HONEYCOMB PLUGGING APPARATUS AND METHODS PROVIDING REDUCED SLUMP
20230110252 · 2023-04-13
Inventors
- Richard Bergman (State College, PA, US)
- Keith Norman Bubb (Beaver Dams, NY, US)
- Anthony Joseph Cecce (Elmira, NY, US)
- Julie Marie Daugherty (Horseheads, NY, US)
- Patrick David Tepesch (Corning, NY)
Cpc classification
F01N2330/06
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
B01D2279/30
PERFORMING OPERATIONS; TRANSPORTING
F01N3/0222
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
F01N2330/34
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
International classification
B28B11/00
PERFORMING OPERATIONS; TRANSPORTING
B01D46/00
PERFORMING OPERATIONS; TRANSPORTING
B01D46/24
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A honeycomb plugging apparatus that reduces slumping of the plugging patty. Honeycomb plugging apparatus includes a plugging head having an open-ended cavity formed from an end wall and a peripheral wall, and a support substructure provided in the open-ended cavity. Methods of plugging and manufacturing honeycomb bodies using the honeycomb plugging apparatus are provided, as are other aspects.
Claims
1. A honeycomb plugging apparatus, comprising: a plugging head having an open-ended cavity formed from an end wall and a peripheral wall; and a support substructure provided in the open-ended cavity.
2. The honeycomb plugging apparatus of claim 1, comprising a sealing surface disposed radially outwardly from an opened end of the open-ended cavity wherein the sealing surface is configured to seal against an outer edge of a mask of a masked honeycomb structure.
3. The honeycomb plugging apparatus of claim 1, wherein the support substructure comprises horizontal support members extending at least part way across the open-ended cavity.
4. The honeycomb plugging apparatus of claim 1, wherein the support substructure comprises horizontal support members and vertical support members positioned within the open-ended cavity.
5. The honeycomb plugging apparatus of claim 1, wherein the support substructure comprises a grid positioned within the open-ended cavity, wherein the grid comprises horizontal support members intersecting with vertical support members and forming grid pockets configured to support plugging material.
6. The honeycomb plugging apparatus of claim 1, wherein the end wall has flow passages formed there through.
7. The honeycomb plugging apparatus of claim 6, wherein the support substructure comprises planar elements extending toward an open end of the open-ended cavity from the end wall.
8. The honeycomb plugging apparatus of claim 6, wherein the support substructure comprises planar elements that are spaced from and do not contact the end wall of the open-ended cavity.
9. The honeycomb plugging apparatus of claim 1, wherein the support substructure comprises planar elements arranged relative to flow passages formed in an end wall of the open-ended cavity.
10. The honeycomb plugging apparatus of claim 9, wherein the planar elements are aligned between locations of at least some of the flow passages.
11. The honeycomb plugging apparatus of claim 9, wherein the planar elements are aligned in front of at least some of the flow passages.
12. The honeycomb plugging apparatus of claim 9, wherein at least some of the planar elements are aligned between the flow passages and aligned in front of the flow passages.
13. The honeycomb plugging apparatus of claim 1, wherein the support substructure extends at least half of an axial distance between the end wall and an open end of the open-ended cavity.
14. A method of plugging channels of a honeycomb body, comprising: abutting the honeycomb body with an open-ended cavity containing plugging material to form a chamber between the honeycomb body and the open-ended cavity, wherein the open-ended cavity contains a support substructure, and the honeycomb body comprises a mask with openings provided on an end face thereof that provide communication into a subset of the channels of the honeycomb body; flowing plugging material from the chamber through the openings into the subset of the channels to form plugs in the honeycomb body and arranging the honeycomb body as a plugged honeycomb body; and separating the plugged honeycomb body from the open-ended cavity, wherein the support substructure supports remaining plugging material contained in the open-ended cavity after the separating and prevents slumping of remaining plugging material in the open-ended cavity.
15. The method of claim 14, wherein the flowing of the plugging material from the chamber through the openings to form plugs in the honeycomb body further comprises flowing plugging material from a reservoir through flow passages formed in an end wall of the open-ended cavity.
16. The method of claim 15, wherein the flow passages are unblocked by motion of a flow control member prior to the flowing of the plugging material from the reservoir.
17. The method of claim 15, wherein the flowing of the plugging material through flow passages further comprises flowing the plugging material through grid pockets formed by the support substructure.
