Injection device (56) for discharging a gas (54), in particular a process gas (54), onto a material (12), in particular onto a battery cathode material (14) that is to be calcined, having at least one inlet (58) through which the gas (54) can be supplied to the injection device (56), and at least one outlet (60) through which the gas (54) can be discharged from the injection device (56), the inlet and outlet being connected to one another by a flow path (62) for the gas (54). According to the invention, the flow path (62) has a heat exchanger (64) with a heat exchanger housing (68) which is accessible from the outside for an ambient atmosphere (66) and in which a duct arrangement (70) is integrated. The duct arrangement (70) comprises a first flow duct (72.1) and a second flow duct (72.2) between which there is formed a redirection region (74.1) such that the gas (54) can flow through the first and second flow duct (72.1, 72.2) in different main flow directions. The invention further relates to a process gas system (52) for supplying a gas (54) and to a device (10) and a method for the thermal or thermo-chemical treatment of material.

A process and apparatus for manufacture of biocide products are described. The biocide properties arise from the caustic calcined powder, from carbonates such as such as magnesite and dolomite, and from hydroxides such as brucite. The method of manufacture is based on the production of high surface area oxide particles using an indirectly heated counterflow reactors for specifically calcining the carbonates and the hydroxides without significant sintering. The biocide products may be a powder or a hydrated slurry. A hydrated slurry is preferred for agricultural applications as a spray. For aquaculture applications, the products have a preferred particle size distribution to impact the aquatic and benthic ecosystems, and a Ca/Mg ratio that promotes the growth of the cultivates species when applied as a powder or a slurry. For applications such as a marine paint, the powder product or the slurry product is mixed with various agents to form a setting coating, and is applied to the infrastructure that is otherwise subject to biofilm growth.

A fluidized-bed-type apparatus and method for treating gypsum, which activates or improves fluidity of gypsum powder to promote an effect of treatment of gypsum, such as modification or homogenization of the gypsum powder. The apparatus for treating gypsum includes a reactor vessel, a conditioned air supply port, a horizontal partition wall and a plurality of stationary vanes. The wall allows a conditioned air flow to flow upward into a reaction region. The vanes are arranged at an angular interval in a circumferential direction. A fluidized bed of calcined gypsum is provided in the vessel. The vane deflects the conditioned air flow flowing upward into the reaction region, toward a radially outward and circumferential direction of the reaction region. The calcined gypsum makes a saltational fluid motion or saltational movement in the vessel with the air flow.

A method and an apparatus for destroying biosecurity hazards in quarantined feed materials and producing valuable products that are safe and have economic value is disclosed. The apparatus includes a continuous converter (3) that has a reaction chamber (5) for producing a solid carbon-containing product, a gas product, and optionally an oil product and a separate water-based condensate product in the chamber, via pyrolysis or other reaction mechanisms.

A method for processing a mixture of recycled polyester material and a polyester prepolymer from a polyester manufacturing process, wherein a recycled polyester material is mixed with a polyester prepolymer, from a polyester manufacturing process, and treated in a bulk thermal treatment reactor (7) with a process gas which flows in a counter-current or a cross-current flow direction to the flow direction of the mixture. In this process, the process gas, before entering a catalyst vessel (14), is passed through a protective bed (11) containing a solid adsorbent material that removes high-boiling organic substances or organic substances, with a high combustion temperature, from the process gas stream.

A process and apparatus for manufacture of biocide products are described. The biocide properties arise from the caustic calcined powder, from carbonates such as such as magnesite and dolomite, and from hydroxides such as brucite. The method of manufacture is based on the production of high surface area oxide particles using an indirectly heated counterflow reactors for specifically calcining the carbonates and the hydroxides without significant sintering. The biocide products may be a powder or a hydrated slurry. A hydrated slurry is preferred for agricultural applications as a spray. For aquaculture applications, the products have a preferred particle size distribution to impact the aquatic and benthic ecosystems, and a Ca/Mg ratio that promotes the growth of the cultivates species when applied as a powder or a slurry. For applications such as a marine paint, the powder product or the slurry product is mixed with various agents to form a setting coating, and is applied to the infrastructure that is otherwise subject to biofilm growth.

A method of producing black phosphorus which includes the steps of: weighing and mixing reaction raw materials which comprises metallic tin, red phosphorus and monocrystalline iodine, wherein a weight ratio of tin: red phosphorus: iodine is 0.6-3.5: 5-45: 0.1-0.8; feeding the mixture to a high-temperature resistant metal reaction tube; removing air by introducing inert gas and sealing the reaction tube tightly; placing the metal reaction tube inside a muffle furnace for carrying out calcination reaction by first increasing a temperature at a preset rate to a maximum temperature and keeping warm and then decreasing a temperature at a preset rate and keeping warm, then to room temperature so that the black phosphorus is produced. The conversion rate is very high and the quality of the produced product is classified as high quality.

A device for producing black phosphorus which includes a reactor having one end connected to a feeding pipe and another end connected to a discharge pipe; a propeller blade unit including a rotating shaft mounted between the two ends of the reactor and a blade element mounted on the rotating shaft; a motor connected to the rotating shaft for controlling a rotation speed of the blade element; a heating device enclosing the reactor at an outer side and defines the reactor into a plurality of heating zones; and an inert gas input connected to the discharge pipe. The device is simple and safe in operation, can optimize the production process at low cost, and has high level of automation, thus facilitating a continuous production of black phosphorus under normal pressure.

The present disclosure relates to processes and apparatus for calcination of particulate feedstock using process waste gas. In at least one embodiment, a process includes heat treating a particulate carbon feedstock in a heating system to form an activated carbon. The process includes removing a waste gas from the heating system. The process includes introducing the waste gas with a particulate material in a thermal oxidizer coupled with the heating system to form a calcined material. In at least one embodiment, a process includes heat treating a particulate carbon feedstock in a heating system to form an activated carbon. The process includes separating a waste gas from the heating system. The process includes introducing the waste gas with a particulate material in a duct coupled with a thermal oxidizer.

The disclosure relates to a co-current co-precipitation method of CoNiO.sub.2 thermistor powders. The method comprises the steps of mixing, stirring, precipitating, aging, suction filtration, washing and drying firstly using nickel nitrate and cobalt nitrate as raw materials to obtain cobalt hydroxide, and then calcining in a tubular furnace at an inert atmosphere to prepare CoNiO.sub.2 nano powders. The method has the advantages of simple operation, low cost, short cycle, high yield and no environmental pollution, and further oxidization of the CoNiO.sub.2 nano material into NiCo.sub.2O.sub.4 thermistor powders can be effectively avoided through selection and adjustment of calcination process parameters and inert atmosphere. A high-precision, fast-response and small-volume temperature sensor material can be prepared from CoNiO.sub.2 thermistor powders obtained by the method of the disclosure.