The present disclosure relates to a method of more efficiently separating and recovering a polyarylene sulfide exhibiting excellent strength, heat resistance, flame retardancy, and processability when processed into a molded product after polymerization.

The present disclosure provides a method and an apparatus for efficiently recovering an amide-based compound such as N-methyl-2-pyrrolidone from an aqueous solution containing an amide-based compound such as N-methyl-2-pyrrolidone.

The present disclosure provides a method and an apparatus for efficiently recovering an amide-based compound such as N-methyl-2-pyrrolidone from an aqueous solution containing an amide-based compound such as N-methyl-2-pyrrolidone.

The present disclosure relates to a preparation method of a polyarylene sulfide, and this method may produce a polyarylene sulfide having properties equal to or higher than those of the conventional method at a high yield by using a dihalogenated aromatic compound in a predetermined equivalent ratio with respect to a sulfur compound and performing both dehydration and polymerization under optimum conditions.

The present disclosure relates to a preparation method of a polyarylene sulfide, and this method may produce a polyarylene sulfide having properties equal to or higher than those of the conventional method at a high yield by using a dihalogenated aromatic compound in a predetermined equivalent ratio with respect to a sulfur compound and performing both dehydration and polymerization under optimum conditions.

There is provided a method for efficiently recovering amide-based compounds such as N-methyl-2-pyrrolidone from a waste liquid containing amide-based compounds such as N-methyl-2-pyrrolidone generated, for example, in a production process of polyarylene sulfide.

The present disclosure relates to a method of more efficiently separating and purifying a polyarylene sulfide exhibiting excellent strength, heat resistance, flame retardancy, and processability when processed into a molded product after polymerization.

The present disclosure relates to a method of more efficiently separating and purifying a polyarylene sulfide exhibiting excellent strength, heat resistance, flame retardancy, and processability when processed into a molded product after polymerization.

A method for forming a polyarylene sulfide is described. The method can include a multi-step cooling and precipitation process in which the cooling rate of the solution that carries the polymer is decreased during a portion of the overall cooling. This slower cooling period can encompass at least a portion of the period during which the polymer precipitates from the solution. The precipitation process can form polyarylene sulfide particles with good particle integrity and a narrow particle size distribution, which can reduce fines and improve downstream processing and final product characteristics.

A method for forming a polyarylene sulfide is described. The method can include a multi-step cooling and precipitation process in which the cooling rate of the solution that carries the polymer is decreased during a portion of the overall cooling. This slower cooling period can encompass at least a portion of the period during which the polymer precipitates from the solution. The precipitation process can form polyarylene sulfide particles with good particle integrity and a narrow particle size distribution, which can reduce fines and improve downstream processing and final product characteristics.