C01P2002/86

Synthesis of graphene nanoribbons from monomeric molecular precursors bearing reactive alkyne moieties

A method of forming a graphene nanoribbon includes: 1) providing monomeric precursors each including an alkyne moiety and at least one aromatic moiety bonded to the alkyne moiety; 2) polymerizing the monomeric precursors to form a polymer; and 3) converting the polymer to a graphene nanoribbon.

Application of lactam as solvent in nanomaterial preparation

The present invention disclosed use of lactam as a solvent in the preparation of nanomaterials by precipitation method, sol-gel method or high temperature pyrolysis. These methods are able to recycle lactam solvent, which meet requirements of environmental protection.

METHOD FOR PREPARING Y TYPE MOLECULAR SIEVE HAVING HIGH SILICA TO ALUMINA RATIO
20170260059 · 2017-09-14 ·

Provided is a method for preparing a Y type molecular sieve having a high silica-to-alumina ratio, comprising: mixing deionized water, a silicon source, an aluminum source, an alkali source, and a tetraalkylammoniumcation source as a template agent to obtain an initial gel mixture; after aging the initial gel mixture at an appropriate temperature, feeding the gel mixture into a high pressure synthesis kettle for crystallization; separating a solid product, and drying to obtain the Y type molecular sieve having a high silica-to-alumina ratio. The method provides a phase-pure Y type molecular sieve having a high crystallinity, the SiO.sub.2/Al.sub.2O.sub.3 thereof being not less than 6.

AEI TYPE ZEOLITE, METHOD FOR PRODUCING SAME, AND USES THEREOF

Provided is a method for producing an inexpensive, high-performance AEI type zeolite and an AEI type zeolite having a Si/Al ratio of 6.5 or less by using neither an expensive Y type zeolite as a raw material nor dangerous hydrofluoric acid. The method for producing an AEI type zeolite having a Si/Al ratio of 50 or less includes: preparing a mixture including a silicon atom material, an aluminum atom material, an alkali metal atom material, an organic structure-directing agent, and water; and performing hydrothermal synthesis of the obtained mixture, in which a compound having a Si content of 20% by weight or less and containing aluminum is used as the aluminum atom material; and the mixture includes a zeolite having a framework density of 14 T/1000 Å.sup.3 or more in an amount of 0.1% by weight or more with respect to SiO.sub.2 assuming that all Si atoms in the mixture are formed in SiO.sub.2.

Phyllosilicate compositions designated CIT-13P and methods of preparing the same

The present disclosure is directed to novel phyllosilicate compositions designated CIT-13P and methods of producing and using the same.

MANUFACTURING METHOD OF SEMI-INSULATING SINGLE-CRYSTAL SILICON CARBIDE POWDER
20210395919 · 2021-12-23 · ·

The present disclosure provides a manufacturing method of semi-insulating single-crystal silicon carbide powder comprising: providing a semi-insulating single-crystal silicon carbide bulk, wherein the semi-insulating single-crystal silicon carbide bulk has a first silicon-vacancy concentration, and the first silicon-vacancy concentration is greater than 5E11 cm{circumflex over ( )}−3; refining the semi-insulating single-crystal silicon carbide bulk to obtain a semi-insulating single-crystal silicon carbide coarse particle, wherein the semi-insulating single-crystal silicon carbide coarse particle has a second silicon-vacancy concentration and a first particle diameter, the second silicon-vacancy concentration is greater than 5E11 cm{circumflex over ( )}−3, and the first particle diameter is between 50 μm and 350 μm; self-impacting the semi-insulating single-crystal silicon carbide coarse particle to obtain a semi-insulating single-crystal silicon carbide powder, wherein the semi-insulating single-crystal silicon carbide powder has a third silicon-vacancy concentration and a second particle diameter, the third silicon-vacancy concentration is greater than 5E11 cm{circumflex over ( )}−3, and the second particle diameter is between 1 μm and 50 μm.

METHOD FOR PRODUCING SOLID ELECTROLYTE, AND ELECTROLYTE PRECURSOR

A solid electrolyte contains a thio-LISICON Region II-type crystal structure, where the solid electrolyte does not contain P.sub.2S.sub.6.sup.4− structure. A solid electrolyte, where:

(1) a signal of a thio-LISICON Region II-type crystal structure is observed in the solid .sup.31P-NMR spectrometry, and

(2) a signal of a P.sub.2S.sub.6.sup.4− structure is not observed in the solid .sup.31P-NMR spectrometry.

GRAPHENE DISPERSION AND METHOD FOR PREPARING THE SAME
20210371618 · 2021-12-02 ·

A graphene dispersion includes a graphene and a polyol compound selected from the group consisting of an aromatic polyol represented by Formula (I), and a modified aromatic polyol made by subjecting the aromatic polyol represented by Formula (I) and an epoxidized vegetable oil to a ring opening reaction,

##STR00001## wherein p and q are independently integers ranging from 1 to 20. A method for preparing the graphene dispersion, a composition for preparing a polyurethane composite material, and a polyurethane composite material made from the composition are also disclosed.

METHOD OF FLUORESCENT NANODIAMONDS PRODUCTION
20210371742 · 2021-12-02 ·

The present invention relates to a fluorescent nanodiamond preparing method including a first operation of preparing nanodiamonds having an average particle diameter of 10 nm or less, a second operation of implanting plasma ions into the nanodiamonds, a third operation of heat-treating the nanodiamonds implanted with the plasma ions under a vacuum or inert gas atmosphere, a fourth operation of oxygen treatment of the heat-treated nanodiamonds under a gas atmosphere including oxygen to oxidize the surfaces of the nanodiamonds, a fifth operation of acid-treating the oxygen-treated nanodiamonds, a sixth operation of centrifuging and cleaning the acid-treated nanodiamonds, and a seventh operation of drying the cleaned nanodiamonds, wherein, in the second operation, the plasma ions are implanted at an incident ion dose of 10.sup.13 ions/cm.sup.2 or more and 10.sup.20 ions/cm.sup.2 or less.

Ligand-exchanged zeolite imidazolate frameworks

Disclosed are zeolitic imidazolate framework (ZIF) compositions in which at least a portion of the ligands in its shell have been exchanged with other ligands, and methods of making such shell-ligand-exchanged ZIFs. Also disclosed is the use of such shell-ligand-exchanged ZIFs in hydrocarbon separation processes.