B01J2219/00096

PRESSED SILICON CARBIDE CERAMIC (SIC) FLUIDIC MODULES WITH INTEGRATED HEAT EXCHANGE
20230219053 · 2023-07-13 ·

A silicon carbide flow reactor fluidic module comprises a monolithic closed-porosity silicon carbide body, a tortuous fluid passage extending through the silicon carbide body, the tortuous fluid passage having an interior surface, and one or more thermal control fluid passages also extending through the silicon carbide body, the interior surface having a surface roughness of less than 10 μm Ra. A process for forming such modules is also disclosed.

Method and system for polymer production

Disclosed herein is a system for solution polymerization comprising a reactor system that is operative to receive a monomer and to react the monomer to form a polymer; a plurality of devolatilization vessels located downstream of the reactor system, where each devolatilization vessel operates at a lower pressure than the preceding devolatilization vessel; and a heat exchanger disposed between two devolatilization vessels and in fluid communication with them, where the heat exchanger has an inlet port temperature of 100° C. to 230° C., an outlet port temperature of 200° C. to 300° C., an inlet port pressure of 35 to 250 kgf/cm.sup.2 and an outlet port pressure of 20 to 200 kgf/cm.sup.2; and wherein the polymer solution remains in a single phase during its residence in the heat exchanger.

IMPROVED CONTINUOUS FLOW REACTOR FOR PHOTOCHEMICAL PROCESSES WITH CONCAVE-FACED SIDES

The invention provides a reactor assembly (1) comprising a reactor (30), wherein the reactor (30) is configured for hosting a fluid (100) to be treated with light source radiation (11) selected from one or more of UV radiation, visible radiation, and IR radiation, wherein the reactor (30) comprises a reactor wall (35) which is transmissive for the light source radiation (11), wherein: (i) the reactor (30) is a tubular reactor (130), and wherein the reactor wall (35) defines the tubular reactor (130); (ii) the tubular reactor (130) is configured in a tubular arrangement (1130); and (iii) the reactor assembly (1) further comprises a reactor support element (40), wherein (a) the reactor support element (40) encloses at least part of the tubular arrangement (1130) or wherein (b) the tubular arrangement (1130) encloses at least part of the reactor support element (40); wherein part of the tubular arrangement (1130) is configured in contact with the reactor support element (40), and wherein another part of the tubular arrangement (1130) and the reactor support element (40) define one or more fluid transport channels (7).

Reactor and Method for Carrying Out a Chemical Reaction

A reactor for carrying out a chemical reaction, which has a reactor vessel and one or more reaction tubes, wherein power input elements for electrical heating of the reaction tube(s) are guided into the reactor vessel. It is provided that the power input elements each have a rod-shaped section that, in each case, runs at a wall passage through a wall of the reactor vessel in such a way that a connection chamber into which the rod-shaped sections project is arranged outside the reactor vessel and adjacently to the wall of the reactor vessel through which the rod-shaped sections run at their wall passages, and that cooling panels through which a cooling fluid can flow are provided in the connection chamber and are arranged between at least two or between at least two groups of the rod-shaped sections that project into the connection chamber.

POLYGONAL CONTINUOUS FLOW REACTOR FOR PHOTOCHEMICAL PROCESSES

The invention provides a photoreactor assembly (1) comprising a reactor (30), wherein the reactor (30) is configured for hosting a fluid (100) to be treated with light source radiation (11) selected from one or more of UV radiation, visible radiation, and IR radiation, wherein the reactor (30) comprises a reactor wall (35) which is transmissive for the light source radiation (11), wherein: (i) the reactor (30) is a tubular reactor (130), and wherein the reactor wall (35) defines the tubular reactor (130); (ii) the tubular reactor (130) is configured in a tubular arrangement (1130); (iii) the photoreactor assembly (1) further comprises a light source arrangement (1010) comprising a plurality of light sources (10) configured to generate the light source radiation (11), wherein the reactor wall (35) is configured in a radiation receiving relationship with the plurality of light sources (10); and (iv) one or more of the tubular arrangement (1130) and the light source arrangement (1010) defines a polygon (50).

