C01F17/00

METHODS AND DEVICES FOR GROWING OXIDE CRYSTALS IN OXYGEN ATMOSPHERE

The present disclosure discloses a method for growing a crystal in oxygen atmosphere. The method may include compensating a weight of a reactant, introducing a flowing gas, improving a volume ratio of oxygen during a cooling process, providing a heater in a temperature field, and optimizing parameters. According to the method, problems may be solved, for example, cracking and component deviation of the crystal during a crystal growth process, and without oxygen-free vacancy. The method for growing the crystal may have excellent repeatability and crystal performance consistency.

Nanoparticles, methods for producing nanoparticles and nanoparticle generators

Compositions are provided that can include nanoscale particles including metal cations such as cerium having an average particle size of less than 10 nm. The nanoscale particles can include cerium and oxygen. Methods for forming nanoparticles are provided. The methods can include exposing a metal cation within a solution to radiation to form metal nanoparticles that can include metal cations. The methods can include exposing a cerium salt solution to radiation to form the nanoparticles. The methods can include exposing solvated metal cations to radiation to precipitate nanoparticles that include metal cations such as Ce. The methods can include exposing the homogeneous solution to radiation to precipitate nanoparticles. The methods can include: providing an aqueous solution comprising metal cations; and increasing the pH of the aqueous solution with radiation to form nanoparticles that include metal cations. Nanoparticle generators are provided. The generators can include: a reactant reservoir comprising a metal cation in solution; a fluid cell in fluid communication with the reactant reservoir; a radiation source operatively aligned with the fluid cell; and a product reservoir in fluid communication with the fluid cell.

SILICON DOPED METAL OXIDE PARTICLES, AND COMPOSITION FOR UV ABSORPTION COMPRISING SILICON DOPED METAL OXIDE PARTICLES
20190367747 · 2019-12-05 · ·

The object of the present invention is to provide silicon doped metal oxide particles for UV absorption, which average molar absorption coefficient in the wavelength range of 200 nm to 380 nm, is enhanced. Provided is silicon doped metal oxide particles in which the metal oxide particles are doped with silicon, wherein an average molar absorption coefficient in the wavelength range of 200 nm to 380 nm, of a dispersion in which the silicon doped metal oxide particles are dispersed in a dispersion medium, is improved as compared with similar metal oxide particles not doped with silicon.

Method for extraction and separation of rare earth elements

The present invention provides a method for recovery, extraction and separation of rare earth elements from rare earth containing materials such as ore and tailings. In accordance with preferred embodiments, the method of the present invention includes grinding rare earth-containing ores to form ore powder and leaching the powered ore with at least one mineral acid. Further, the method of the present invention includes forming a leach solution of metal ions, forming an aqueous-metal concentrate, and precipitating the aqueous-metal concentrate to selectively remove the metal ions from the leach solution. Further, the method of present invention includes the steps of obtaining a precipitate of the rare earth elements, mixing the precipitate with ammonium salt and subjected the mixture to an electrowinning process.

PREPARATION OF SINTERABLE COMPLEX OXIDE POWDER AND MANUFACTURING OF TRANSPARENT CERAMICS
20190359496 · 2019-11-28 · ·

To a co-precipitating aqueous solution, aqueous solutions containing (a) Tb ions, (b) at least one other rare earth ions selected from the group consisting of Y ions and lanthanoid rare earth ions (excluding Tb ions), (c) Al ions and (d) Sc ions are added; the resulting solution is stirred at a liquid temperature of 50 C. or less to induce a co-precipitate of the components (a), (b), (c) and (d); the co-precipitate is filtered, heated and dehydrated; and the co-precipitate is fired thereafter at from 1,000 C. to 1,300 C., thereby forming a sinterable garnet-type complex oxide powder.

Fluorescent material, method of producing the same, and light emitting device using the same

Provided are a fluorescent material having a high light emission intensity, a method for producing the same, and a light emitting device using the same. The present fluorescent material includes a composition represented by formula (I): Si.sub.uEu.sub.vAl.sub.wO.sub.xN.sub.y, wherein when the sum of a parameter u and a parameter w is taken as 13, parameters u, v, w, x, and y in the formula (I) satisfy the following formulae (1) to (5).
2.77u2.88(1)
0.04v0.08(2)
10.12w10.23(3)
0.42x0.95(4)
12.89y13.65(5)

Piezoelectric film and piezoelectric element including the same
10483452 · 2019-11-19 · ·

In the piezoelectric film including a perovskite oxide which is represented by General Formula P, 0.1x0.3 and 0<y0.49x are satisfied, A.sub.1+[(Zr,Ti).sub.1-x-yNb.sub.xSc.sub.y]O.sub.z . . . General Formula P, in General Formula P, A is an A-site element primarily containing Pb, =0 and z=3 are standard values, but and z may deviate from standard values in a range in which a perovskite structure is capable of being obtained.

Shaded zirconia ceramic material and machinable sintered ceramic bodies made therefrom

Shaded, zirconia ceramic materials are disclosed that are suitable for use in dental applications. Ceramic bodies are made from a zirconia-containing ceramic material and a coloring composition comprising a terbium (Tb)-containing component and a chromium (Cr)-containing component as a coloring agent. The pre-shaded ceramic body is machinable into a dental restoration either as a bisque body or sintered body. A pre-shaded machinable sintered ceramic body may obviate the need for further processing steps, such as shading or sintering, and may be suitable for use in chair-side machining applications, such as in a dentist's office, significantly reducing the time to create a custom finished product.

Nano-inhibitors

Novel hybrid nanoparticles, useful for inhibiting or slowing down the formation of sulfur deposits or minerals in a well during the extraction of gas or oil. Specifically, the nanoparticles each include (i) a polyorganosiloxane (POS) matrix; and, optionally as a coating over a lanthanide oxide core, (iii) at least one polymeric scale inhibitor during the extraction of gas or oil. The invention also relates to the method for obtaining the nano-inhibitors and the application of same.

Yttrium aluminum garnet based thermal barrier coatings

Embodiments of a microstructure that allows arrest of contaminant infiltration includes an inter layer and at least one highly reactive ceramic layer. The inter layer is not reactive to an infiltrating reactive species. The HRC layer includes materials that react with a reactive contaminant species to slow or arrest infiltration of such contaminant species.