B01J2219/0286

FERRITIC STEEL PARTS IN UREA PLANTS

The application provides in an aspect a process for producing urea in a urea plant comprising a high pressure synthesis section comprising a reactor, wherein the process comprises reacting NH.sub.3 feed and CO.sub.2 feed under urea formation conditions in said reactor to form a urea synthesis solution comprising urea, water, carbamate and ammonia, wherein the process further comprises contacting a carbamate—containing liquid stream with an equipment part of said high pressure synthesis section that is made of a ferritic steel alloy.

DUPLEX STAINLESS STEEL AND FORMED OBJECT THEREOF

The present disclosure relates to a corrosion resistant duplex stainless steel (ferritic austenitic alloy) which is suitable for use in a plant for the production of urea and uses thereof. The disclosure also relates to objects made of said duplex stainless steel. Furthermore, the present disclosure relates to a method for the production of urea and to a plant for the production of urea having one or more parts made from the duplex stainless steel, and to a method of modifying an existing plant for the production of urea.

DEVICE AND METHOD FOR CONTINUOUSLY PRODUCING CATALYSTS BASED ON LOW-TEMPERATURE COPRECIPITATION
20210316294 · 2021-10-14 ·

The present disclosure discloses a device and a method for continuously producing catalysts based on low-temperature coprecipitation. The device mainly includes: a metal salt preparation kettle, a primary reaction kettle, a secondary reaction kettle, a precipitant preparation kettle, a circulating refrigeration system, an automatic control system, a non-aqueous solvent storage tank and a water storage tank. Independent preparation kettles are provided for rapid dissolution of the raw materials, and can be used to prepare the raw materials for the next batch during the reactions that are carried out in the primary and secondary reaction kettles; the circulating refrigeration system refrigerates the primary and secondary reaction kettles, and thus during the reaction, the low-temperature precipitant makes it possible to offset the precipitation reaction heat and the heat caused by the stirring in the primary reaction kettle, and improve the refrigeration efficiency of the primary reaction kettle.

Fenton apparatus for safety of industrial exothermic reactions

A Fenton apparatus of the present disclosure includes a reactor vessel, gas injection inlets that allow ejection of aeration coolant perpendicular to axis of the reactor vessel to agitate a reaction composition present in the reactor vessel under vortex conditions, a jacket cooling loop encasing the reactor vessel to allow circulation of a jacket coolant selected from a group consisting of forced air, nitrogen gas, and water, a coil cooling loop coiling around the reactor vessel to allow circulation of a coil coolant selected from a group consisting of forced air, nitrogen gas, water, and carbon dioxide. Multiple programmable solenoid valves are provided to individually control injection of the aeration coolant, the jacket coolant, and the coil coolant. A controller is provided to communicate with a temperature sensor and each programmable solenoid valve.

Corrosion resistant duplex steel alloy, objects made thereof, and method of making the alloy

Disclosed is a Hot Isostatic Pressed ferritic-austenitic steel alloy, as well objects thereof. The elementary composition of the alloy comprises, in percentages by weight: TABLE-US-00001 C  0-0.05; Si 0-0.8; Mn 0-4.0; Cr more than 29-35; Ni 3.0-10;  Mo 0-4.0; N 0.30-0.55;   Cu 0-0.8; W 0-3.0; S  0-0.03; Ce 0-0.2;
the balance being Fe and unavoidable impurities. The objects can be particularly useful in making components for a urea production plant that require processing such as machining or drilling. A preferred use is in making, or replacing, liquid distributors as used in a stripper as is typically present in the high-pressure synthesis section of a urea plant.

METHOD FOR PRODUCING A LITHIUM BIS(FLUOROSULFONYL)IMIDE SALT

A method for producing a lithium bis(fluorosulfonyl)imide salt F—(SO.sub.2)—NLi—(SO.sub.2)—F, comprising a step comprising a step of chlorination of sulfamic acid HO—(SO.sub.2)—NH.sub.2 in order to obtain the bis(chlorosulfonyl)imide Cl—(SO.sub.2)—NH—(SO.sub.2)—Cl, said step being carried out in a reactor made of a corrosion-resistant material M3, or in a reactor containing a base layer made of a material M1 coated with a surface layer made of a corrosion-resistant material M2.

OZONIZED BIOCHAR: PHOSPHORUS SUSTAINABILITY AND SAND SOILIZATION
20210198162 · 2021-07-01 ·

The present invention discloses a systematic method for phosphorus sustainability, sand soilization and odor removal utilizing the phosphorus-unlocking and odor removing green chemistry of a surface-oxygenated biochar composition made through ozonization in combination with sonication. Surface-oxygenated biochar compositions and sonication-ozonization methods create advanced hydrophilic biochar materials having higher cation exchange capacity, optimized pH, improved wettability, and toxin free components. These sonicated and ozonized biochar compositions are used as filtration materials for clean water and air, as phosphorus solubilizing reagents to mix with phosphate rock materials to make a slow-releasing phosphate fertilizer, as biochar soil additives to help solubilize phosphorus and reduce phosphorus fertilizer additions required to achieve desired soil phosphorus activity, crop uptake, and yield goals, as sand soilization reagents by utilizing their liquid gel-forming activity in the spaces among sand particles to retain water and nutrients and hold the sand particles together, as plant growth stimulants by using the humic acids-like surface-oxygenated biochar substances at a proper ppm concentration and as carbon sequestration agents to help control climate change for energy and environmental sustainability on Earth.

METHOD FOR MODIFYING FLUORINE DISTRIBUTION IN A HYDROCARBON COMPOUND
20210114955 · 2021-04-22 ·

The present invention relates to a process for modifying the fluorine distribution in a hydrocarbon compound, comprising a step of making contact between said hydrocarbon compound and a catalytic composition comprising a chromium-based catalyst, said process being performed in a reactor made of a material comprising a base layer made of a material M1 and an inner layer made of a material M2, said base layer and said inner layer being laid against each other by bonding.

Urea production process and plant

Processes and plants for the production of purified urea solution are described. In a described urea production process, urea is produced in a synthesis section without a high pressure stripper and the urea solution is subjected to purification after the recovery section, to give purified urea solution and off-gas. The purification comprises e.g. steam stripping.

METHOD OF PRODUCING HYDROCARBON AND APPARATUS FOR PRODUCING HYDROCARBON

A hydrocarbon is produced by applying mechanical energy to a metal body containing stainless steel by solid-solid contact so that a contact pressure per unit area is 30 kPa or more, in the presence of a gas containing carbon dioxide and a hydrogen source, thereby adding hydrogen to carbon dioxide. Further, a hydrocarbon is produced by providing a reaction vessel for applying mechanical energy to a metal body by solid-solid contact in the presence of a gas containing carbon dioxide and a hydrogen source, a gas introduction unit for introducing the gas containing carbon dioxide to the reaction vessel, a hydrogen source introduction unit for introducing the hydrogen source to the reaction vessel, and a gas discharge unit for discharging a gas containing the hydrocarbon produced in the reaction vessel, and adding hydrogen to the carbon dioxide in the reaction vessel.