C05F7/00

Fractioned separation of valuable substances from aqueous many-component mixtures
11584672 · 2023-02-21 · ·

The invention relates to a method for the fractioned separation of valuable substances from aqueous many-component mixtures such as aqueous wastes, sludges and sewage sludge under supercritical conditions. The invention also comprises valuable substance fractions that are enriched after the method according to the invention, more particularly phosphorous-containing and phosphorous- and ammonium-containing compounds such as fertilisers and synthesis gas as an energy source and as a valuable substance for the chemicals industry. The invention comprises devices for carrying out the methods. With the method and devices according to the invention, valuable substances can be completely recovered from wastes, sludges and sewage sludge and given a new use. The methods and devices are particularly suitable for recovering phosphorous and ammonium in the form of plant-available fertiliser, for recovering metals and heavy metals, for producing synthesis gas and for obtaining hydrogen from synthesis gas, i.e. for mobility.

Fractioned separation of valuable substances from aqueous many-component mixtures
11584672 · 2023-02-21 · ·

The invention relates to a method for the fractioned separation of valuable substances from aqueous many-component mixtures such as aqueous wastes, sludges and sewage sludge under supercritical conditions. The invention also comprises valuable substance fractions that are enriched after the method according to the invention, more particularly phosphorous-containing and phosphorous- and ammonium-containing compounds such as fertilisers and synthesis gas as an energy source and as a valuable substance for the chemicals industry. The invention comprises devices for carrying out the methods. With the method and devices according to the invention, valuable substances can be completely recovered from wastes, sludges and sewage sludge and given a new use. The methods and devices are particularly suitable for recovering phosphorous and ammonium in the form of plant-available fertiliser, for recovering metals and heavy metals, for producing synthesis gas and for obtaining hydrogen from synthesis gas, i.e. for mobility.

Systems, Methods, and Compounds for Sustainable Wastewater Treatment and Co-Products Thereof
20220356100 · 2022-11-10 ·

A sequential batch reactor wastewater treatment system and method, a material combination for practicing the method, and a fertilizer co-product deriving therefrom. A pH lowering agent comprising an acid lowers the pH of wastewater. A first compound including chitin or chitosan comprises a filtering medium, a coagulant, and a flocculant, and a second compound comprises an adsorbent and a pH raising agent. Wastewater is mixed and aerated subsequent to introduction of each of the first and second compounds, and flocculation yields treated water and a sludge byproduct that may be dewatered and further processed to yield a useful fertilizer co-product. Within the first compound, diatomaceous earth operates as a filtering medium and bentonite clay acts as a coagulant and filtering medium. Within the second compound, activated carbon, calcium oxide (CaO), and caustic soda (NaOH) are operative to adsorb, disinfect, and raise the pH of the wastewater.

Systems, Methods, and Compounds for Sustainable Wastewater Treatment and Co-Products Thereof
20220356100 · 2022-11-10 ·

A sequential batch reactor wastewater treatment system and method, a material combination for practicing the method, and a fertilizer co-product deriving therefrom. A pH lowering agent comprising an acid lowers the pH of wastewater. A first compound including chitin or chitosan comprises a filtering medium, a coagulant, and a flocculant, and a second compound comprises an adsorbent and a pH raising agent. Wastewater is mixed and aerated subsequent to introduction of each of the first and second compounds, and flocculation yields treated water and a sludge byproduct that may be dewatered and further processed to yield a useful fertilizer co-product. Within the first compound, diatomaceous earth operates as a filtering medium and bentonite clay acts as a coagulant and filtering medium. Within the second compound, activated carbon, calcium oxide (CaO), and caustic soda (NaOH) are operative to adsorb, disinfect, and raise the pH of the wastewater.

Systems, Methods, and Compounds for Sustainable Wastewater Treatment and Co-Products Thereof
20220356100 · 2022-11-10 ·

A sequential batch reactor wastewater treatment system and method, a material combination for practicing the method, and a fertilizer co-product deriving therefrom. A pH lowering agent comprising an acid lowers the pH of wastewater. A first compound including chitin or chitosan comprises a filtering medium, a coagulant, and a flocculant, and a second compound comprises an adsorbent and a pH raising agent. Wastewater is mixed and aerated subsequent to introduction of each of the first and second compounds, and flocculation yields treated water and a sludge byproduct that may be dewatered and further processed to yield a useful fertilizer co-product. Within the first compound, diatomaceous earth operates as a filtering medium and bentonite clay acts as a coagulant and filtering medium. Within the second compound, activated carbon, calcium oxide (CaO), and caustic soda (NaOH) are operative to adsorb, disinfect, and raise the pH of the wastewater.

