METHOD OF MANUFACTURING ELECTRODE PLATE FOR PLASMA PROCESSING DEVICE AND ELECTRODE PLATE FOR PLASMA PROCESSING DEVICE
20230077433 · 2023-03-16
Assignee
Inventors
Cpc classification
H01L21/31
ELECTRICITY
International classification
Abstract
Provided is a method of manufacturing an electrode plate for a plasma processing apparatus for forming a plurality of gas holes having a straight portion exceeding 12 mm in length in a thickness direction of an electrode plate main body in a penetrating state and in parallel to each other, the method including: a prepared hole forming step of forming a prepared hole with a diameter of 50% or more and 80% or less of a diameter of a hole forming the straight portion with a first drill from one surface of the electrode plate main body; and a straight portion forming step of forming the straight portion to overlap the prepared hole with a second drill.
Claims
1. A method of manufacturing an electrode plate for a plasma processing apparatus for forming a plurality of gas holes having a straight portion exceeding 12 mm in length in a thickness direction of an electrode plate main body in a penetrating state and in parallel to each other, the method comprising: a prepared hole forming step of forming a prepared hole with a diameter of 50% or more and 80% or less of a diameter of a hole forming the straight portion with a first drill from one surface of the electrode plate main body; and a straight portion forming step of forming the straight portion to overlap the prepared hole with a second drill.
2. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 1, wherein the prepared hole is formed to a middle of a thickness of the electrode plate main body.
3. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 1, wherein the prepared hole has a machining depth of more than 5 mm.
4. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 1, wherein hole drilling with the second drill is performed from the one surface of the electrode plate main body.
5. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 1, wherein hole drilling with the second drill is performed from the other surface of the electrode plate main body.
6. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 5, wherein the second drill reaches the prepared hole and forms the straight portion to a middle of a thickness of the electrode plate main body.
7. An electrode plate for a plasma processing apparatus where a plurality of gas holes are provided in a thickness direction of an electrode plate main body in a penetrating state and in parallel to each other, the gas hole having a straight portion exceeding 12 mm in length and the straight portion having a diameter of 0.5 mm or more and 1.0 mm or less and a circularity of 0.01 mm or less.
8. The electrode plate for a plasma processing apparatus according to claim 7, wherein, in the gas hole, a smaller-diameter part opening on one surface of the electrode plate main body and a larger-diameter part opening on the other surface communicate with each other in a middle of the thickness direction, and the larger-diameter part is the straight portion.
9. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 2, wherein the prepared hole has a machining depth of more than 5 mm.
10. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 2, wherein hole drilling with the second drill is performed from the one surface of the electrode plate main body.
11. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 3, wherein hole drilling with the second drill is performed from the one surface of the electrode plate main body.
12. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 9, wherein hole drilling with the second drill is performed from the one surface of the electrode plate main body.
13. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 2, wherein hole drilling with the second drill is performed from the other surface of the electrode plate main body.
14. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 3, wherein hole drilling with the second drill is performed from the other surface of the electrode plate main body.
15. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 9, wherein hole drilling with the second drill is performed from the other surface of the electrode plate main body.
16. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 13, wherein the second drill reaches the prepared hole and forms the straight portion to a middle of a thickness of the electrode plate main body.
17. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 14, wherein the second drill reaches the prepared hole and forms the straight portion to a middle of a thickness of the electrode plate main body.
18. The method of manufacturing an electrode plate for a plasma processing apparatus according to claim 15, wherein the second drill reaches the prepared hole and forms the straight portion to a middle of a thickness of the electrode plate main body.
Description
BRIEF DESCRIPTION OF DRAWINGS
[0029]
[0030]
[0031]
[0032]
[0033]
[0034]
[0035]
[0036]
[0037]
DESCRIPTION OF EMBODIMENTS
[0038] Hereinafter, an embodiment of the present disclosure will be described with reference to the drawings.
[0039]
[0040] In an electrode plate 11 for a plasma processing apparatus (hereinafter, also simply referred to as “electrode plate 11”), a plurality of (in this case, several hundreds to 1,000, at least 100 or more, or at least 500 or more, etc.) gas holes 21 are formed so as to, for example, penetrate an electrode plate main body 12 in parallel in the thickness direction in a state of being aligned vertically and horizontally at a pitch of several mm to 10 mm and the electrode plate main body 12 is formed of single crystal silicon, columnar crystal silicon, or polycrystalline silicon into a disk with a thickness t of more than 12 mm and 30 mm or less and a diameter of 200 mm or more and 550 mm or less. The gas hole 21 has a straight portion 22 exceeding 12 mm in length in the thickness direction of the electrode plate main body 12. In the example shown in
[0041] The electrode plate 11 for a plasma processing apparatus is manufactured by performing, for example, etching and polishing after forming the gas holes in the disk-shaped electrode plate main body 12 obtained by slicing a silicon ingot of single crystal silicon or the like.
