An apparatus for collecting and storing fluid samples from vehicles and machinery comprises a storage container having a fluid inlet sealed by a cap, the cap having an aperture releasably sealed by a lid. An adapter connects the cap releasably to a fluid outlet coupling port of a fluid sampling device. The adapter comprises a lumen, having an inlet and an outlet aperture, an external screw thread engageable with an internal screw thread of the coupling port and a connector assembly for connecting the adapter releasably to the cap. A penetrable diaphragm provides an airtight seal over a storage region of the storage container. When the adapter is connected to the coupling port and the cap is connected to the adapter, a fluid outlet tube extending from the coupling port extends through the aperture and protrudes through one or more perforations provided in the penetrable diaphragm into the storage region.

An apparatus for collecting and storing fluid samples from vehicles and machinery comprises a storage container having a fluid inlet sealed by a cap, the cap having an aperture releasably sealed by a lid. An adapter connects the cap releasably to a fluid outlet coupling port of a fluid sampling device. The adapter comprises a lumen, having an inlet and an outlet aperture, an external screw thread engageable with an internal screw thread of the coupling port and a connector assembly for connecting the adapter releasably to the cap. A penetrable diaphragm provides an airtight seal over a storage region of the storage container. When the adapter is connected to the coupling port and the cap is connected to the adapter, a fluid outlet tube extending from the coupling port extends through the aperture and protrudes through one or more perforations provided in the penetrable diaphragm into the storage region.

A device may include a memory storing instructions and a processor configured to execute the instructions to determine an initial mass of a sample; distill the sample up to at least a thermal destruction temperature; record, at a set of time points during the distilling, vapor temperature values, liquid temperature values, and vapor pressure values associated with the sample; and determine a residual mass of the sample. The processor may be further configured to generate a pressure curve based on the vapor pressure values; calculate a summary integral surface for the generated pressure curve; and generate a distillation curve that relates the vapor temperature values and the liquid temperature values to mass percentage of the sample that has evaporated, based on the calculated summary integral surface, the initial mass of the sample, and the residual mass of the sample.

A device may include a memory storing instructions and a processor configured to execute the instructions to determine an initial mass of a sample; distill the sample up to at least a thermal destruction temperature; record, at a set of time points during the distilling, vapor temperature values, liquid temperature values, and vapor pressure values associated with the sample; and determine a residual mass of the sample. The processor may be further configured to generate a pressure curve based on the vapor pressure values; calculate a summary integral surface for the generated pressure curve; and generate a distillation curve that relates the vapor temperature values and the liquid temperature values to mass percentage of the sample that has evaporated, based on the calculated summary integral surface, the initial mass of the sample, and the residual mass of the sample.

A method of determining an API gravity of a crude oil is provided. The method includes obtaining a reservoir sample containing the crude oil and heating the sample to a first temperature using an oxidative testing apparatus. The sample is then heated to a second temperature, which is greater than the first temperature, over a period using a fixed heating rate. The rate of carbon dioxide emission from the sample is detected during the period of heating to the second temperature. The peak rate of carbon dioxide emission from the sample is then determined and the peak carbon dioxide emission temperature associated with the peak rate of carbon dioxide emission is also determined. The API gravity of the crude oil in the reservoir sample is determined using an empirical correlation between API gravity and the peak carbon dioxide emission temperature associated with the fixed heating rate.

A system for measuring fluid flow in a wellbore is provided. A probe includes at least a heater. A fiber optic cable is connected to the probe. The system is programmed to perform operations including: changing an output of the heater to thereby change a temperature of drilling fluid moving over a fiber optic cable; measuring a strain on the fiber optic cable caused by changing the temperature of the drilling fluid; preliminarily determining a velocity of the drilling fluid from the measured strain; measuring at least a second parameter of the drilling fluid; adjusting the preliminary determined velocity based on the measured at least a second parameter to yield an adjusted velocity; and determining a flow rate of the drilling fluid based on the adjusted velocity.

Assemblies and methods to enhance a fluid catalytic cracking (FCC) process associated with a refining operation, during the FCC process, may include supplying a hydrocarbon feedstock to first processing units associated with the refining operation. The assemblies and methods also may include conditioning a hydrocarbon feedstock and unit material samples, and analyzing the samples via one or more spectroscopic analyzers. The assemblies and methods further may include prescriptively controlling, via one or more FCC process controllers, based at least in part on the hydrocarbon feedstock properties and the unit material properties, the FCC processing assembly, so that the prescriptively controlling results in causing the FCC process to produce intermediate materials, the unit materials, and/or the downstream materials having properties within selected ranges of target properties, thereby to cause the FCC process to achieve material outputs that more accurately and responsively converge on one or more of the target properties.

Assemblies and methods to enhance a fluid catalytic cracking (FCC) process associated with a refining operation, during the FCC process, may include supplying a hydrocarbon feedstock to first processing units associated with the refining operation. The assemblies and methods also may include conditioning a hydrocarbon feedstock and unit material samples, and analyzing the samples via one or more spectroscopic analyzers. The assemblies and methods further may include prescriptively controlling, via one or more FCC process controllers, based at least in part on the hydrocarbon feedstock properties and the unit material properties, the FCC processing assembly, so that the prescriptively controlling results in causing the FCC process to produce intermediate materials, the unit materials, and/or the downstream materials having properties within selected ranges of target properties, thereby to cause the FCC process to achieve material outputs that more accurately and responsively converge on one or more of the target properties.

A method may comprise forming a data matrix, extracting chromatographs of a mud filtrate and a formation fluid, extracting concentration profiles of the mud filtrate and the formation fluid, and decomposing a data set on an information handling machine using a bilinear model. A system may comprise a downhole fluid sampling tool and an information handling tool. The downhole fluid sampling tool may comprise one or more multi-chamber sections, one or more fluid module sections, one or more gas chromatographers, wherein the one or more gas chromatographers are disposed in the one or more fluid module sections, and an information handling system.

A microfluidic device includes a microfluidic substrate having a porous media channel, an oil inlet port in fluid communication with the porous media channel, a fluid inlet port in fluid communication with the porous media channel, and an outlet port in fluid communication with the porous media channel. The porous media channel has a plurality of dividers that provide the porous media channel with a network of fluid pathways. A method for assessing miscibility of an oil composition and a fluid includes flowing an aliquot of a fluid through a porous media channel to displace at least an oil composition from the porous media channel, and conducting an optical investigation of the porous media channel to assess the miscibility of the oil composition and the fluid at the test pressure and test temperature.