This invention relates to a robotic device 10.1, 10.2 and method for handling catalyst material 106, 206 in a reactor 100 by removing spent catalyst from the reactor and/or loading the reactor with fresh catalyst without an operator having to enter an interior of the reactor which increases operator safety. The robotic device includes a body 12, which is configured to engage a flange 104 of the reactor, and a handling arm which is configured for use both as a cleaning arm 18 and a loading arm 218. The handling arm is connected to the body and is angularly and longitudinally displaceable relative to the body. The handling arm has a segment which is telescopically extendible/retractable relative to the body. When used as a cleaning arm, the arm receives a vacuum line for removing catalyst. When used as a loading arm, a telescopic loading sleeve is connected to the segment.

Provided herein are methods for effectively loading reactor material into fixed bed reactors. The subject methods and systems for loading catalyst particles and inert particles onto a reactor bed utilize a novel sock having a helical-shape that can restrict reactor material traveling through the elevation of the fixed bed reactor to the reactor bed and avoid damaging the reactor material upon impact. The sock comprises a cylindrical tube having a plurality of helixes. Each helix of the cylindrical tube has a downward slope. The downward slope of each helix exceeds an angle of repose of the reactor material. The present methods and system are particularly effective for improving the performance of reactor bed configurations of vertically-oriented fixed bed reactors and flow distribution through the bed at designated operating conditions.

This invention relates to a robotic device 10.1, 10.2 and method for handling catalyst material 106, 206 in a reactor 100 by removing spent catalyst from the reactor and/or loading the reactor with fresh catalyst without an operator having to enter an interior of the reactor which increases operator safety. The robotic device includes a body 12, which is configured to engage a flange 104 of the reactor, and a handling arm which is configured for use both as a cleaning arm 18 and a loading arm 218. The handling arm is connected to the body and is angularly and longitudinally displaceable relative to the body. The handling arm has a segment which is telescopically extendible/retractable relative to the body. When used as a cleaning arm, the arm receives a vacuum line for removing catalyst. When used as a loading arm, a telescopic loading sleeve is connected to the segment.

An apparatus and process for the activation of catalyst material utilized in ammonia cracking can include an initial use of hydrogen and heat to perform an initial stage of catalyst activation and a subsequent use of ammonia and heat to perform a subsequent state of catalyst activation. The subsequent use of ammonia can be configured so that different catalytic material at different plant elements are activated in a pre-selected sequence to provide activation of the catalytic material utilized in different plant elements. Some embodiments can be configured to avoid excess temperatures that can be detrimental to equipment that can be positioned upstream of a furnace in some embodiments while also avoiding sintering of the catalytic material.