An apparatus and a method for making lithium iron phosphate are disclosed. The apparatus comprises a raw material system to provide a raw material mixed solution of raw materials of a hydrothermal reaction or a solvothermal reaction; a tubular reaction device to make the raw material mixed solution in a plug flowing and reacting state to obtain a reacted material; and a kettle reaction device to make the reacted material in a complete mixing and reacting state to obtain a product. The method comprises providing a raw material mixed solution of raw materials of a hydrothermal reaction or a solvothermal reaction; making the raw material mixed solution in a plug flowing and reacting state to obtain a reacted material; and making the reacted material in a complete mixing and reacting state. The lithium iron phosphate can be continuously produced by the apparatus and method.

The present invention relates to nanostructured materials for use in rechargeable energy storage devices such as lithium batteries, particularly rechargeable secondary lithium batteries, or lithium-ion batteries (LIBs). The present invention includes materials, components, and devices, including nanostructured materials for use as battery active materials, and lithium ion battery (LIB) electrodes comprising such nanostructured materials, as well as manufacturing methods related thereto. Exemplary nanostructured materials include silicon-based nanostructures such as silicon nanowires and coated silicon nanowires, nanostructures disposed on substrates comprising active materials or current collectors such as silicon nanowires disposed on graphite particles or copper electrode plates, and LIB anode composites comprising high-capacity active material nanostructures formed on a porous copper and/or graphite powder substrate.

Process for the preparation of electrodes from a porous material making it possible to obtain electrodes that are useful in electrochemical systems and that have at least one of the following properties: a high capacity in mAh/gram, a high capacity in mAh/liter, a good capacity for cycling, a low rate of self-discharge, and a good environmental tolerance.

Various methods and apparatus relating to three-dimensional battery structures and methods of manufacturing them are disclosed and claimed. In certain embodiments, a three-dimensional battery comprises a battery enclosure, and a first structural layer within the battery enclosure, where the first structural layer has a first surface, and a first plurality of conductive protrusions extend from the first surface. A first plurality of electrodes is located within the battery enclosure, where the first plurality of electrodes includes a plurality of cathodes and a plurality of anodes, and wherein the first plurality of electrodes includes a second plurality of electrodes selected from the first plurality of electrodes, each of the second plurality of electrodes being in contact with the outer surface of one of said first plurality of conductive protrusions. Some embodiments relate to processes of manufacturing energy storage devices with or without the use of a backbone structure or layer.

Systems and methods for the treatment of materials with an alkali metal such as lithium for the manufacturing of batteries and capacitors. In one illustrative embodiment, a liquid lithium composition may be formed by dissolving metallic lithium in a solution that includes a suitable organic agent, a suitable solvent and suitable film forming agent. Each component of the solution may be present in an effective amount to perform its desired function. The lithium may be dissolved into the solution to obtain a lithium to organic agent molar ratio of from 1:1 to 10:1. The liquid lithium composition may then be dispensed onto a suitable substrate material and allowed to remain thereon for a suitable time for a prelithiation reaction to proceed, followed by drying. Dispensing may be performed by spraying the liquid lithium composition and drying may be performed at a relatively low temperature and a reduced pressure.

An electrical energy storage device and a method of forming such electrical energy storage device. The electrical energy storage device includes an electrolyte that is arranged to dissipate energy when subjected to external mechanical load applied to the electrical energy storage device. The electrolyte includes a polymer matrix of at least two crosslinked structures, including a first polymeric material and a second polymeric material; and an electrolytic solution retained by the polymer matrix.

The formation method of graphene includes the steps of forming a layer including graphene oxide over a first conductive layer; and supplying a potential at which the reduction reaction of the graphene oxide occurs to the first conductive layer in an electrolyte where the first conductive layer as a working electrode and a second conductive layer with a as a counter electrode are immersed. A manufacturing method of a power storage device including at least a positive electrode, a negative electrode, an electrolyte, and a separator includes a step of forming graphene for an active material layer of one of or both the positive electrode and the negative electrode by the formation method.

Among other things, the present disclosure relates to re-purposing used lithium-ion batteries. The present disclosure includes treating an electrode using a solvent prior to electrochemically relithiating the electrode. In some embodiments, the relithiation may be done using a roll-to-roll device, wherein the electrode may be secured on a first pin and a second pin, then it may be unwound and submerged in an electrolyte solution. Lithium ions may be inserted into the electrode using a voltage. The layer of lithium may provide lithium ions to the electrode.

The formation method of graphene includes the steps of forming a layer including graphene oxide over a first conductive layer; and supplying a potential at which the reduction reaction of the graphene oxide occurs to the first conductive layer in an electrolyte where the first conductive layer as a working electrode and a second conductive layer with a as a counter electrode are immersed. A manufacturing method of a power storage device including at least a positive electrode, a negative electrode, an electrolyte, and a separator includes a step of forming graphene for an active material layer of one of or both the positive electrode and the negative electrode by the formation method.

The present invention provides a cathode active material dehydration apparatus using electroosmosis, the dehydration apparatus accommodating a cathode active material that has passed through a washing process, and applying an electric field to the cathode active material to remove, through electroosmosis, a washing solution remaining in the cathode active material.