[0042] The gas hole formation has a prepared hole forming step of forming a prepared hole 23 with a diameter of 50% or more and 80% or less of the diameter of the hole forming the straight portion 22 with a first drill 31 from one surface of the electrode plate main body 12 to the middle of the thickness of the electrode plate main body 12 and a straight portion forming step of forming the gas hole 21 by forming the straight portion 22 to overlap the prepared hole 23 with a second drill 32.
[0043] A drill made of a sintered material of tungsten (W), a drill obtained by diamond particle electrodeposition, a polycrystal drill of diamond, a single crystal drill of diamond, and so on can be used as the drills 31 and 32. As a result of selecting these drills, it has been found that the single crystal drill is particularly suitable with the smallest drill breakage count.
[0044] To describe the gas hole forming step in more detail, first, in the prepared hole forming step, the prepared hole 23 with an inner diameter of 50% or more and 80% or less with respect to the inner diameter of the straight portion 22 of the gas hole 21 is machined to the middle of the thickness of the electrode plate main body 12. In a case where the diameter of the straight portion 22 is 0.5 mm or more and 1.0 mm or less, the diameter of the prepared hole 23 is, for example, 0.3 mm to 0.8 mm. The prepared hole 23 is machined with the first drill 31 to the middle of the thickness of the electrode plate main body 12 to, for example, a depth L1 of approximately 8 mm. Accordingly, a diameter d1 of the first drill 31 is smaller than the diameter of the straight portion 22.
[0045] Next, in the straight portion forming step, the straight portion 22 with a diameter of 0.5 mm to 1.0 mm, which is larger than the prepared hole 23, is machined with the second drill 32 and penetrates the electrode plate main body 12. For example, the straight portion 22 is formed with a diameter exceeding the diameter of the prepared hole 23 by approximately 0.2 mm (0.1 mm on each side). Accordingly, a diameter d2 of the second drill 32 is larger than the diameter d1 of the first drill 31.
[0046] In
[0047] In the above manufacturing method, before the gas hole 21 is formed in the electrode plate main body 12, the prepared hole 23 with an inner diameter of 50% or more and 80% or less with respect to the inner diameter of the straight portion 22 of the gas hole 21 is formed to the middle in the thickness direction. Since the prepared hole 23 may be formed to the middle of the electrode plate main body 12 in the thickness direction, the cutting length of the first drill 31 may be shorter than the thickness of the electrode plate main body 12. In other words, the first drill 31 for the prepared hole is small in diameter but short and thus hard to break.
[0048] Although the second drill 32 is larger in diameter and longer in length than the first drill 31 and exceeds 12 mm in linear length, the hole drilling with the second drill 32 may be performed from above the prepared hole 23 made by the first drill 31 until the electrode plate main body 12 is penetrated coaxially with the prepared hole 23. In other words, by performing the hole drilling coaxially with the prepared hole 23, the machining load corresponding to the already-removed prepared hole cutting region 41 is reduced. Accordingly, the hole drilling with the second drill 32 can be performed with the small machining load that is the original cutting region of the gas hole 21 (straight portion 22) as a whole from which the prepared hole cutting region 41 is subtracted. Accordingly, in the second drill 32, buckling attributable to a cumulative increase in machining load is unlikely to occur. As a result, even if the second drill 32 is longer in cutting length than the first drill 31, the risk of breakage is reduced as the machining load is reduced. In this manner, the first drill 31 and the second drill 32 have different drill diameters. Accordingly, the gas hole 21 of the electrode plate main body 12 is a hole formed by at least two drills having different drill diameters (for example, the first drill 31 and the second drill 32).
[0049] Although it is preferable that the hole drilling with the second drill 32 is performed coaxially with the prepared hole 23 formed by the first drill 31, a slight deviation is allowed within the diameter difference between the drills 31 and 32.
