part of the walls of the single treatment-station (13) exposed to said reaction space comprise an inverse-tempering arrangement (81).
10. The vacuum treatment apparatus of claim 1 whereby, in said tempering position, a sealed tempering space (21) is defined in said tempering-station (13).
11. The vacuum treatment apparatus of claim 1 said tempering-station comprising a pumping port (25p) connectable or connected to a pump (25).
12. The vacuum treatment apparatus of claim 1 comprising more than one of said station-group (11), located one behind the other, considered in said conveyance direction (W), particularly located directly one behind the other, and/or wherein particularly said more than one station-groups are equal or at least some of said more than one station-groups are different from others of said more than one station-groups, the number of said workpiece carriers (17) on said workpiece conveyer arrangement (3) being at least equal to the sum of the number of the at least one tempering-stations (13) of said more than one station-groups (11) and of the number of the one single treatment-stations (15) of said more than one station-groups (11).
13. The vacuum treatment apparatus of one of claim 1 at least one station group (11) comprising more than one of said tempering-stations (13) preceding said one single treatment-station (15), said more than one tempering-stations (13) being neighboring each other and spaced by said distance, the number of said workpiece carriers (17) on said workpiece conveyer arrangement (3) being at least equal to the sum of the number of tempering-stations (13) and of the number of single treatment-stations (15) provided.
14. The vacuum treatment apparatus of claim 1 wherein said workpiece conveyer arrangement (3) comprises at least one conveyer, driven by a forwards/backwards step-drive ((3,9)a, (3,9)ai) of said step-drive arrangement (3).
15. The coating apparatus of one of claim 1 wherein said workpiece carriers (17) are movable relative to said tempering-station (13) by said tempering-station drive (19), perpendicularly to said conveyance direction (W), towards and from the tempering position (TP).
16. The vacuum treatment apparatus of claim 15 wherein said workpiece carriers (17) are movable, by said tempering-station drive (19), perpendicularly to said conveyance direction (W) towards and from said tempering position (TP).
17. The vacuum treatment apparatus of claim 1 wherein said workpiece carriers (17) are movable by said treatment-station drive (27), relative to said single treatment-station (15), perpendicularly to said conveyance direction (W) towards and from the treatment position.
18. The vacuum treatment apparatus of claim 17 wherein said workpiece carriers (17) are movable, by said treatment-station drive (27), perpendicularly to said conveyance direction (W) towards and from said treatment position.
19. The vacuum treatment apparatus of claim 1 wherein said workpiece carriers (17) are movable by said treatment-station drive (27) and by said tempering-station drive (19), respectively, perpendicularly to said conveyance direction (W), towards and from said tempering position (TP) and towards and from said treatment position (DP) by moving said workpiece conveyer arrangement (3).
20. The vacuum treatment apparatus of claim 1 wherein said workpiece carriers (17) are movable relative to said tempering-station by said tempering-station drive (19) towards and from said tempering position (TP) by moving at least a part of said tempering-station (13) perpendicularly to said conveyance direction (W) towards and from said workpiece carrier (17).
21. The vacuum treatment apparatus of claim 1 wherein said workpiece carriers (17) are movable relative to said single treatment-station (15) by said treatment-station drive (27) towards and from said treatment position by moving at least a part of said single treatment-station (15) perpendicularly to said conveyance direction (W) towards and from said workpiece carrier (17).
22. The vacuum treatment apparatus of claim 1 wherein said workpiece carriers (17) comprise contact areas (51) for supporting a workpiece (5) which contact areas (51) provide thermal isolation of the workpiece (5) from the workpiece carrier (17).
23. The vacuum treatment apparatus of claim 1 wherein said workpiece carriers (17) and/or said workpiece conveyer arrangement (3) comprise mutual contact areas (52) which provide thermal isolation of the workpiece carrier (17) from the workpiece conveyer arrangement (3).
24. The vacuum treatment apparatus of claim 1 wherein the workpiece carriers (17) comprise a rigid, membrane-like plate (54), with at least one trough-opening (53,53p), wherein, particularly, said at least one through-opening extends over the predominant extent of said membrane-like plate (54).
