B22F2301/20

STEEL TO TUNGSTEN FUNCTIONALLY GRADED MATERIAL SYSTEMS
20230043638 · 2023-02-09 ·

Functionally graded materials may comprise a graded volume extending between a tungsten-based structure and a steel-based structure, where the graded volume comprises a plurality of additively manufactured layers. At least one of the plurality of additively manufactured layers may comprise a ternary element selected from vanadium and chromium. Some of the additively manufactured layers may further comprise aluminum.

METHODS OF MANUFACTURING OF MOLYBDENUM AND MOLYBDENUM-BASED STRUCTURES BY ELECTRON BEAM ADDITIVE MANUFACTURING, PARTICULARLY STRUCTURES FOR NUCLEAR COMPONENTS

Methodologies and manufacturing processes to manufacture components by electron beam melting additive manufacturing, particularly components of molybdenum or a molybdenum-based alloy and particularly of complex nuclear component geometries. Input parameters are provided for controlling electron beam melting additive manufacturing equipment, such as electron beam melting machines. The input parameters relate to various process steps, including build set-up, initial thermal treatment, initial layering of powder, pre-consolidation thermal treatment, consolidation, post-consolidation thermal treatment, indexing of layers, and post-build thermal treatment. The methodologies and manufacturing processes allow manufacture of components of molybdenum having a purity of ≥99.0% and a density of ≥99.75%. Metallographic cross-sections of the manufactured molybdenum components were porosity-free and crack-free.

Sputtering target

A sputtering target containing molybdenum and at least one metal from the group tantalum and niobium. The average content of tantalum and/or niobium is from 5 to 15 at % and the molybdenum content is greater than or equal to 80 at %. The sputtering target has at least a matrix with an average molybdenum content of greater than or equal to 92 at % and particles which are composed of a solid solution containing at least one metal from the group of tantalum and niobium, and molybdenum, with an average molybdenum content of greater than or equal to 15 at % and are embedded in the matrix. There is also described a method of producing a sputtering target.

Additively manufactured component and production method therefor
11565322 · 2023-01-31 · ·

A component includes a multiplicity of individual powder particles of Mo, a Mo-based alloy, W or a W-based alloy that have been fused together to give a solid structure by a high-energy beam via an additive manufacturing method. The component has an oxygen content of not more than 0.1 at %. An additive manufacturing method includes producing the powder via the melt phase and providing a carbon content in the region of not less than 0.15 at %. The components are crack-free and have high grain boundary strength.

Dust core and inductor element

A dust core includes large particles having an average particle size of 8-15 μm, medium particles having an average particle size of 1-5 μm, and small particles having an average particle size of 300-900 nm when a cross section thereof is observed. An area ratio occupied by the large particles is 50% to 90%, an area ratio occupied by the medium particles is 0% to 30%, and an area ratio occupied by the small particles is 5% to 30%, when a total area ratio occupied by the large particles, the medium particles and the small particles is 100% in the cross section. Vickers hardness (Hv) of the large particles, the medium particles and the small particles is 150-600 respectively. The small particles are alloy powder containing Fe and at least Si or N. The dust core may be included in an inductor element.

METHOD FOR FORMING METAL SINTERED BODY
20230024857 · 2023-01-26 ·

Provided is a method of forming a sintered metal, the method including a first step of inserting tungsten (W) powder in a graphite mold, a second step of interposing tantalum (Ta) foil between the W powder and the graphite mold, and a third step of forming sintered W from the W powder through a sintering process.

METHOD FOR PRODUCING MOLYBDENUM ALLOY TARGETS

The present invention relates to a method for producing a molybdenum alloy target, and solves the problem of low density and coarser grains of the molybdenum alloy targets in the prior art. The present invention comprises subjecting a mixed powder with a mass ratio depending upon the formula composition of a molybdenum alloy to a pre-press forming process to obtain a preformed molybdenum alloy target blank; placing the preformed molybdenum alloy target blank in a capsule and subjecting the capsule to processes of preheating for degassing and vacuum seal welding; subjecting the target blank to a hot isostatic pressing process to obtain a densified molybdenum alloy prefabricated target; removing the capsule; and subjecting the molybdenum alloy prefabricated target with the capsule removed to a temperature-rising and pressure-decreasing process, followed by finish machining to obtain a molybdenum alloy target.

METAL-Si BASED POWDER, METHOD FOR PRODUCING SAME, METAL-Si BASED SINTERED BODY, SPUTTERING TARGET, AND METAL-Si BASED THIN FILM MANUFACTURING METHOD
20230220538 · 2023-07-13 · ·

A metal-Si based powder contains a metal-Si based particle including a plurality of crystal phase grains. The crystal phase grains include a crystal phase containing a compound of a metal and Si. The crystal phase grains have an average grain size of, for example, 20 μm or less. The metal-Si based particle has an average particle size of, for example, 5 to 100 μm.

METHOD FOR PRODUCING PELLETIZED FUEL FROM URANIUM-MOLYBDENUM POWDERS

The invention relates to the nuclear industry and can be used for producing fuel pellets from uranium-molybdenum metal powders enriched to 7% uranium 235 for nuclear reactor fuel elements. The pellets are sintered in an inert atmosphere of argon at a temperature ranging from 1100° C. to 1155° C., and the initial powder is a uranium-molybdenum powder having a fraction size of 160 .Math.m and a molybdenum con¬tent of 9.0 to 10.5 wt%. The powder is pre-heated at a temperature of 500° C. for 10-20 hours (in an atmosphere of argon) and is subsequently cold pressed into pellets in a die under a force of up to 950 MPa. In an alternative emb¬odiment for producing uranium-molybdenum pellets with a binder (plasticizer), the step of sintering is preceded by heating the pellets in an atmosphere of argon at 300° C. to 450° C. for 2-4 hours to remove the binder. The invention makes it possible to increase the uranium intensity of the fuel, reduce the amount of heat buildup in a reactor core, and lower the amount of energy released in the event of abnormalities in the operation of a nuclear reactor, thus providing increased reactor safety and resilience to accidents.

Spherical tantalum powder, products containing the same, and methods of making the same

Tantalum powder that is highly spherical is described. The tantalum powder can be useful in additive manufacturing and other uses. Methods to make the tantalum powder are further described as well as methods to utilize the tantalum powder in additive manufacturing processes. Resulting products and articles using the tantalum powder are further described.