[0050] The depth of machining of the prepared hole 23 with the first drill 31 is preferably more than 5 mm and less than 15 mm whereas the length of the straight portion 22 is more than 12 mm and 30 mm or less. At a shallow machining depth of the prepared hole 23 (5 mm or less), the machining load on the second drill 32 cannot be reduced, which may cause the second drill 32 to break or result in a decline in circularity. At a deep machining depth of the prepared hole 23, the machining load on the first drill 31 increases, which causes the first drill 31 to break. 7 mm or more and 13 mm or less is more preferable. Accordingly, at a thickness of the electrode plate main body 12 of less than 15 mm, preferably 13 mm or less, the prepared hole 23 prepared with the first drill 31 may be formed so as to penetrate the electrode plate main body 12.
[0051] In the electrode plate 11 obtained by this manufacturing method, the gas hole 21 has the straight portion 22 exceeding 12 mm in length. In the example shown in
[0052] According to the electrode plate 11, the length of the straight portion 22 exceeds 12 mm, and thus the electrode plate main body 12 is formed with a thickness exceeding 12 mm and the life thereof can be extended. Further, an uneven gas flow is unlikely to occur by the circularity of the straight portion 22 being 0.01 min or less in addition thereto.
[0053] The following methods are also conceivable in a case where hole drilling is performed with two drills.
[0054] (1) Method by which the outer diameters of the two drills are the same outer diameter at which final gas hole formation is possible, hole drilling with the first drill is performed at the middle of the thickness of an electrode plate main body, and second hole drilling with the second drill is performed from above the hole to penetrate the electrode plate main body
[0055] (2) Method by which the outer diameters of the two drills are the same outer diameter at which final gas hole formation is possible, first hole drilling with the first drill is performed at the middle of the thickness of an electrode plate main body, and second hole drilling is performed from the end portion of the hole drilled first with the tip portion of the second drill inserted in the hole to penetrate the electrode plate main body
[0056] In these methods (1) and (2), a drill with a short cutting length can be used for the first hole drilling, and thus the risk of drill breakage is small. However, a positional deviation is likely to occur between the holes machined first and second, a strain is likely to occur at the opening end of the hole, and a decline in hole circularity is likely to arise. Besides, there is a risk of breakage by the drill swinging during the second hole drilling.
[0057] In the present disclosure, the hole drilling with the second drill 32 may be performed from the same direction as the first drill 31 by which the prepared hole 23 is formed as described above or may be performed from the surface of the electrode plate main body 12 on the side opposite to the first drill 31.
[0058]
[0059] In the present disclosure, the straight portion 22 does not necessarily have to be formed with a length at which the electrode plate main body 12 is penetrated.
[0060] In
[0061] In this case, the prepared hole 23 is a smaller-diameter part 24 formed from one surface side of the electrode plate main body 12 to the middle in the thickness direction. The straight portion 22 is a larger-diameter part 25 formed from the other surface side of the electrode plate main body 12 to the middle of the electrode plate main body 12 in the thickness direction so as to be coaxial and communicate with the smaller-diameter part 24. As a result, the electrode plate main body 12 is formed with the stepped gas hole 211 in which the smaller-diameter part 24 and the larger-diameter part 25 are connected.
[0062] The gas holes 21 and 211 formed by the above methods shown in
[0063] In a case where a stepped gas hole is formed, the hole may be formed by the method shown in
[0064] In the method of this example, first, as shown in
[0065] Although the third drill 33 is smaller in diameter than the second drill 32, a hole communicating with the straight portion 22 may be machined using the third drill that is larger in diameter than the second drill 32, which is not shown. Then, the straight portion 22 can be a smaller-diameter part and the hole formed by the third drill 33 can be a larger-diameter part.
EXAMPLES
[0066] Specimens were prepared by the following hole drilling methods, hole drilling was performed, and then image processing was performed using a three-dimensional image measuring machine manufactured by Mitutoyo Co., Ltd. (Quick Vision QVX606-PRO manufactured by Mitutoyo Co., Ltd.) to perform hole diameter and circularity measurement in the opening portion on the second drill inlet side and confirm the presence or absence of drill breakage during machining. The test was performed 5 times (5 holes were drilled), the average hole diameter and circularity values were obtained, and the number of times of drill breakage in the 5 tests was examined. Cases of breakage were excluded from the measurement specimens.
Example 1
[0067] Aiming at a diameter of 0.8 mm, a straight hole is formed in a penetrating state in an electrode plate main body with a thickness of 20 mm.
[0068] (1) Conventional Example Machining Method A
[0069] A drill with a diameter of 0.8 mm and a cutting length of 20 mm was used to drill holes at once from one surface of the electrode plate main body.