18. The method of claim 17, wherein the plugging material flowing through an individual one of the flow passages flows through multiple support cells formed by the support substructure.
19. The method of claim 17, wherein the plugging material flowing through multiple adjacent ones of the flow passages flows through a common support cell formed by the support substructure.
20. A method of plugging a honeycomb body, comprising: abutting a honeycomb body comprising a mask on an end face thereof with a volume of plugging material contained in an open-ended cavity to form a chamber between the honeycomb body and the open-ended cavity, the open-ended cavity comprising a support substructure therein; flowing plugging material from the chamber into the honeycomb body through openings in the mask to arrange the honeycomb body as a plugged honeycomb body; separating the plugged honeycomb body from the open-ended cavity; and priming the chamber with plugging material for a subsequent plugging process, wherein slumping of the plugging material remaining in the open-ended cavity for the subsequent plugging process is reduced by the support substructure supporting the plugging material.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0027] The accompanying drawings, which are included to provide a further understanding of the disclosure, are incorporated in and constitute a part of this specification, illustrate example embodiments of the disclosure, and together with the description, serve to explain the principles of the disclosure.
[0028]
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DETAILED DESCRIPTION
[0040] Particulate filters can comprise plugged honeycomb bodies that are received in a canning structure or other housing. The filters can be coupled within a pollution abatement system, such as in an engine exhaust system. An example particulate filter is formed using a honeycomb body 100 as is shown in
[0041] In the depicted embodiment, the channels 104 have a rectangular (e.g., square) cross-sectional shape. However, the walls 102 can have other orientations and can form channels 104 that have cell shapes that are rectangular non-square, quadrilateral, circular, triangular, pentagonal, hexagonal, heptagonal, octagonal, trapezoidal, diamond (rhombus), polygonal, wedge, pie, radial, or other closed geometric shapes, and combinations thereof. For example, combinations can include such cell shape combinations as “octa-square” (combinations of octagonal and square cell shapes), “hexa-diamond” (combinations of hexagonal and diamond cell shapes), “recta-square” (combinations of squares and rectangular non-squares), and the like. In embodiments, some of the channels can have a larger cross-sectional area than others. For example, some cells can have relatively smaller cross-sectional area square cell shapes and others can have relatively larger cross-sectional area square cell shapes or relatively larger cross-sectional area octagonal shapes.
[0042] The porous walls 102 can have any suitable thickness in the transverse direction (across the wall 102), such as from 0.004 inch to 0.020 inch, for example. Other wall thicknesses could be used. The honeycomb body 100 can comprise a skin 111 formed as a peripheral layer, which can be somewhat thicker than the wall thickness (e.g., 3X or more), for example. Other skin thicknesses could be used. The honeycomb body 100 can have a cell density of from about 50 to about 600 cells per square inch (cpsi), for example, however other cell densities can be used.
[0043] The honeycomb body 100 comprising the honeycomb structure 101 can be formed using conventional methods from a batch mixture containing inorganic and organic materials. For example, a suitable batch mixture can comprise ceramic particles or ceramic precursor particles, or both, an organic binder, a liquid vehicle (e.g., water), and an optional rheology modifier, an optional pore former, and/or one or more optional processing additives. The batch mixture can be extruded through an extrusion die coupled to an extruder to form a green honeycomb body, as is conventional. The extrusion can be performed using any conventional extruder or method. Other suitable methods could be used to form the green honeycomb body.
[0044] When fired, the green honeycomb body is transformed (sintered) into a porous honeycomb body 100. The porous honeycomb body 100 can comprise interconnected porosity and may be suitable for high temperatures encountered when used in exhaust gas treatment systems. The porous ceramic material of the porous honeycomb body 100 can comprise cordierite, aluminum titanate, alumina, mullite, silicon carbide, silicon nitride, and the like, or combinations thereof. Other suitable ceramics, glass-ceramics, glass, or combinations thereof can be used.