POLYGONAL FLOW REACTOR FOR PHOTOCHEMICAL PROCESSES

The invention provides a photoreactor assembly (1) comprising a reactor (30), wherein the reactor (30) is configured for hosting a fluid (100) to be treated with light source radiation (11) selected from one or more of UV radiation, visible radiation, and IR radiation, wherein the reactor (30) comprises a reactor wall (35) which is transmissive for the light source radiation (11), wherein the photoreactor assembly (1) further comprises: a light source arrangement (1010) comprising a plurality of light sources (10) configured to generate the light source radiation (11), wherein the reactor wall (35) is configured in a radiation receiving relationship with the plurality of light sources (10); one or more fluid transport channels (7) configured in functional contact with one or more of (i) the reactor (30) and (ii) one or more of the plurality of light sources (10); a cooling system (90) configured to transport a cooling fluid (91) through the one or more fluid transport channels (7).

IMPROVED COOLING OF TUBE CONTAINING REACTANTS

The invention provides a reactor assembly (1) comprising a reactor (30), wherein the reactor (30) is configured for hosting a fluid (100) to be treated with light source radiation (11) selected from one or more of UV radiation, visible radiation, and IR radiation, wherein the reactor (30) comprises a reactor wall (35) which is transmissive for the light source radiation (11), wherein: the reactor (30) is a tubular reactor (130), and wherein the reactor wall (35) defines the tubular reactor (130); the tubular reactor (130) is configured in a tubular arrangement (1130); the reactor assembly (1) further comprises a reactor support element (40), wherein the reactor support element (40) comprises a track (42), wherein the track (42) partly encloses the tubular reactor (130), wherein the reactor support element (40) comprises a thermally conductive element (2), and wherein the tubular reactor (130) is configured in thermal contact with the thermally conductive element (2).

HEAT EXCHANGER COMPRISING AT LEAST ONE PARTICLE FILTER, METHOD OF ASSEMBLING SUCH A HEAT EXCHANGER
20220236022 · 2022-07-28 ·

The invention concerns a heat exchanger having an exchange body having first passages for the flow of a first fluid and second passages for the flow of a second fluid exchanging heat with the first fluid, a first inlet manifold for introducing the first fluid into the first passages, a first outlet manifold for discharging the first fluid from the first passages). The heat exchanger also includes an inlet filter arranged facing the inlet surface of the exchange body, and/or an outlet filter arranged facing the outlet surface of the exchange body, the inlet filter and/or the outlet filter having a sheet metallic material selected from a metal gauze, a non-woven fabric of metallic fibres, a sintered metallic powder or sintered metallic fibres.

REACTOR FOR CARRYING OUT A GAS-LIQUID TWO-PHASE HIGH-PRESSURE REACTION WITH A FOAMING MEDIUM

A reactor for performing a gas/liquid biphasic high-pressure reaction with a foaming medium, comprising an interior formed by a cylindrical, vertically oriented elongate shell, a bottom and a cap, wherein the interior is divided by internals into a backmixed zone and a zone of limited backmixing, wherein the backmixed zone and the zone of limited backmixing are consecutively traversable by the reaction mixture, wherein the backmixed zone comprises means for introducing gas and liquid and a gas outlet and also comprises at least one mixing apparatus selected from a stirrer, a jet nozzle and means for injecting the gas, and the zone of limited backmixing comprises a reaction product outlet, a first cylindrical internal element which in the interior extends in the longitudinal direction of the reactor and which delimits the zone of limited backmixing from the backmixed zone, backmixing-preventing second internal elements in the form of random packings, structured packings or liquid-permeable trays arranged in the zone of limited backmixing and a riser tube whose lower end is arranged within the backmixed zone and whose upper end opens into the zone of limited backmixing so that liquid from the backmixed zone can ascend into the zone of limited backmixing via the riser tube, wherein flow into the zone of limited backmixing enters from below. The reactor is configured such that the high-pressure reaction space is optimally utilized and contamination of workup steps or subsequent reactions arranged downstream of the high-pressure reaction with foam is substantially avoided. The invention further relates to a process for performing a continuous gas/liquid biphasic high-pressure reaction in the reactor.

CONTINUOUS PRODUCTION OF POLYURETHANE PREPOLYMERS

Described herein is a continuous process for producing polyurethane prepolymers in a residence time reactor with plug flow. Also described herein is a method of using these prepolymers for producing polyurethanes.