[0070] (2) Comparative Example Machining Method A
[0071] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with a drill with a diameter of 0.8 mm and a cutting length of 10 mm (first drill: also in the comparative example, the initial drill is the first drill and the next drill is the second drill, the same applies below), and then hole drilling for a depth of 20 mm was performed with a drill (second drill) with a diameter of 0.8 mm and a cutting length of 20 mm from one surface of the electrode plate main body so as to include the prepared hole to penetrate the electrode plate main body.
[0072] (3) Comparative Example Machining Method B
[0073] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with the drill (first drill) with a diameter of 0.8 mm and a cutting length of 10 mm, and then the tip portion of the drill (second drill) with a diameter of 0.8 mm and a cutting length of 20 mm was inserted into the prepared hole and hole drilling for a depth of 10 mm was performed from a depth position of 10 mm to penetrate the electrode plate main body.
[0074] (4) Example Machining Method A
[0075] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with the first drill with a diameter of 0.6 mm and a cutting length of 10 mm, and then hole drilling for a depth of 20 mm was performed with the second drill with a diameter of 0.8 mm and a cutting length of 20 mm from one surface of the electrode plate main body so as to include the prepared hole to penetrate the electrode plate main body.
[0076] The results are shown in Table 1. The evaluation of the drill breakage of the conventional example is described in the column of the first drill (the same applies to Tables 2 and 3).
TABLE-US-00001 TABLE 1 Hole diameter Circularity First drill Second drill (mm) (mm) breakage breakage Conventional — — 5/5 — Example A Comparative 0.818 0.073 0/5 3/5 Example A Comparative 0.814 0.065 0/5 3/5 Example B Example A 0.802 0.005 0/5 0/5
[0077] In Conventional Example A, the hole diameter and circularity were not measured because the drill was broken in all of the five tests.
[0078] In both Comparative Examples A and B, the drill (second drill) was broken in three out of the five tests, the hole diameter had a large error with respect to the target hole diameter, and the circularity was poor.
[0079] On the other hand, in the machining method of Example A, drill breakage was not observed at all, the error in the hole diameter of the machined hole was small, and a small-circularity hole could be machined.
Example 2
[0080] Aiming at a diameter of 0.8 mm, a straight hole is formed in a penetrating state in an electrode plate main body with a thickness of 30 mm.
[0081] (1) Conventional Example Machining Method B
[0082] A drill with a diameter of 0.8 mm and a cutting length of 30 mm was used to drill holes at once from one surface of the electrode plate main body.
[0083] (2) Comparative Example Machining Method C
[0084] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with a drill (first drill) with a diameter of 0.8 mm and a cutting length of 10 mm, and then hole drilling for a depth of 30 mm was performed with a drill (second drill) with a diameter of 0.8 mm and a cutting length of 30 mm from one surface of the electrode plate main body so as to include the prepared hole to penetrate the electrode plate main body.
[0085] (3) Comparative Example Machining Method D
[0086] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with the drill (first drill) with a diameter of 0.8 mm and a cutting length of 10 mm, and then the tip portion of the drill (second drill) with a diameter of 0.8 mm and a cutting length of 30 mm was inserted into the prepared hole and hole drilling for a depth of 20 mm was performed from a depth position of 10 mm to penetrate the electrode plate main body.
[0087] (4) Example Machining Method B
[0088] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with the first drill with a diameter of 0.6 mm and a cutting length of 10 mm, and then hole drilling for a depth of 30 mm was performed with the second drill with a diameter of 0.8 mm and a cutting length of 30 mm from one surface of the electrode plate main body so as to include the prepared hole to penetrate the electrode plate main body.
[0089] The results are shown in Table 2.
TABLE-US-00002 TABLE 2 Hole diameter Circularity First drill Second drill (mm) (mm) breakage breakage Conventional — — 5/5 — Example B Comparative — — 0/5 5/5 Example C Comparative — — 0/5 5/5 Example D Example B 0.801 0.009 0/5 0/5
[0090] The drill was broken in all of the five tests in Conventional Example B, the second drill was broken in all of the five tests in Comparative Examples C and D, and thus the hole diameter and circularity were not measured in the examples.
[0091] In the machining method of Example B, drill breakage was not observed at all, the error in the hole diameter of the machined hole was small, and a small-circularity hole could be machined. As described above, the method of the present disclosure is also effective for machining a gas hole that has a straight portion with a length of 30 mm.
