C01F11/36

CALCIUM NITRATE AND POTASSIUM NITRATE FERTILISER PARTICLES

The present disclosure concerns fertilizer particles comprising calcium nitrate and potassium nitrate. It is found that fertilizer particles comprising 43 to 47% w/w calcium nitrate and 46 to 54% w/w potassium nitrate can be produced by melt granulation. Due to undercooling problems, such particles were not expected to be suitable for industrial production by melt granulation. However, the present disclosure provides a composition which forms a low viscosity melt with short solidification time. This was successfully achieved by reducing the water content of a fertilizer melt comprising 43 to 47% w/w calcium nitrate and 46 to 54% w/w potassium nitrate to less than 3% w/w of the melt.

Calcium nitrate and potassium nitrate fertiliser particles

The present disclosure concerns fertilizer particles comprising calcium nitrate and potassium nitrate. It is found that fertilizer particles comprising 43 to 47% w/w calcium nitrate and 46 to 54% w/w potassium nitrate can be produced by melt granulation. Due to undercooling problems, such particles were not expected to be suitable for industrial production by melt granulation. However, the present disclosure provides a composition which forms a low viscosity melt with short solidification time. This was successfully achieved by reducing the water content of a fertilizer melt comprising 43 to 47% w/w calcium nitrate and 46 to 54% w/w potassium nitrate to less than 3% w/w of the melt.

Prevention of the emission of hydrogen sulphide in the production of hot bitumen or asphalt

The present application relates to a method to prevent the emission of hydrogen sulphide in the production of hot bitumen or asphalt having a temperature of between 150 and 200° C., wherein the method comprises the steps of providing a bituminous or asphalt mixture, heating the mixture until a temperature of between 150-200° C. and adding an aqueous calcium nitrate solution or a calcium nitrate powder while mixing the bituminous or asphalt mixture. The present application furthermore relates to the use of an aqueous calcium nitrate solution or a calcium nitrate powder during mixing of a bituminous or asphalt mixture in the production of a hot bitumen or asphalt having a temperature of between 150 and 200° C. to prevent the emission of hydrogen sulphide.

SYSTEM FOR THE PRODUCTION OF MOLTEN SALT USED AS A HEAT TRANSFER MEDIUM FOR A PYROLYSIS SYSTEM
20210187441 · 2021-06-24 ·

A system for the production of molten salt. The system can have a preparation tank configured to melt raw salts, and a bubbler system in communication with the preparation tank. The bubbler can be configured to maintain vacuum conditions within the preparation tank and to remove gases from the preparation tank. A method for producing molten salt includes a step of providing a system for the production of molten salt. The system can have a preparation tank configured to melt raw salts, and a bubbler system in communication with the preparation tank. The bubbler can be configured to maintain vacuum conditions within the preparation tank and to remove gases from the preparation tank. Then, the method can include inserting raw salt into the preparation tank, and heating the raw salt to form molten salt. Then filtering the molten salt, and storing the molten salt.

Methionine-metal chelate and manufacturing method thereof

The present disclosure relates to a preparation method of a methionine-metal chelate, and the methionine-metal chelate, which is prepared by first reacting Ca(OH).sub.2 and methionine and adding metal nitrate, can be widely used as feeds and feed additives.

Methionine-metal chelate and manufacturing method thereof

The present disclosure relates to a preparation method of a methionine-metal chelate, and the methionine-metal chelate, which is prepared by first reacting Ca(OH).sub.2 and methionine and adding metal nitrate, can be widely used as feeds and feed additives.

Method for the management of phosphogypsum

A method for the management of phosphogypsum consists in that a reactor (2) is charged with apatite and/or phosphorite phosphogypsum and with an aqueous or ammoniacal solution of ammonium carbonate and/or bicarbonate from a pre-reactor (1), at 1: (0.1-4) ratio of phosphogypsum to the aqueous or ammoniacal solution of ammonium carbonate and/or bicarbonate, the entire contents are stirred at 10 C. to 200 C. for at least 2 minutes, CO.sub.2 being released in the course of the process is directed to the pre-reactor (1), and the post-reaction mixture is directed to a filter (3) to obtain an aqueous ammonium sulphate solution, whereas the precipitate from the filter (3) is heat-treated, followed by dissolving it in nitric acid in a reactor (5), and the resultant suspension is filtered through a filter (6) to obtain an aqueous calcium nitrate solution, and CO.sub.2 being released in the reactor (5) is recirculated to the pre-reactor (1) wherein CO.sub.2 is reacted with ammonia in an aqueous solution to obtain the aqueous or ammoniacal solution of carbonate and/or bicarbonate which is directed to the reactor (2), with the process for obtaining the aqueous or ammoniacal solution of ammonium carbonate and/or bicarbonate being conducted until the pH 7-12 of the solution is reached.

Method for the management of phosphogypsum

A method for the management of phosphogypsum consists in that a reactor (2) is charged with apatite and/or phosphorite phosphogypsum and with an aqueous or ammoniacal solution of ammonium carbonate and/or bicarbonate from a pre-reactor (1), at 1: (0.1-4) ratio of phosphogypsum to the aqueous or ammoniacal solution of ammonium carbonate and/or bicarbonate, the entire contents are stirred at 10 C. to 200 C. for at least 2 minutes, CO.sub.2 being released in the course of the process is directed to the pre-reactor (1), and the post-reaction mixture is directed to a filter (3) to obtain an aqueous ammonium sulphate solution, whereas the precipitate from the filter (3) is heat-treated, followed by dissolving it in nitric acid in a reactor (5), and the resultant suspension is filtered through a filter (6) to obtain an aqueous calcium nitrate solution, and CO.sub.2 being released in the reactor (5) is recirculated to the pre-reactor (1) wherein CO.sub.2 is reacted with ammonia in an aqueous solution to obtain the aqueous or ammoniacal solution of carbonate and/or bicarbonate which is directed to the reactor (2), with the process for obtaining the aqueous or ammoniacal solution of ammonium carbonate and/or bicarbonate being conducted until the pH 7-12 of the solution is reached.

METHIONINE-METAL CHELATE AND MANUFACTURING METHOD THEREOF

The present disclosure relates to a preparation method of a methionine-metal chelate, and the methionine-metal chelate, which is prepared by first reacting Ca(OH).sub.2 and methionine and adding metal nitrate, can be widely used as feeds and feed additives.

METHIONINE-METAL CHELATE AND MANUFACTURING METHOD THEREOF

The present disclosure relates to a preparation method of a methionine-metal chelate, and the methionine-metal chelate, which is prepared by first reacting Ca(OH).sub.2 and methionine and adding metal nitrate, can be widely used as feeds and feed additives.