[0045] After firing to attain the porous honeycomb body 100 having the desired porosity and microstructure, plugging (formation of plugs) of channels 104 of one or more end faces 107, 108 of the honeycomb body 100 can be accomplished by the use of the plugging apparatus 500 and components thereof shown and described with reference to
[0046] As is shown in
[0047] With reference to
[0048] The mask 328 (only half shown) can comprise holes 430 precisely positioned therein. Holes 430 can be formed so that they are aligned with respective channels 104 desired to be plugged. In embodiments, the mask 328 is a thin polymer film that is transparent or translucent and the holes 430 can be formed/cut with a laser or other suitable method after imaging the exact locations of the channels 104 to be plugged through the mask 328. Other suitable methods for forming the mask can be used. In embodiments, such as where the cell density is relatively low, the mask 328 can comprise locator members (e.g., nubs) that locate in the some of the channels 104 not being plugged and position the mask 428 relative to the end face (e.g., inlet end face 107).
[0049] As is shown in
[0050] The open-ended cavity 543 is formed from an end wall 545 and a peripheral wall 546. The end wall 545 can be planar and can comprise a plurality of flow passages 547 formed there through. Flow passages 547 can be arranged in rows as shown in
[0051] The outer peripheral portion 540 of the mask 528 can extend radially outward, such as from an outer surface 111 (e.g., skin) of the honeycomb body 100. In embodiments, the mask 528 extends past the outer surface 111 of the skin 110, such as about 1 inch (2.54 cm) past, but it could extend to any distance sufficient to allow secure sealing, such as by clamping of the outer portion 540 between the clamping portions 552, 554 and the sealing surface 555 as shown in
[0052] Within the plugging apparatus 500, the volume of plugging material 544 is contained in the open-ended cavity 543. The open-ended cavity 543 can have a shape that can generally approximate the shape of the end face (e.g., inlet end face 107 or outlet end face) of the honeycomb body 100 being plugged. For example, the shape can be round if the outer perimeter shape of the honeycomb body 100 is round or another shape if the outer perimeter shape is another shape. At least a portion of the plugging material 544 is transferred through operation of the honeycomb plugging apparatus 500 to form the plugs 406 in the honeycomb body 100 (See
[0053] In the embodiment shown, the open-ended chamber 543 is sized to hold a patty of the plugging material 544. The patty of plugging material 544 in the open-ended chamber 543 can be substantially uniform in thickness to reduce the effects of compressibility of the plugging material 544. This aids in forming plugs 406 of uniform depth within the masked honeycomb body 300.
[0054] In embodiments, the open-ended chamber 543 has a depth D. For example, the depth D can be on the order of approximately ½ inch (1.27 cm). Alternatively, the open-ended chamber 543 can have any depth that is large enough to ensure sufficient plugging material 544 flow such that the entire cross-sectional area of the open-ended chamber 543 is filled.
[0055] In order to substantially reduce, minimize, or substantially eliminate slumping of the plugging material 544 in the open-ended cavity 543 after separation of a plugged honeycomb body 400 from the plugging head 538 (as shown in
[0056] The support substructure 548 can have any suitable structure for supporting and holding the plugging material 544 upon separation of the plugged honeycomb body 400. Nonetheless, it should be apparent that the mask 328 of the next masked honeycomb body 400 to be plugged should be quickly sealed between clamping members 552, 554 and the sealing surface 555 after removing the prior plugged honeycomb body 400 that was plugged according to the plugging method 900.
[0057]
[0058] As best shown in
[0059] Other grid spacings are possible including more than one flow passage 547 aligned with each grid pocket 550. For example,
[0060] Honeycomb plugging apparatus 500 comprising the support substructure 548 can comprises planar elements, as shown in
[0061]
[0062] The planar elements of the suspended grid can be coupled to a peripheral support member 759 coupled to the peripheral wall 546 by any suitable means such as welding or press fit. In this depicted embodiment, four flow passages 547 are included and aligned with at least some of the grid pockets 550, wherein the grid pockets 550 are configured to support the plugging material 544, and the ratio of flow passages 547 to grid pockets 550 is four-to-one.
[0063] Various other arrangements of the grid pockets are possible, as is shown in partial views of
[0064] Referring to
[0065] The movement of the piston 561 transfers the plugging material 544 from the reservoir 560 to the open-ended chamber 563. The plugging material 544 forced into the chamber 564 formed from the closing of the open-ended chamber 543 with the mask 328 concomitantly forces approximately the same amount of the plugging material 544 out of the chamber 564. This fills/charges the selected channels 104 of the masked honeycomb body 300 mounted to the plugging head 538 and form plugs 406 to a desired plug depth. The piston 561 moves in the direction of arrow 565 (extending for plugging and retracting for refilling with plugging material 544), for example, by piston actuator 561A mounted between the piston 561 and a moveable frame 566.