Example 3
[0092] Aiming at a diameter of 0.8 mm, a straight hole is formed in a penetrating state in an electrode plate main body with a thickness of 13 mm.
[0093] (1) Conventional Example Machining Method C
[0094] A drill with a diameter of 0.8 mm and a cutting length of 13 mm was used to drill holes at once from one surface of the electrode plate main body.
[0095] (2) Comparative Example Machining Method E
[0096] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with a drill (first drill) with a diameter of 0.8 mm and a cutting length of 10 mm, and then hole drilling for a depth of 13 mm was performed with a drill (second drill) with a diameter of 0.8 mm and a cutting length of 13 mm from one surface of the electrode plate main body so as to include the prepared hole to penetrate the electrode plate main body.
[0097] (3) Comparative Example Machining Method F
[0098] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with the drill (first drill) with a diameter of 0.8 mm and a cutting length of 10 mm, and then the tip portion of the drill (second drill) with a diameter of 0.8 mm and a cutting length of 13 mm was inserted into the prepared hole and hole drilling for a depth of 3 mm was performed from a depth position of 10 mm to penetrate the electrode plate main body.
[0099] (4) Example Machining Method C
[0100] A prepared hole with a depth of 10 mm was machined from one surface of the electrode plate main body with the first drill with a diameter of 0.6 mm and a cutting length of 10 mm, and then hole drilling for a depth of 13 mm was performed with the second drill with a diameter of 0.8 mm and a cutting length of 13 mm from one surface of the electrode plate main body so as to include the prepared hole to penetrate the electrode plate main body.
[0101] (5) Example Machining Method D
[0102] A prepared hole (penetration) with a depth of 13 mm was machined from one surface of the electrode plate main body with the first drill with a diameter of 0.6 mm and a cutting length of 13 mm, and then hole drilling for a depth of 13 mm was performed with the second drill with a diameter of 0.8 mm and a cutting length of 13 mm from one surface of the electrode plate main body so as to include the prepared hole to manufacture an electrode plate main body.
[0103] The results are shown in Table 3.
TABLE-US-00003 TABLE 3 Hole diameter Circularity First drill Second drill (mm) (mm) breakage breakage Conventional 0.805 0.015 3/5 — Example C Comparative 0.808 0.035 0/5 1/5 Example E Comparative 0.807 0.040 0/5 1/5 Example F Example C 0.802 0.003 0/5 0/5 Example D 0.803 0.003 1/5 0/4
[0104] Although the drill was broken in three out of the five tests in the conventional example C and the second drill was broken in one of the five tests in Comparative Examples E and F, the hole machining depth was smaller than in Examples 1 and 2 and thus there was little drill breakage and hole drilling could be performed, and yet the formed hole has a large hole diameter error and the circularity is not satisfactory, either. Although it is conceivable that the hole drilling with the second drill of Comparative Example F is machining for a depth of 3 mm and the load is small, it was easy to swing in the hole made first, and thus breakage occurred in one of the five tests.
[0105] In Example C, none of the drills was broken, the hole diameter error was small, and the circularity was also small.
[0106] In Example D, breakage in the first drill was observed in one of the five tests, but the hole diameter error was small and the circularity was also small.
[0107] As is clear from the above examples, according to the manufacturing method of the present disclosure, a hole that has a straight portion exceeding 12 mm in length can be formed with high accuracy (small circularity) even with a thick electrode plate main body.
INDUSTRIAL APPLICABILITY
[0108] According to the method of manufacturing an electrode plate for a plasma processing apparatus of the present disclosure, the risk of drill breakage can be reduced and a highly accurate gas hole can be formed even in a case where a gas hole is machined in an electrode plate for a plasma processing apparatus exceeding 12 mm in thickness. According to the electrode plate for a plasma processing apparatus, life extension can be achieved by the thick electrode plate. Further, an uneven gas flow is unlikely to occur by the circularity of the straight portion being 0.01 mm or less in addition thereto.
REFERENCE SIGNS LIST
[0109] 11: Electrode plate (electrode plate for plasma processing apparatus) [0110] 12: Electrode plate main body [0111] 21, 211, 212: Gas hole [0112] 22: Straight portion [0113] 23: Prepared hole [0114] 24: Smaller-diameter part [0115] 25: Larger-diameter part [0116] 31: First drill [0117] 32: Second drill [0118] 41: Prepared hole cutting region [0119] 42: Straight portion cutting region