Patent classifications
B01J2219/0213
METHOD FOR PRODUCING A LITHIUM BIS(FLUOROSULFONYL)IMIDE SALT
A method for producing a lithium bis(fluorosulfonyl)imide salt F—(SO.sub.2)—NLi—(SO.sub.2)—F, comprising a step comprising a step of chlorination of sulfamic acid HO—(SO.sub.2)—NH.sub.2 in order to obtain the bis(chlorosulfonyl)imide Cl—(SO.sub.2)—NH—(SO.sub.2)—Cl, said step being carried out in a reactor made of a corrosion-resistant material M3, or in a reactor containing a base layer made of a material M1 coated with a surface layer made of a corrosion-resistant material M2.
Process and apparatus for production of granular polycrystalline silicon
Prolonged operation campaigns in a fluidized bed reactor for producing granular polysilicon by deposition of silicon onto silicon seed particles from a silicon-containing precursor gas is made possible by employing a silicon-coated reaction tube which is not insulated above a region of the fluidized bed and as a result has a lower temperature such that the ratio of the thickness of the silicon on the reactor tube adjoining the fluidized bed to the coating thickness over the total reactor tube is from 7:1 to 1.5 to 1 after production campaign of from 15 to 500 days.
PROCESS AND APPARATUS FOR PRODUCTION OF GRANULAR POLYCRYSTALLINE SILICON
Prolonged operation campaigns in a fluidized bed reactor for producing granular polysilicon by deposition of silicon onto silicon seed particles from a silicon-containing precursor gas is made possible by employing a silicon-coated reaction tube which is not insulated above a region of the fluidized bed and as a result has a lower temperature such that the ratio of the thickness of the silicon on the reactor tube adjoining the fluidized bed to the coating thickness over the total reactor tube is from 7:1 to 1.5 to 1 after production campaign of from 15 to 500 days.