[0066] The flow of plugging material 544 between the reservoir 560 and the chamber 564 is controlled by opening (aligning) and closing (misaligning) the passages 562 of the flow control member 563 (
[0067] The passages 547, 562 can be of any size, shape, or spatial proximity to allow flow of the plugging material 544 there through, yet still allow sufficient shut off of flow of the plugging material 544 when misaligned. In embodiments, the passages 547, 562 cover approximately 25 percent of the possible surface area of the control member 563 and end wall 545, respectively. In embodiments, the passages of the control member 563 are substantially similar to the apertures 547 in the end wall 545, to allow smooth transition of the plugging material 544 from the reservoir 560 to the chamber 564 and allow precise flow control thereof. After the aligning of the passages 547, 562 and transfer of the plugging material 544, the passages 547, 562 can be misaligned and the reservoir 560 can be refilled with plugging material 544, such as from pressurized supply 570 via opening valve 571.
[0068] According to the plugging method, the flow control member 563 is moved to the opened position and then the piston 561 moves towards the masked honeycomb body 300. Once the piston 561 has begun forcing plugging material 544 into the masked honeycomb body 300, the piston 561 preferably does not stop until the plugs 406 have reached the desired depth. This aids in forming plugs 406 of uniform depth.
[0069] Once the desired depth is achieved, the piston 561 stops and is retracted slightly to allow the pressure built up by the plugging process to be relieved. At this point the pressure has been relieved and the flow control member 563 is actuated to close (misalign) the passages 547, 562 between the reservoir 560 and the chamber 564. Once closed, the plugged honeycomb body 400 can be removed from the open-ended chamber 543 by first separating and then cutting adjacent the open-ended chamber 543 with a cutting implement 569, which can comprise a wire spanning horizontally across the sealing surface 555 and which is moveable vertically. Other suitable cutting implements can be used to provide a planar surface of the patty of the plugging material 544 in the open-ended cavity 543 upon separation.
[0070] Because of the improved slump control provided by the support substructure 548, viscosity of the plugging material 544 can be decreased slightly to provide better control of plug depth. Other features and operation of the plugging apparatus 500 not described herein are described in U.S. Pat. Nos. 7,922,951 and 8,609,002, which are hereby incorporated by reference herein.
[0071] In embodiments, a method 900 of plugging channels (e.g., channels 104) of a honeycomb body (e.g., honeycomb body 100) is provided as shown and described with reference to the flowchart of
[0072] The method 900 further comprises, in block 904, flowing the plugging material (e.g., plugging material 544) from the chamber (e.g., chamber 564) through the openings (e.g., openings 340) to form plugs (e.g., plugs 406) in the masked honeycomb body (e.g., masked honeycomb body 400) and forming a plugged honeycomb body (e.g., plugged honeycomb body 400).
[0073] The method 900 further comprises, in block 906, separating the open-ended cavity (e.g., open-ended cavity 543) from the plugged honeycomb body (e.g., plugged honeycomb body 400), wherein the support substructure (e.g., support substructure 548, 548A, 548B) supports remaining plugging material (e.g., plugging material 544) contained in the open-ended cavity (e.g., open-ended cavity 543) after the separating and substantially prevents slumping of the plugging material (e.g., plugging material 544) remaining in the open-ended cavity (e.g., open-ended cavity 543).
[0074] In more detail, the method 900 comprising flowing of the plugging material 544 from the chamber 564 through the openings 340 to form plugs 406 in the masked honeycomb body 300 can further comprise flowing plugging material 544 from a reservoir 560 through flow passages 547 formed in an end wall 545 of the open-ended cavity 543. In particular, the flow passages 547 are unblocked through motion of a flow control member 563 prior to the flowing of the plugging material 544 from the reservoir 560. Further, the flowing of the plugging material 544 through flow passages 547 further comprises flowing the plugging material 544 through grid pockets 550 formed by the support substructure 548, 548A, 548B wherein embodiments of such grid pockets 550 are shown in
[0075] As can be seen in
[0076] It will be apparent to those skilled in the art that various modifications and variations can be made in the present disclosure without departing from the scope of the disclosure. Thus, it is intended that the claims cover the modifications and variations of this disclosure provided they come within the scope of the claims and their equivalents.