Integrated waste conversion system and method

An entirely water-based, energy self-sufficient, integrated in-line waste management system is provided for comprehensive conversion of all organic fractions of municipal and wider community waste to fuels suitable for use in transportation, with all solid residues converted to high nutrition compost. The system is based on a combination of pre-treatment, involving alkaline hydrolysis and saponification; three-way separation of the pre-treated waste into different streams that are each directed to suitable further processing including fuel production; which includes biodiesel generation in a continuous-flow catalytic esterification unit, and anaerobic digestion to produce methane or other small molecule biofuel. Remaining solids are converted to compost in a quasi-continuous process.

Integrated waste conversion system and method

An entirely water-based, energy self-sufficient, integrated in-line waste management system is provided for comprehensive conversion of all organic fractions of municipal and wider community waste to fuels suitable for use in transportation, with all solid residues converted to high nutrition compost. The system is based on a combination of pre-treatment, involving alkaline hydrolysis and saponification; three-way separation of the pre-treated waste into different streams that are each directed to suitable further processing including fuel production; which includes biodiesel generation in a continuous-flow catalytic esterification unit, and anaerobic digestion to produce methane or other small molecule biofuel. Remaining solids are converted to compost in a quasi-continuous process.

Organics recovery from dry fraction

Solid waste, for example source separated organics (SSO) or commercial and industrial (C&I) waste or both, are treated by first pressurizing the waste against a screen to produce a solids fraction and a liquid fraction. The liquid fraction can be treated in an anaerobic digester. The solids fraction is pulverized or milled, for example with a hammer mill, preferably after being diluted. The pulverized or milled waste is separated again to provide a second solids faction and a second liquid fraction. The liquid fraction can be treated in an anaerobic digester. The solids fraction is primarily inert and can be landfilled, preferably after being washed.

Organics recovery from dry fraction

Solid waste, for example source separated organics (SSO) or commercial and industrial (C&I) waste or both, are treated by first pressurizing the waste against a screen to produce a solids fraction and a liquid fraction. The liquid fraction can be treated in an anaerobic digester. The solids fraction is pulverized or milled, for example with a hammer mill, preferably after being diluted. The pulverized or milled waste is separated again to provide a second solids faction and a second liquid fraction. The liquid fraction can be treated in an anaerobic digester. The solids fraction is primarily inert and can be landfilled, preferably after being washed.

BIOPOWERPLANT: THIRD GENERATION BIOREFINERY WITH IMPROVED CAPACITY TO USE DOMESTIC WASTEWATER, LANDFILL LEACHATE AND SEA SALT WATER AS AN INPUT TO GENERATE GREEN ENERGY, WATER FOR REUSE, BIOFUEL, ORGANIC FERTILIZERS AND CAPTURE ATMOSPHERIC CO2
20230045512 · 2023-02-09 ·

The Biopowerplant is a system that integrates the generation of carbon-neutral energy through the cultivation and conversion of microalgal biomass, with sewage sanitation and environmental carbon recovery, with the additional and secondary production of biofertilizer, biofuel, water for reuse. This system integrates a suboptimal anaerobic digestion subsystem focused on the generation of biogas, the processing of the resulting digestate through a microalgal consortium culture subsystem with biofilm induction and smooth decreasing gradient of light radiation, and the transformation of the generated microalgal biomass into syngas through a subsystem of evaporation, torrefaction, pyrolysis, gasification, and combustion in separate chambers. The syngas and methane from the biogas are subsequently used as fuel in an electric power generator capable of operating with mixed gases. The biogas generation process is enriched through the recirculation of the microalgal biomass supernatant, the residual heat from the syngas generation subsystem, and the heat transferred from the combustion gases of the electric generator. The residual sludge from the biogas generation subsystem is recirculated towards a longitudinal biopile subsystem, where it acts as an anaerobic medium compared to the aerobic medium that constitutes the concentrated microalgal biomass, and both streams are mixed to be transformed into the syngas generation subsystem. Input inflows for system operation are mainly sewage, and optionally seawater and/or leachate. The inflows must be bioaugmented with a microalgal consortium dosed automatically by a Compact in situ bioaugmentation system, preferably more than 3 kilometers before the inflow enters the system.