The present disclosure relates to a system and method for synthesis of condensed, nano-carbon materials to create nanoparticles. In one embodiment the system may have a source of liquid precursor, a flow control element and a shock wave generating subsystem. The flow control element is in communication with the source of the liquid precursor and creates a jet of liquid precursor. The shock wave generating subsystem drives a shock wave through at least a substantial portion of a thickness of the jet of liquid precursor to sufficiently compress the jet of liquid precursor, and to increase a pressure and a temperature of the jet of liquid precursor, to create solid state nanoparticles.

A polycrystalline diamond construction comprising a body of polycrystalline diamond material formed of a mass of diamond grains exhibiting inter-granular bonding, wherein between around 50 wt % to around 99 wt % of the diamond grains in a cross-section of the body of polycrystalline diamond material taken at any orientation have a sectorial growth structure. A method of making the polycrystalline diamond construction is also disclosed.

The present disclosure relates to a system and method for synthesis of condensed, nano-carbon materials to create nanoparticles. In one embodiment the system may have a source of liquid precursor, a flow control element and a shock wave generating subsystem. The flow control element is in communication with the source of the liquid precursor and creates a jet of liquid precursor. The shock wave generating subsystem drives a shock wave through at least a substantial portion of a thickness of the jet of liquid precursor to sufficiently compress the jet of liquid precursor, and to increase a pressure and a temperature of the jet of liquid precursor, to create solid state nanoparticles.

A vertical autoclave according to an embodiment of the present disclosure is a vertical autoclave including an inlet port through which a process solution is introduced, an outlet port through which the process solution is discharged, an oxygen inlet port through which oxygen is supplied to the process solution, an agitator configured to mix the process solution, an inner wall, an acid-resistant brick layer lined on a lower portion and a side portion of the inner wall, and an acid-resistant metal layer lined on an upper portion of the inner wall. A method of removing salt from an autoclave includes raising a surface level of a solution in the autoclave from a first level to a second level such that salt in the autoclave is immersed in the solution, and maintaining the surface level of the solution at the second level. The salt is dissolved in the solution while the surface level of the solution is maintained at the second level.

A polycrystalline diamond construction comprising a body of polycrystalline diamond material formed of a mass of diamond grains exhibiting inter-granular bonding, wherein between around 50 wt % to around 99 wt % of the diamond grains in a cross-section of the body of polycrystalline diamond material taken at any orientation have a sectorial growth structure. A method of making the polycrystalline diamond construction is also disclosed.

A method of forming polycrystalline diamond comprised placing a plurality of graphene nano-platelets into a capsule; and subjecting the platelets to a pressure of around 10 GPa to around 20 GPa and a temperature of around 1600 degrees Celsius to around 3000 degrees Celcius to convert the graphene platelets to nano-polycrystalline diamond. There is also disclosed a polycrystalline super hard construction comprising a polycrystalline diamond region comprising polycrystalline diamond material formed according to said method.

A vertical autoclave according to an embodiment of the present disclosure is a vertical autoclave including an inlet port through which a process solution is introduced, an outlet port configured through which the process solution is discharged, an oxygen inlet port through which oxygen is supplied to the process solution, an agitator configured to mix the process solution, an inner wall, an acid-resistant brick layer lined on a lower portion and a side portion of the inner wall, and an acid-resistant metal layer lined on an upper portion of the inner wall.

Disclosed herein are systems and methods for producing H2 from low carbon fuels (LCFs) using metal oxides in a chemical looping process.

Methods of forming polycrystalline diamond include encapsulating diamond particles and a hydrocarbon substance in a canister, and subjecting the encapsulated diamond particles and hydrocarbon substance to a pressure and a temperature sufficient to form inter-granular bonds between the diamond particles. Cutting elements for use in an earth-boring tool include a polycrystalline diamond material formed by such processes. Earth-boring tools include such cutting elements.

Methods of forming polycrystalline diamond include encapsulating diamond particles and a hydrocarbon substance in a canister, and subjecting the encapsulated diamond particles and hydrocarbon substance to a pressure and a temperature sufficient to form inter-granular bonds between the diamond particles. Cutting elements for use in an earth-boring tool includes a polycrystalline diamond material formed by such processes. Earth-boring tools include such cutting elements.