25. The vacuum treatment apparatus according to claim 1 wherein said workpiece carriers (17) are frame shaped and particularly comprise trough-openings (53p) along the frame periphery.
26. The vacuum treatment apparatus of claim 1 wherein said workpiece conveyer arrangement (3) comprises a ring-shaped conveyer with a center axis or a circular disc-shaped conveyer (3d) with a center axis (Ad), which conveyer is rotated around said center axis by said step-drive arrangement (9).
27. The vacuum treatment apparatus of claim 1 wherein said workpiece conveyer arrangement (3) defines a surface of revolution (104) around a center axis (A), said step-drive arrangement (9) rotating said workpiece conveyer arrangement (3) around said center axis (A) and said workpiece carriers (17) are provided tangentially to and along said surface of revolution.
28. The vacuum treatment apparatus of claim 1 said workpiece carrier (17) in said tempering position facing, via a gap, a tempering surface (14) of said tempering-station, at least a part of said tempering surface being the surface of a heater arrangement or of a cooler arrangement (61,61b).
29. The vacuum treatment apparatus of claim 1, opposed surfaces of said workpiece carrier (17) in said tempering position facing, via a respective gap, a respective tempering surface (14,14′) of said tempering-station (13), at least a part of said tempering surfaces being surfaces of heater arrangements or of cooler arrangements (61,61b).
30. The vacuum treatment apparatus of claim 28, said one tempering surface (14) or both said tempering surfaces (14,14′) and said respective surface of said workpiece carrier being spaced via said respective gap by an averaged distance d for which there is valid: 0.1 mm≤d≤30 mm, particularly 0.1 mm≤d≤5 mm.
31. The vacuum treatment apparatus of claim 1 a sealed tempering space (21) being defined in said tempering-station (13) and in said tempering position, said tempering-station comprising a gas-feed line arrangement (65) dispatching into said tempering space (21).
32. The vacuum treatment apparatus of claim 31, said tempering space (21) comprising no pumping port, a flow communication from said tempering space to a pumping port being established by unsealing said tempering space thereby establishing a gas-flow communication of negligible flow resistance out of said tempering space.
33. The vacuum treatment apparatus of claim 1, said tempering-station (13) comprising a pumping port.
34. The vacuum treatment apparatus of claim 31 said gas-feed line arrangement (65) being in flow connection with a gas supply (73) particularly containing at least one of helium, hydrogen, argon.
35. The vacuum treatment apparatus of claim 31 comprising a gas-heater or a gas-cooler (69) interconnected between said tempering space (21) and said gas supply (73), along said gas-feed line arrangement (65).
36. The vacuum treatment apparatus of claim 1 said single treatment-station (15) comprising a gas feed arrangement (35) for a reactive gas which gas feed arrangement comprising an input line (100) dispatching in said reaction space (29), an input to said input line (100) branching via a controllable valve arrangement (99a,99b) to at least two gas supply sources (97a,97b) containing reactive gas.
37. The vacuum treatment apparatus of claim 1 wherein said single treatment-station (15) comprises a gas feed arrangement (35) connectable or connected in gas-flow communication with a gas supply (37) containing a reactive gas which reactive gas comprises or consists of a monomer gas with a characteristic according to which said monomer gas polymerizes on a surface with an increasing polymerization rate as the temperature of said surface decreases.
38. The vacuum treatment apparatus of claim 1 wherein said single treatment-station (15) comprises a gas feed arrangement (35) connectable or connected in gas-flow communication with a gas supply (37) containing a reactive gas which reactive gas does not comprise or does not consist of a monomer gas with a characteristic according to which said monomer gas polymerizes on a surface with an increasing polymerization rate as the temperature of said surface decreases.
