An ion exchange membrane separated two electrode flow analyzer for continuous aqueous electrochemical heavy metal detection is disclosed. The electrochemical cell includes a gas diffusion counter/reference electrode, a flooded flow through working electrode, and an ion exchange membrane that separates the gas diffusion counter/reference electrode and the flooded flow through working electrode. A method of continuous fluid analysis using a multi-electrode flow analyzer is also disclosed, including passing an aqueous sample through a first inlet flow area and into a working electrode of a multi-electrode flow analyzer, passing a gas mixture through a second inlet flow area and into a counter/reference electrode of the multi-electrode flow analyzer, depositing an analyte onto a surface of the working electrode, stripping the analyte from the surface of the working electrode by sweeping a range of a potential applied to the surface of the working electrode.

A single electron transistor conjugated to a bacteriophage form a detectable probe where an RF signal identify the location of such probe at the site of specific biological matrix and provide a unique electronic signal such as a Coulomb Staircase and where such signal act as a diagnostic beacon and where such probe and a detector form a mesoscopic detector. The detector uses: a bioprobe containing the phage with its conjugated SET and the properties of the phage specificity; phage mobility within the biological environment and the phage ability to act as a carrier for the SET; and the SET's ultimate use as a beacon for the detection.

An embodiment provides a method for digesting at least one analyte of an aqueous sample, including: introducing an aqueous sample comprising at least one analyte into a digestion device comprising one or more carbon substituted material electrodes; digesting the at least one analyte by applying an electrical potential between an anode and a cathode of the digestion device, wherein the digesting comprises a step-wise disintegration; measuring the at least one analyte of the aqueous sample from the digested material, using a measurement device selected from the group consisting of: an electrochemical device and an optical measurement device; and modifying the electrical potential based upon the measurement of the at least one analyte. Other aspects are described and claimed.

Provided is a method for selecting a material for an organic light-emitting device, the method including comparing the reversibilities (electrical stability in the (+) radical and (−) radical states of a material) of the material using cyclic voltammetry (CV).

Provided is a method for selecting a material for an organic light-emitting device, the method including comparing the reversibilities (electrical stability in the (+) radical and (−) radical states of a material) of the material using cyclic voltammetry (CV).

A carbon nanotube-based reference electrode and an all-carbon nanotube microelectrode assembly for electrochemical sensing and specialized analytics are disclosed, along with methods of manufacture, and applications including detection of ionic species including heavy metals in municipal and environmental water, monitoring of steel corrosion in steel-reinforced concrete, and analysis of biological fluids.

A carbon nanotube-based reference electrode and an all-carbon nanotube microelectrode assembly for electrochemical sensing and specialized analytics are disclosed, along with methods of manufacture, and applications including detection of ionic species including heavy metals in municipal and environmental water, monitoring of steel corrosion in steel-reinforced concrete, and analysis of biological fluids.

A sensor for detecting lead in an aqueous solution includes a copper working electrode, a counter electrode, a power supply for applying underpotential deposition of lead onto the copper electrode, a measuring device for providing measurement of a hydrogen evolution reaction (HER) current on the Pb.sub.upd-modified electrode, and a controller configured to correlate the degree of suppression of the HER current to Pb.sub.upd coverage to determine the lead coverage and lead concentration of the solution.

A sensor for detecting lead in an aqueous solution includes a copper working electrode, a counter electrode, a power supply for applying underpotential deposition of lead onto the copper electrode, a measuring device for providing measurement of a hydrogen evolution reaction (HER) current on the Pb.sub.upd-modified electrode, and a controller configured to correlate the degree of suppression of the HER current to Pb.sub.upd coverage to determine the lead coverage and lead concentration of the solution.

A trace metal analysis detector and method of operating the same to detect metals in various fluid samples using boron doped diamond working electrodes.