Method of concentrating aqueous alkali and apparatus suitable for this purpose. A very energy-saving method of concentrating aqueous alkali originating, for example, from a chloralkali electrolysis plant and an apparatus suitable for this purpose are described. The method/the apparatus utilizes heat of reaction from the formation of 1,2-dichloroethane and includes multistage concentration of the aqueous alkali, where at least part of the heat required for concentrating the aqueous alkali originates from the plant for preparing 1,2-dichloroethane and at least a further part of the heat required for concentrating the aqueous alkali originates from at least one of the higher stages of the plant for concentrating the aqueous alkali and is used for partial heating of the first stage. The apparatus can be used for retrofitting existing integrated plants made up of a DCE plant and chloralkali electrolysis or in the erection of new plants.

A method for fabricating a super-hydrophobic surface having excellent surface strength and an evaporator having the super-hydrophobic surface fabricated by the method are provided. The method includes preparing a metal base material, anodizing the metal base material to form a ceramic layer having a complex structure of a microstructure and nano-fiber structures on a surface of the metal base material, and applying a hydrophobic polymer material on the complex structure to form a polymer layer having the same surface shape as the complex structure.

Distillative process for obtaining ditrimethylolpropane from solutions includes separating ditrimethylolpropane from the solution in a first distillation unit into a first tops fraction comprising low-boiling compounds having a lower boiling point than ditrimethylolpropane and a first bottoms fraction; introducing the first bottoms fraction into a second distillation unit having at least 5 theoretical plates, said unit being configured as a thin-film evaporator with a column attachment and drawing off a second tops fraction comprising intermediate-boiling compounds having a lower boiling point than ditrimethylolpropane as well as withdrawing a second bottoms fraction from the second distillation unit and introducing the second bottoms fraction into a third distillation unit having at least 4 theoretical plates, said unit being configured as a thin-film evaporator with a column attachment, such that ditrimethylolpropane is obtained as a third tops fraction and high boilers are removed as a third bottoms fraction.

A system for processing cannabinoids and recovering solvent has a vessel for a mixture of cannabinoids and solvent. A pump forms a vacuum in the system to draw the mixture into a first heat exchanger to pre-heat the mixture. A falling film evaporator receives the mixture from the first heat exchanger, and boils the mixture to form a solvent vapor. The falling film evaporator collects the cannabinoids from the mixture as a crude oil. The first heat exchanger receives the solvent vapor. Heat is transferred to incoming mixture of the system, and cools and condenses the solvent vapor to form solvent condensate and vapor. A second heat exchanger receives and further cools the solvent condensate and vapor to form further condensed solvent and some solvent vapor. The pump receives the further condensed solvent and some solvent vapor and increases pressure to form solvent liquid and recovers solvent liquid for reuse.

A process for conversion of a hydro-carbonaceous feed including ionic halides to a hydrocarbon product stream by hydrotreatment, wherein the stream is combined with wash water, the weight ratio between wash water and hydrocarbon product stream water is between 1:10 and 10:1, wherein the combined hydrocarbon product stream and wash water are separated in a non-polar stream of hydrocarbon product and a polar stream of wash water including ionic halides, such that from 50% of the ionic halides are transferred from the hydrocarbon product stream to the polar stream of wash water including ionic halides, wherein the polar stream of wash water is directed to a means of concentrating, to provide a stream of purified water and a stream of brine having a concentration of ionic halides being more than 2 times and less than 100 times above that of the polar stream of waste water including ionic halides.

The present disclosure relates to isolating one or more cannabinoids from an input mixture. There is disclosed an apparatus that comprises a first reaction vessel, a volatizing unit, and a distillation unit. The first reaction vessel provides a derivatized input mixture that comprises one or more derivatized cannabinoids. The volatizing unit volatilizes the derivatized input mixture into a derivatized cannabinoid-containing vapor-stream and a residue. The distillation unit receives the derivatized cannabinoid-containing vapor stream and separates a first derivatized cannabinoid within the derivatized cannabinoid-containing vapor stream from at least a second cannabinoid. There is also a method that comprises the steps of derivatizing one or more cannabinoids in an input mixture; volatilizing the derivatized input mixture to provided a derivatized cannabinoid-containing vapor stream; conducting the derivatized cannabinoid-containing vapor stream to distillation unit; and collecting a product that comprises the first derivatized cannabinoid.

A method is disclosed for stripping in a stripper a urea synthesis solution received from a urea forming process wherein ammonia and CO2 are reacted under urea forming conditions. The shell space of the stripper comprises a continuous vertical zone.

Falling film evaporator systems, devices, and methods are disclosed in the present application. In some embodiments, the falling film evaporator system can include a hollow cylindrical glass tube configured to enclose the major parts of the falling film evaporator system. Furthermore, in some embodiments, inserted into the cylindrical glass tube is another hollow evaporator tube with a dispensing bowl at the top, a reservoir of the dispending bowl facing the inside top of the cylindrical glass tube. Inserted into the hollow evaporator tube is a heating element configured to heat the hollow evaporator tube such that an outside surface of the evaporator tube is heated. At the top of the hollow cylindrical glass is an inlet where liquid flows into the dispensing bowl, spilling over the edges of the bowl, generating a thin film of liquid that is evaporated as it falls down the outside surface of the evaporator tube.

A heat exchanger apparatus includes a tube having a wall with an inner surface and an outer surface. The tube is configured to receive heat exchange fluid at one end, and output, when heated through the wall, vapor of the heat exchange fluid at the opposing end. A first layer of thermally conductive porous material is disposed on the inner surface of the tube. Heating equipment, a heat exchanger, and a method of heating are also disclosed.

A method of making a cobalt compound for feed supplements includes the steps of dissolving cobalt acetate tetrahydrate in water to form a mixture, adding an acid to the mixture, sonicating the mixture for a selected time, removing acetic acid from the mixture, and separating crystals of the cobalt compound from the mixture.