39. A method of vacuum-process treating surfaces of workpieces or of manufacturing workpieces having a vacuum-process treated surface, comprising: a) feeding a workpiece into a vacuum atmosphere; b) conveying said workpiece into a tempering position in an evacuated tempering-station; c) tempering said workpiece during a tempering time span in said tempering position by heating or by cooling a surface of said workpiece to a predetermined first temperature; d) conveying said tempered workpiece in vacuum into a treatment position in an evacuated treatment-station; e) treating said surface of said workpiece during a treatment time span in said treating position thereby exposing said surface to a second temperature; f) removing said workpiece from said treatment-station, thereby selecting said first temperature so that said workpiece, after being conveyed into said treatment position, exhibits a surface temperature, which is different from said second temperature by a desired, selected amount, and selecting said tempering time span to be equal to said treatment time span.
40. The method of claim 39 comprising selecting said amount to be at least 50° C.
41. The method of claim 39 comprising selecting said amount to be at least 100° C.
42. The method of claim 39 comprising performing in said step c) said tempering by more than one consecutive tempering steps, each of said tempering steps lasting during said tempering time span.
43. The method of claim 39 comprising repeating steps b) to e) at least once.
44. The method of claim 39 comprising a step g) between said step b) and said step c) said step g) comprising sealing a tempering pace in said tempering-station to which said surface of said workpiece is exposed.
45. The method of claim 44 wherein said step g) comprises pressurizing said tempering space after said sealing of said tempering space.
46. The method of claim 45 comprising a step h) between said step c) and said step d), said step h) comprising depressurizing said tempering space, particularly by pumping, particularly by directly pumping said tempering space.
47. The method of claim 39 comprising a step i) between said step d) and said step e) said step i) comprising sealing a reaction space in said treatment-station to which said surface of said workpiece is exposed.
48. The method of claim 47 wherein said step i) comprises feeding a reactive gas into said reaction space after said sealing of said reaction space.
49. The method of claim 39 comprising, at least during said step e), inverse tempering of wall surfaces of said treatment-station which are exposed to said reaction space.
50. The method of claim 39 performed by making use of a vacuum treatment apparatus comprising a vacuum recipient (1); a workpiece conveyer arrangement (3) in said vacuum recipient, driven by a controlled step-drive arrangement (9) in a conveyance direction (W) and comprising at least two workpiece carriers (17); at least one station-group (11) coupled to said vacuum recipient (1) and consisting of at least one tempering-station (13) and of one single treatment-station (15), said one single treatment-station (15) being located subsequent said at least one tempering-station (13) in said conveyance direction, said at least one tempering-station (13) and said one single treatment-station (15) being mutually spaced by a distance in said conveyance direction (W); said workpiece conveyer arrangement (3) and said step-drive arrangement (9) being constructed to convey said workpiece carriers (17) by one or more than one steps in said conveyance direction (W) simultaneously and thereby simultaneously into alignment with said at least one tempering-station (13) and with said one single treatment-station (15); each of said at least two workpiece carriers (17) being movable by a tempering-station drive (19) into and from a tempering position (TP) relative to said one single tempering-station (13), once aligned with said tempering-station; each of said at least two workpiece carriers (17) being movable by a treatment-station drive (27) into and from a treatment position (DP) relative to said one single treatment-station (15), once aligned with said one single treatment-station, said at least one tempering-station being configured to heat or to cool a workpiece in said tempering-station to such a temperature that said heated or cooled workpiece, once conveyed from said at least one tempering-station into said treatment-station, enters said treatment-station with a surface temperature which is different from the temperature said surface is exposed to in said treatment-station by a desired, selected amount.
51. The method of claim 39 comprising performing a step i) between said step d) and said step e), said step i) comprising feeding a reactive gas into said reaction space after said sealing of said reaction space, said reaction gas comprising or consisting of a monomer gas with a characteristic according to which said monomer gas polymerizes on a surface with an increasing polymerization rate as the temperature of said surface decreases.
52. The method of claim 39 comprising performing a step i) between said step d) and said step e), said step i) comprises feeding a reactive gas into said reaction space after said sealing of said reaction space, said reactive gas not comprising or not consisting of a monomer gas with a characteristic according to which the monomer gas polymerizes on a surface with an increasing polymerization rate as the temperature of said surface decreases.
