The present disclosure relates to an apparatus for preparing an oligomer, including: a reactor receiving a monomer stream and performing an oligomerization reaction to prepare a reaction product; a product discharge line for transferring a reaction product stream discharged from the reactor; and a bubble catcher provided in any area of the product discharge line to remove bubbles contained in the reaction product stream.

System and methods for plasma treatment of a fluidized bed of particles are disclosed. The systems include an energy coupling zone configured to generate a plasma from microwave radiation and an interface element configured to propagate the plasma from the energy coupling zone to a reaction zone. The reaction zone is configured to receive the plasma, receive a plurality of reactant particles in a fluidization plane direction from a fluidization assembly positioned below the reaction zone, and form a product in presence of the plasma. The fluidization plane is substantially perpendicular to the propagated plasma.

The present invention relates to a pressure vessel (1, 1′), having a lower part (20) and the lid (24) which can be locked to one another, in order, in the state in which they are locked to one another, to surround a reaction chamber (22) on all sides as a pressure space for initiating and/or promoting chemical and/or physical pressure reactions of samples (P) which are received in the reaction chamber (22), and a fluid inlet (FE) with a check valve (4) for feeding a fluid into the reaction chamber (22), the check valve (4) extending at least partially in the lid (24).

A foam sensor device is used for monitoring foam within a vessel. The sensor (e.g. accelerometer) is encapsulated inside a water-tight, sterilizable, shell, which floats on a liquid contained. In one example, the foam sensor device includes an accelerometer for detecting and measuring rotation and movement of the foam sensor device and generates movement data based on the detected movement. During a learning or calibration process, sensor data (e.g., movement data) from the foam sensor device is analyzed and classified using machine learning and/or signal processing methods to extract features indicative of different possible foam statuses, including varying levels of foam, or no foam and generate models for the different statuses. During normal operation, the foam sensor device transmits sensor data to an analyzer containing the pre-calibrated models, which determines whether there is foam or not. Based on the foam status, a pump controller adds anti-foam solution.

An elastomer rheology process can include: receiving material formation data associated with an elastomer; conveying the elastomer towards one or more rollers that compress and stretch the elastomer according to a predetermined rolling profile comprising roller gap and speed settings; sensing a first dimension of a first portion of the elastomer before the first portion of the elastomer is passed through the sheeter; sensing a second dimension of a second portion of the elastomer after the second portion of the elastomer is passed through the sheeter; and calculating an elastomer property of the elastomer based on the controlled roller gap width, a measured roller force, the first dimension, and the second dimension.

The invention relates to a method for an economically and technically improved embodiment of a production interruption in a production method for isocyanates by phosgenation of the corresponding amines, in which the entire production plant is not closed while one or more parts of the plant is taken out of operation, rather the input materials and/or reaction products available in the production plant are recirculated through at least one part of the plant that has not been taken out of operation. The invention further relates to a plant for producing isocyanates and to a method for operating a plant for producing isocyanates.

A method can include: mixing two or more feedstocks to produce a distillate product; optionally adding a cetane improver to the distillate product; collecting the distillate product in a tank; extracting a distillate product sample from the distillate product after mixing and before collecting in the tank; measuring a derived cetane number and/or a indicated cetane number (DCN/ICN) for the distillate product sample with an online DCN/ICN analyzer; communicating the DCN/ICN to a plant distributed control system; calculating an integrated DCN/ICN for the cumulative distillate product in the tank based on the measured DCN/ICN, previously measured DCN/ICN for portions of the distillate product in the tank, and process variables related to the mixing and cetane improver; and adjusting one or more of the process variables based on the integrated DCN/ICN.

A process for the regeneration of a catalyst is presented. The catalyst is in a reactor for use in benzene alkylation, and periodically needs to be regenerated. The reactor is taken off-line, and a regenerant is passed through the reactor, producing an effluent stream. A portion of the effluent stream is recycled through the reactor without passing through a clean-up process.

A reactor as a heat treatment device includes heat transfer structures removably placed in first flow channels, a first information acquisition unit connected to the inlet side of the first flow channels to acquire information for specifying a temperature and a flow rate of the first fluid which are reference conditions after lapses of time, a second information acquisition unit connected to the outlet side of the first flow channels to acquire the information for specifying the temperature of the first fluid after each lapse of time, and a control unit that calculates a heat exchange amount after each lapse of time in accordance with the temperature and the flow rate specified according to the information acquired by the first information acquisition unit and the second information acquisition unit, so as to estimate a service life of the heat transfer structures in accordance with the heat exchange amount.

A reactor as a heat treatment device includes heat transfer structures removably placed in first flow channels, a first information acquisition unit connected to the inlet side of the first flow channels to acquire information for specifying a temperature and a flow rate of the first fluid which are reference conditions after lapses of time, a second information acquisition unit connected to the outlet side of the first flow channels to acquire the information for specifying the temperature of the first fluid after each lapse of time, and a control unit that calculates a heat exchange amount after each lapse of time in accordance with the temperature and the flow rate specified according to the information acquired by the first information acquisition unit and the second information acquisition unit, so as to estimate a service life of the heat transfer structures in accordance with the heat exchange amount.