G01N33/44

METHOD FOR DETERMINING ORIGIN OF CARBON SOURCE OF CHEMICAL SUBSTANCE
20220334093 · 2022-10-20 · ·

Provided is a method for determining origin of carbon source of chemical substance, which makes it possible to determine whether resource-recycled carbon is used as a carbon raw material from a chemical substance in various goods. The method for determining origin of carbon source of chemical substance includes: a step S1 of acquiring a carbon-14 content rate R.sub.1 of a standard chemical substance having carbon element in which carbon has been recycled as a resource; a step S2 of acquiring a carbon-14 content rate R.sub.2 of a chemical substance to be identified; a step S3 of calculating a ratio (R.sub.2/R.sub.1) of the content rate R.sub.2 to the content rate R.sub.1; and a step S4 of determining that a carbon raw material in the chemical substance to be identified contains resource-recycled carbon based on the ratio (R.sub.2/R.sub.1).

METHOD OF ASSESSING THE HOMOGENEITY OF PLASTICS
20230106029 · 2023-04-06 ·

Fluorescent pigment is introduced into the plastic composition, preferably a thermoplastic, especially polyethylene or polypropylene, in the granules formation stage, in addition to possible standard components of the composite, mixed, granules are formed, and then the granules are formed into a finished building material component, and then, with the help of a known fluorimeter, the fluorescence intensity of individual parts of the surface of a plastic element is measured and the homogeneity of the material is inferred on the basis of the differences in the results of the fluorescence intensity measurements.

A METHOD FOR MEASURING THE CROSS-LINKING DEGREE OF A COMPONENT OF ELASTOMERIC MATERIAL

A method for measuring a degree of cross-linking of a component of elastomeric material obtained as a result of a hot-forming process, includes a preliminary calibration step in which a plurality of samples are provided, made of the same material as the component. The samples have different degrees of cross-linking following respective hot-forming processes conducted for different periods of time. The preliminary calibration step includes providing a measuring device having an electrical circuit, in which a voltage generator is arranged in series with metal contacts configured to selectively receive a sample, and an ammeter, positioning a sample between said metal contacts, providing a predetermined voltage value, and detecting the corresponding current value by means of said ammeter. The aforesaid steps are repeated for each sample so as to obtain a calibration map that associates a given degree of cross-linking of the material constituting said component with each determined value of electrical conductivity.

SIMULATION SAMPLE DESIGN METHOD, SIMULATION SAMPLE MANUFACTURING METHOD, SIMULATION SAMPLE DESIGN DEVICE, PROGRAM, AND RECORDING MEDIUM
20220317036 · 2022-10-06 · ·

A phantom design method includes a correction step and a calculation step. In the correction step, an absorption spectrum of a target of spectroscopic measurement by a near infrared spectrometer is corrected based on a refractive index of the target and a refractive index of a resin used as a base material of a phantom to generate a corrected absorption spectrum. In the calculation step, based on an absorption spectrum of the resin and an absorption spectrum of each of N types of dyes, a concentration of each of the N types of dyes to be contained in the base material is calculated such that an absorption spectrum of the phantom constituted by the base material containing the N types of dyes approximates the corrected absorption spectrum in a predetermined wavelength range of a near infrared region.

A method for measuring the quantity of super absorbent polymers in post-consumer absorbent sanitary products

A method is provided for measuring a quantity of super absorbent polymers (SAP) in a sample obtained from post-consumer absorbent sanitary products comprising at least one portion of a portion of cellulose and/or a portion of plastic in addition to a portion of SAP, said post-consumer absorbent sanitary products having been, preferably, previously subjected to at least one treatment comprising the separation of said portions; the SAP contained in said sample comprise linear polyacrylate polymers (LPA) and/or cross-linked polyacrylate polymers (CLPA).

METHOD FOR CHARACTERIZING MELTING TRANSITION AND CRYSTALLIZATION IN A SEMICRYSTALLINE POLYMER

A method for characterizing a melting transition in a semicrystalline polymer is disclosed. The method includes incorporating a fluorophore into the semicrystalline polymer, changing a temperature of the semicrystalline polymer to vary across a range of temperatures comprising a plurality of temperatures, and capturing an emission spectrum of the incorporated fluorophore at each temperature of the plurality of temperatures. The method also includes integrating each emission spectrum to determine a temperature-dependent integrated fluorescence intensity for the semicrystalline polymer, numerically differentiating the temperature-dependent integrated fluorescence intensity, and characterizing the melting transition of the semicrystalline polymer by identifying a stepwise change in value of the differentiated intensity. The semicrystalline polymer may be a thermoplastic. Incorporating the fluorophore into the semicrystalline polymer may include physically doping the semicrystalline polymer with the fluorophore or covalently labeling the semicrystalline polymer with the fluorophore.

Deterioration analyzing method

The present invention provides a method of deterioration analysis that enables detailed analysis of the deterioration, especially of the surface, of a polymer material containing at least two diene polymers. The present invention relates to a method of deterioration analysis including: irradiating a polymer material containing at least two diene polymers with high intensity x-rays; and measuring x-ray absorption while varying the energy of the x-rays, to analyze the deterioration of each diene polymer.

UTILIZING ATREF DATA WITH CHEMOMETRIC ANALYSIS FOR DETERMINING THE TYPES OF POLYETHYLENE PRESENT IN POLYMER BLENDS AND MULTILAYER FILMS

A method of analyzing a polymer resin comprising: providing a polymer resin sample having two or more polymer components; subjecting the sample to aTREF analysis to yield aTREF elution trace by contacting the sample with aTREF solvent to form sample solution; introducing sample solution into aTREF column and allowing elution of polymer components at different elution rates along the column; eluting from the aTREF column an aTREF eluent comprising the polymer components eluting at different rates; and subjecting the aTREF eluent to IR detection to yield the aTREF elution trace; identifying the components of the sample to yield identified components by comparing the elution trace with an identification library that comprises a plurality of known polymer aTREF elution traces correlated with known polymer components characterized by identifying parameters (density, SCB, crystallization temperature, MI, HLMI, MWD); and quantifying each of the identified components to yield quantified polymer components via chemometric analysis.

Methods for Characterizing Branching Distribution in Polymers
20170363605 · 2017-12-21 ·

New metrics are disclosed for characterizing polyethylene copolymers which can be computed from the Cross-Fractionation Chromatography data of these polymers. These metrics are able to quantify the Broad Orthogonal Composition Distribution (BOCD) character of the polymers, and they can be used to discriminate polymers with an enhanced BOCD character from polymers that have the BOCD character to a lesser extent or from polymers that have the conventional molecular weight distribution and/or branching distribution.

Resin Flow Analysis Method and Non-Transitory Computer-Readable Recording Medium

A resin flow analysis method includes dividing a mold space model into small elements, acquiring a penetration coefficient, acquiring a flow conductance, and performing flow analysis of a resin in each of the small elements in the mold space model based on a first relational expression of the small elements of a base material portion relating to the penetration coefficient and a second relational expression of the small elements of a space portion relating to the flow conductance.