Description
[0130] The invention shall now be further exemplified with the help of figures.
[0131] The figures show:
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[0155]
[0156] According to
[0157] Coupled to the vacuum recipient 1, e.g. within the vacuum recipient 1, there is provided a station-group 11, shown in dash-dotted line, which consists of at least one tempering-station 13 and of one single treatment-station 15. All the one or more than one tempering-station 13 and the one single treatment-station 15 are mutually spaced by an equal distance “a” considered in the conveyance direction W of the workpiece conveyer arrangement 3. The workpieces 5 are simultaneously conveyed stepwise, by a single or by multiple steps, by the workpiece conveyer arrangement 3, simultaneously and simultaneously into alignment with the one or more than one tempering-station 13 and with the one single treatment-station 15 of the station-group 11, respectively. The number of workpieces 5 simultaneously conveyed by the workpiece conveyer arrangement 3 and spaced by distance “a”, is at least equal to the number of stations 13,15 provided along the workpiece conveyer arrangement 3. Thus, after each stepped movement of the workpiece conveyer arrangement 3 one workpiece is aligned with a tempering-station 13 and one workpiece is aligned with a single treatment-station 15.
[0158] On the workpiece conveyer arrangement 3, the workpieces 5 are respectively held on workpiece carriers 17.
[0159] Once aligned with the at least one tempering-station of the station-group 11, the workpiece 5 is moved relative to the tempering-station 13 into a tempering position TP, as schematically shown in
[0160] In the tempering-station 13 the workpieces are either heated or cooled.
[0161] Tempering may be performed in different ways, according to the respective application in which the apparatus according to the invention is involved. [0162] a) If tempering is performed in the atmosphere prevailing in the remaining volume R of the vacuum recipient 1, a tempering space 21 to which the workpiece 5 is exposed in the tempering position TP may not be sealed at all towards the remaining volume R. [0163] b) In one embodiment a gas HG is exploited, which we also call “heat conduction gas”, to rise the pressure in the tempering space 21 with respect to the pressure in the remaining volume R so as to improve heat conductance to or from the surface of the workpiece 5 and from or towards a tempering surface 14. In this case, on one hand, the tempering space 21 is provided with a gas feed arrangement 65 for the heat conduction gas HG, in flow connection with a HG supply 73. On the other hand and in this case the tempering space 21 in the tempering-station 13 is sealed as the workpiece carrier 17 and thus the workpiece 5 are in the tempering position TP. This is schematically shown in
[0164] As in this latter case an overpressure with respect to the pressure in the remaining volume R is established in the tempering space 21, this overpressure has to be equalized with the pressure in the remaining volume R before unsealing the tempering space 21 at the seal arrangement 43.
[0165] This as well may be done according to the respective application in which the apparatus according to the invention is involved. [0166] b1) If tempering is cooling or if tempering is heating but no gas is degassed from the workpiece 5 which would contaminate in an undesired manner the atmosphere in the remaining volume R, equalization of the addressed pressures may be performed by opening the seal arrangement 43 i.e. unsealing the tempering space 21 and directly equalizing the overpressure into the remaining volume R. The remaining volume R is pumped by the pump 2 in flow communication with the pumping port 2p. Thereby rapid and wide opening the sealed tempering space 21 towards the remaining volume R and thereby establishing a flow-connection of a negligible or minimized flow resistance results in a very fast, burst-like pressure equalization, so that practically the total tempering time span, in which the workpiece carrier 17 is in the tempering position TP, may be exploited for tempering purpose. We refer with respect to this equalization approach to the WO2016/091927 of the same applicant as the applicant of the present application. [0167] b2) Especially if tempering is heating and gaseous material is degassed from the workpiece 5 such gaseous material may spoil the atmosphere in the remaining volume R. In this case the tempering space 21 is wide opened by the flow connection of negligible or minimized flow resistance, by opening the seal arrangement 43 into a sealed auxiliary enclosure 44, shown in dash line in
[0169] The single treatment-station 15 of the station-group 11 in any case directly follows the tempering-station 13 or follows the last one of more than one tempering-stations 13, considered in the conveyance direction W.
