A method for manufacturing a pillar-shaped honeycomb structure filter including preparing a pillar-shaped honeycomb structure having a plurality of first cells and a plurality of second cells that are alternately arranged adjacent to each other with a porous partition wall interposed therebetween; adhering ceramic particles containing 50% by mass or more in total of one or two selected from SiC and SiN to a surface of the first cells; and performing a heat-oxidation treatment on the pillar-shaped honeycomb structure in which the ceramic particles are adhered to the surface of the first cells to form a porous film comprised of the ceramic particles having an oxide film thereon so as to satisfy: (1) 0.05≤T≤0.5; (2) 0.05≤T/D50; and (3) 4≤{(W.sub.1−W.sub.0)/W.sub.0×100}/D50.

The present disclosure belongs to the field of biological materials, and particularly relates to a multilayer zirconia ceramic with uniform transition and a method for preparing the same. The specific technical solution of the present disclosure is as follows: a zirconia ceramic with a formula comprising, in percentage by mass, 0-3% of lanthana, 1.5-16% of yttria, 0-2.5% of silicon carbide nano-whiskers, and 0-1.5% of a coloring agent, the balance being zirconia. Correspondingly provided are a multi-layer zirconia ceramic with uniform transition prepared using the formula and a method for preparing the same. By using the method of the present disclosure, multilayer zirconia ceramics with good and uniformly transitioning core properties can be quickly and conveniently prepared, meeting the requirements of patients with dental disorders on the use and esthetics of dentures.

The present disclosure belongs to the field of biological materials, and particularly relates to a multilayer zirconia ceramic with uniform transition and a method for preparing the same. The specific technical solution of the present disclosure is as follows: a zirconia ceramic with a formula comprising, in percentage by mass, 0-3% of lanthana, 1.5-16% of yttria, 0-2.5% of silicon carbide nano-whiskers, and 0-1.5% of a coloring agent, the balance being zirconia. Correspondingly provided are a multi-layer zirconia ceramic with uniform transition prepared using the formula and a method for preparing the same. By using the method of the present disclosure, multilayer zirconia ceramics with good and uniformly transitioning core properties can be quickly and conveniently prepared, meeting the requirements of patients with dental disorders on the use and esthetics of dentures.

A method of applying a protective coating to a substrate includes the steps of: providing a turbine engine component substrate formed of a ceramic matrix composite material, forming an environmental barrier coating layer including a rare earth disilicate material directly on the substrate, treating an outer surface of the environmental barrier coating layer to form a thermal barrier coating layer including a porous rare earth monociliate material directly on the environmental barrier coating layer. The step of treating the outer surface is performed using a thermal process consisting of the application of heat or a chemical-thermal process consisting of the application of heat and a chemical. The method further includes infiltrating at least a portion of the pores with a metal solution or suspension.

A method of applying a protective coating to a substrate includes the steps of: providing a turbine engine component substrate formed of a ceramic matrix composite material, forming an environmental barrier coating layer including a rare earth disilicate material directly on the substrate, treating an outer surface of the environmental barrier coating layer to form a thermal barrier coating layer including a porous rare earth monociliate material directly on the environmental barrier coating layer. The step of treating the outer surface is performed using a thermal process consisting of the application of heat or a chemical-thermal process consisting of the application of heat and a chemical. The method further includes infiltrating at least a portion of the pores with a metal solution or suspension.

A method of producing a ceramic matrix composite including a protective ceramic coating thereon comprises applying a surface slurry onto an outer surface of an impregnated fiber preform. The surface slurry includes particulate ceramic solids dispersed in a flowable preceramic polymer comprising silicon, and the impregnated fiber preform comprises a framework of ceramic fibers loaded with particulate matter. The flowable preceramic polymer is cured, thereby forming on the outer surface a composite layer comprising a cured preceramic polymer with the particulate ceramic solids dispersed therein. The cured preceramic polymer is then pyrolyzed to form a porous ceramic layer comprising silicon carbide, and the impregnated fiber preform and the porous ceramic layer are infiltrated with a molten material comprising silicon. After infiltration, the molten material is cooled to form a ceramic matrix composite body with a protective ceramic coating thereon.

A method of producing a ceramic matrix composite including a protective ceramic coating thereon comprises applying a surface slurry onto an outer surface of an impregnated fiber preform. The surface slurry includes particulate ceramic solids dispersed in a flowable preceramic polymer comprising silicon, and the impregnated fiber preform comprises a framework of ceramic fibers loaded with particulate matter. The flowable preceramic polymer is cured, thereby forming on the outer surface a composite layer comprising a cured preceramic polymer with the particulate ceramic solids dispersed therein. The cured preceramic polymer is then pyrolyzed to form a porous ceramic layer comprising silicon carbide, and the impregnated fiber preform and the porous ceramic layer are infiltrated with a molten material comprising silicon. After infiltration, the molten material is cooled to form a ceramic matrix composite body with a protective ceramic coating thereon.

A coating according to an exemplary embodiment of this disclosure, among other possible things includes a bond coat including gettering particles and diffusive particles dispersed in a matrix, a top coat disposed over the bond coat, and an intermediate layer between the bond coat and the top coat. The intermediate layer includes non-silicate oxide particles dispersed in a matrix. An article and a method of protecting a ceramic-based substrate are also disclosed.

A coating according to an exemplary embodiment of this disclosure, among other possible things includes a bond coat including gettering particles and diffusive particles dispersed in a matrix, a top coat disposed over the bond coat, and an intermediate layer between the bond coat and the top coat. The intermediate layer includes non-silicate oxide particles dispersed in a matrix. An article and a method of protecting a ceramic-based substrate are also disclosed.

A method for applying a coating 1 to a surface 2 of a mullite material 3 is specified, which comprises pretreating the surface 2 of the mullite material 3 by means of a plasma-chemical process in which molecular hydrogen is excited in such a way that plasma-activated hydrogen is produced S1, and applying an aluminum oxide-containing layer 4 by means of a PVD process to the pretreated surface 2 of the mullite material 3 S2. Furthermore, a mullite material 3 with a coating and a gas turbine component with such a mullite material 3 are specified.