[0170] Once aligned with the one single treatment-station 15 of the station-group 11, the workpiece 5 is moved into the treatment position DP relative to the single treatment-station 13 as schematically shown in
[0171] As was addressed above, the treatment-station 15 may be any kind of station in which the surface of a workpiece is treated by a vacuum process.
[0172] In
[0173] Whenever the workpiece carrier 17 is in a position in which the workpiece 5 is in treatment position DP, in the embodiment shown in
[0174] The treatment-station 15 has, in this case, a pumping port 33p which may be, or which is connected to a pump 33.
[0175] The gas feed arrangement 35 is in gas flow connection with a supply 37 containing the reactive gas RG. A source or sink of thermal energy 39 operatively coupled to the reaction space 29 of the single treatment-station 15 supplies thermal energy to or, respectively, removes thermal energy from the reaction space 29 dependent on the reactive gas supplied to the reaction space 29.
[0176] If the temperature in the reaction space 29 is higher than the desired surface temperature Tsd of the surface of the workpiece 5 to be treated, e.g. to be coated by deposition of material comprising material resulting from reacting the reactive gas RG within the sealed reaction space 29, then tempering in the tempering-station 13 is cooling and the tempering-station 13 comprises a cooler arrangement with the tempering surface 14.
[0177] If the temperature in the reaction space 29 is lower than the desired surface temperature Tsd of the surface of the workpiece 5 e.g. to be coated by deposition of material comprising material resulting from reacting the reactive gas RG within the sealed reaction space 29, then tempering in the tempering station 13 is heating and the tempering station 13 comprises a heater arrangement with the tempering surface 14.
[0178] In some applications it is desired, on one hand to improve characteristics of the surface treatment e.g. of layer deposition on the surface of the workpiece 5—which is achieved by tempering- and, on the other hand, to avoid such improvement on other surfaces as especially on the surfaces surrounding the and exposed to the reaction space 29. If by the tempering of the workpiece 5 in the tempering-station 13, e.g. an increased deposition rate of layer material on the surface of the workpiece is achieved, such increased deposition rate of layer material on the addressed other surfaces should be avoided. As schematically shown in the block of
[0179] The thermal behaviour of the surface of the workpiece 5, first in the at least one tempering-station 13 of the station-group 11, then in the directly succeeding single treatment-station 15, depends from the thermal mass M of the workpiece 5 including the thermal masses which are thermally narrowly coupled to the workpiece 5, i.e. possibly of the workpiece carrier 17 and possibly of the workpiece conveyer arrangement 3.
[0180]
[0181] According to
M.sub.1<M.sub.2<M.sub.3.
[0182] Taking heat losses into account which might occur during the conveyance from the tempering-station 13 towards and into the single treatment-station 15, the temperature TeT to be achieved during tempering by the surface temperature T.sub.s is normally selected higher than the desired surface temperature Tsd for surface treatment in the single treatment-station 15.
[0183] Departing from the representation of
[0184] Please note that the considerations according to the
[0185] With an eye on
[0186] Taking this fact and the thermal behaviours according to
[0190] In
[0191] Following the conclusions i. to iii. as addressed above, it might not be possible to realize a desired treatment effect, e.g. a desired coating thickness, in the one tempering-station 13 and the one single treatment-station 15 in the one station-group 11 according to
[0192] According to the representation of
[0193] Although the embodiment according to
[0194] Previous, and/or between and/or succeeding one or more than one of station—the groups 11, further vacuum treatment stations, as e.g. degasser- or etching-stations may be provided which are not member of a station-group 11—as succeeding a single treatment-station 15 of a station-group—and which are not shown in the figs.
[0195] In another embodiment, shown in
[0196] Although an embodiment according to
[0197] In dependency from the thermal mass M it might be that the tempering time span TT in a single tempering-station 13 does not suffice to reach a desired temperature Tsd.
[0198] In such a case two or more than two tempering-stations 13 may precede the one single treatment-station 15 in the or in one of the station-groups 11. This is shown in
[0199] Please note, that the tempering time spans at each of the more than one tempering-stations 13 preceding the single treatment-stations 15 are equal and are equal to the treatment time span in the single treatment-stations 15 of the one or more than one station-groups 11.
[0200] Summarizing the processes which may be realized by a vacuum treatment apparatus according to the invention comprising more than one station-groups 11: [0201] All station-groups 11 have equal numbers of tempering stations 13, commonly performing equal tempering results per station-group, and all single treatment-stations 15 of the station-groups 11 perform equal vacuum surface treatments: The result is a substantially homogeneous surface treatment over time e.g. a layer of substantially homogeneous characteristics along its thickness extent. [0202] At least some station-groups 11 have equal or different numbers of tempering-stations 13, commonly performing different tempering results per station-group 11, and all single treatment-stations 15 of the station groups 11 perform equal vacuum surface treatments: there results a surface treatment structured over time e.g. a layer of a layer material but with structured characteristics along its thickness extent. [0203] The station-groups 11 have equal or different numbers of tempering-stations 13, commonly performing different or equal tempering results per station-group 11, and at least some single treatment-stations 15 of the station-groups 11 perform mutually different vacuum surface treatments: there results a surface treatment structured over time, e.g. a stack of sublayers with different characteristics or of different materials along the thickness extent of the stack.
[0204] In one embodiment of either the tempering-station 13 or of the treatment-station 15 or of both stations, the workpiece carriers 17 with the workpieces 5 are moved relative to the respective station, into and from the tempering position TP or, respectively, into and from the treatment position DP perpendicularly to the conveyance direction W, by moving the workpiece carriers 17 from and towards the workpiece conveyer arrangement 3. Such an embodiment is schematically shown in
[0205] The workpieces 5 with the workpiece carriers 17 are conveyed by the workpiece conveyer arrangement 3 on a valve member 41 which may be integral with the workpiece carrier 17. The valve member 41 which is shown in the embodiment according to
[0206] In
[0207] A further embodiment of the vacuum treatment apparatus and of the methods according to the invention is shown in
[0208] As was addressed above the throughput rate may be drastically increased by tailoring the equal treatment time spans ID and tempering time spans TT as short as possible. Whereas the overall time span for treating the surface of the workpiece 5 e.g. to depositing a desired thickness of a coating on the workpiece 5, may be subdivided in short treatment time spans by having the workpiece pass a respective number of station-groups 11 and the overall time span for tempering the surface of the workpiece 5 to the desired temperature Tsd may be subdivided by providing a respective number of consecutive tempering-stations at the station-group 11, with respectively shortened tempering time spans, the time spans for tempering the surface of the workpiece 5 in one or more than one succeeding tempering stations 13 is dependent from the thermal mass M.
[0209]
[0210]
[0211] A further efficient third approach of reducing the thermal mass M is to reduce the mass of the workpiece carrier 17.
[0212] According to
[0213] Also having been exemplified for a square workpiece 5, a workpiece carrier 17 according to
[0214] By conceiving the interconnection between the workpiece conveyer arrangement 3, the workpiece carrier 17 and the workpiece 5 according to the principle shown in the
[0215]
[0216] To increase heat transfer from the tempering surface 14 and possibly 14′ of the wall 59 exposed to the tempering space 21 to the workpiece 5 or inversely, the pressure in the sealed tempering space 21 is increased over the vacuum pressure established in the vacuum recipient 1 by pump 25 (see
[0217] To just increase the addressed heat transfer from or to the workpiece 5, it suffices to establish an increased pressure in the tempering space 21 by a static cushion of the gas HG and to vent or pump such overpressure by the pump 25 as shown in
[0218] Nevertheless, as exemplified in
[0219] The pre-heated or pre-cooled gas HG is in this case circulated along one, or, in the embodiment of
[0220] In some embodiments the heated or cooled tempering surfaces 14,14′as of the wall 59 or possibly of the valve member 41 facing the workpiece carrier 17 are spaced from the workpiece carrier 17 by a distance d for which there is valid: [0221] 0.1 mm≤d≤30 mm, or even [0222] 0.1 mm≤d≤5 mm.
[0223] For a workpiece 5 which is plate-shaped like a membrane as shown in
[0224] Based on the generic representation in
[0225] In the embodiment of
[0226] So as to avoid that surface areas of the single treatment-station 15 which are exposed to the reaction space 29 are treated equally to the pre-tempered surface of the workpiece 5 in the single treatment-station 15, in the embodiment of
[0227] Thus, if tempering of the surface of the workpiece 5 to be treated in the one or more than one preceding tempering-station 13 is heating, the respective inverse tempering at the single treatment station 15 by the inverse-tempering arrangement 81 is cooling. As schematically shown in
[0228]
[0229] The treatment station 15 according to the embodiment of
[0230] According to
[0231] In the single treatment-station 15 according to
[0232] The apparatus and methods by which a vacuum treatment of the surface of a workpiece is performed at a desired temperature of the surface to be treated, may be applied practically to any technique of vacuum treating or—processing surfaces of workpieces, be it e.g. to PVD, CVD, PECVD, ALD, polymer coating etc.
[0233] As we have addressed, very short time spans for surface treating e.g. coating deposition, at the single treatment stations 15 may be realized due to the fact that a desired treatment result or effect e.g. a desired coating thickness, may nevertheless be reached namely by successively exposing the respective workpiece to more than one of the station-groups 11, each with a single treatment-station 15. Thereby the treatment at single treatment-stations 15 becomes in fact a partial treatment with respect to the desired final treatment of the surface of the workpiece 5.
[0234] Because the thermal mass M to be tempered at the at least one tempering-station 13 may be minimized practically to the thermal mass of the workpiece, and the thermal mass governs the tempering time span at a given tempering power, and final tempering before entering the one treatment-station 15 of a station-group 11 may be realized by successive tempering-stations 13 at such a station-group 11, thus performing each a partial tempering, very short tempering and treatment time spans per respective stations 13/15 may be realized and thus very high throughput rates.
[0235] In an embodiment of the apparatus and of the methods according to the invention a constant availability of reactive gas—if used—in the single treatment-station 15 is ensured as schematically and simplified shown in
[0236] Thereby an ongoing constant availability of reactive gas RG to the single treatment-station 15 is ensured.
[0237] In
[0238] To show, that the vacuum treatment apparatus and the methods according to the present invention may be realized with multiple types of workpiece conveyer arrangements 3 as long as they are driven by a step-drive arrangement 9 as was described,
[0239]
[0240] The workpiece conveyer arrangement 3d is stepwise driven by the step-drive arrangement 9 around the center axis Ad so that the workpiece carriers (not shown in
[0241] Workpieces are loaded on and unloaded from the respective workpiece carriers (not shown in
[0242] Summarizing one may say:
[0243] It is desired to expose the surface of a workpiece to a vacuum treatment at a desired surface temperature. This is achieved according to the invention by tempering the addressed surface in at least one tempering-station remote from and directly upstream the vacuum treatment in a treatment-station.
[0244] Because no tempering is necessary if the vacuum treatment process itself exposes the addressed surface to the desired surface temperature, there is established by the addressed tempering a temperature of the surface of the workpiece in such a manner, that this surface enters the treatment station with a surface temperature which is different from the temperature to which the surface is exposed during the treatment process by a predetermined, desired temperature difference or temperature amount.
[0245] Providing the tempering facilities as described is especially then justified, when the desired temperature at which the surface of the workpiece enters the treatment-station is at least different from the temperature this surface will be exposed to during the treatment process, by a temperature amount of at least 50° C. and even of at least 100° C. If the temperature of the surface, as it enters the treatment station, is too similar to the temperature to which that surface is exposed during the treatment process, then the result with respect to the treatment characteristics on the surface will not be substantially different from those characteristics achieved without tempering, and thus providing the tempering facilities as described are rather not justified.