Patent classifications
C01F11/466
Method for preparing a-calcium sulfate hemihydrate with calcium sulfate dihydrate
A method for preparing α-calcium sulfate hemihydrate with calcium sulfate dihydrate includes steps of: uniformly mixing the calcium sulfate dihydrate with an additive solution, and obtaining a mixture, wherein weight percentages of the calcium sulfate dihydrate and the additive solution in the mixture are respectively 90.00-95.00% and 5.00-10.00%, and the additive solution contains water, inorganic salt, organic salt, organic acid, surfactant, and seed crystal; rising a temperature of the mixture to 130-150° C., keeping for 20-120 minutes, and the calcium sulfate dihydrate in the mixture transforming to the α-calcium sulfate hemihydrate; drying the mixture after reaction at 105-160° C., and thereafter obtaining α-calcium sulfate hemihydrate product. The used calcium sulfate dihydrate can be natural raw materials and industrial by-products. The industrial by-products can be directly applied. Through utilizing characteristics of the industrial by-products, a dehydration reaction time and a drying time are shortened, and a product quality is obviously increased.
Calcined gypsum treatment device and calcined gypsum treatment method
A calcined gypsum treatment apparatus has an agitating type of cooler provided with a cooling region for cooling the calcined gypsum, and a moisture supplying device for incorporating moisture into the calcined gypsum. The moisture supplying device includes a humid gas-feeding port which introduces humid gas including moisture or steam, directly into the cooling region. The calcined gypsum is introduced through a calcined gypsum introduction port into the cooling region, and the moisture is incorporated into the calcined gypsum to modify the calcined gypsum. The humid gas-feeding port is positioned in vicinity to the calcined gypsum introduction port so as to allow the spouted or delivered flow of the humid gas to be brought into contact with the calcined gypsum immediately after introduced into the cooling region.
SULFUR MANAGEMENT METHOD
A method of managing sulfur in a sulfur-containing stream may include steps of providing a sulfur-containing stream; converting sulfur within the sulfur-containing stream to elemental sulfur; transporting the elemental sulfur to a location at or near a sulfur oxide injection location; converting the elemental sulfur to sulfur oxides; recovering electrical energy from said step of converting the elemental sulfur to sulfur oxides; injecting the sulfur oxides into the sulfur oxide injection location. The method may include steps of screening a plurality of injection locations and selecting, from the screened plurality of injection locations, a particular sulfur dioxide injection location with specific reservoir characteristics for the sulfur oxides.
Method for producing phosphoric acid and by-producing alpha-hemihydrate gypsum by wet-process
Provided is a method for producing phosphoric acid and at the same time obtaining alpha-hemihydrate gypsum including: adding a phosphate rock powder and a part of dilute sulfuric acid into an extraction tank, carrying out an extraction reaction on same, separating a clear liquid from the obtained mixed slurry, sending the clear liquid, as a finished product phosphoric acid, into an acid storeroom, and transferring a separated solid, together with the rest mixed slurry, into a crystal transformation tank; and adding sulfuric acid and a crystal transformation agent into the crystal transformation tank, carrying out a crystal transformation reaction for 1.5-7.5 h at 60 C.-130 C., and solid-liquid separating the obtained mixed acid slurry, wherein the solid can be dried into a gypsum powder, or may be not subjected to a drying step and made into gypsum products such as gypsum boards, gypsum building blocks and gypsum members by directly adding water.
Method for producing calcium sulfate
A method for preparing calcium sulphate comprising a production of DCP by the attack of a source of phosphate by an acid, a digestion of the isolated DCP by the sulphuric acid under conditions giving rise to the formation of a first slurry of gypsum suspended in an acidic aqueous phase having a content of free SO.sub.3 equal to or less than 1.5% and a content of free P.sub.2O.sub.5, a conversion of at least part of said first slurry by heating to a temperature greater than 80 C. and potentially by adding sulphuric acid, with solubilisation of the gypsum crystals and recrystallisation of the solubilised calcium sulphate in a second slurry of -calcium sulphate hemihydrate crystals suspended in an aqueous phase based-on phosphoric acid, wherein the content of free SO.sub.3 is less than 10% by weight, and a separation between said aqueous phase and a filter cake based on particularly pure -calcium sulphate hemihydrate.
Method for producing calcium sulphate hemihydrate with unique properties
The present invention relates to a new method for producing a calcium sulphate hemihydrate with unique properties for use for therapeutic applications in the cosmetic or pharmaceutical industry. Calcium sulphate hemihydrate is a biocompatible and biodegradable inorganic substance and thus suitable as a carrier in pharmaceutical compositions, e.g. a controlled release composition, containing at least one pharmaceutically active ingredient.
Two-stage calcination method, and plant for same
A method for the calcination of powdery or fine-particled plaster, comprising two steps: the plaster is subjected to a flash-calcination in a calcinator and the hot plaster is post-calcinated in a reaction vessel. Post-calcination is carried out in the reaction vessel by adding humid gas, said reaction vessel not being heated. The postcalcination takes place over a long period of time, that is at least 10 times, preferably 50-100 times longer than the amount of time taken for flash calcination. Calcination takes place without expending additional energy, and the remaining dihydrate produced during the flash calcination is also transformed into semi-hydrate and undesired anhydrite fractions are reduced. The method can ensure consistency in the product quality and also increase product quality. The temperature in the upstream calcinator can be lowered thus saving more energy. The method can also be used to accelerate the ageing of calcinated plaster.
METHOD FOR PRODUCING CALCIUM SULPHATE HEMIHYDRATE WITH UNIQUE PROPERTIES
The present invention relates to a new method for producing a calcium sulphate hemihydrate with unique properties for use for therapeutic applications in the cosmetic or pharmaceutical industry. Calcium sulphate hemihydrate is a biocompatible and biodegradable inorganic substance and thus suitable as a carrier in pharmaceutical compositions, e.g. a controlled release composition, containing at least one pharmaceutically active ingredient.
METHOD FOR PRODUCING CALCIUM SULFATE
A method for preparing calcium sulphate comprising a production of DCP by the attack of a source of phosphate by an acid, a digestion of the isolated DCP by the sulphuric acid under conditions giving rise to the formation of a first slurry of gypsum suspended in an acidic aqueous phase having a content of free SO.sub.3 equal to or less than 1.5% and a content of free P.sub.2O.sub.5, a conversion of at least part of said first slurry by heating to a temperature greater than 80 C. and potentially by adding sulphuric acid, with solubilisation of the gypsum crystals and recrystallisation of the solubilised calcium sulphate in a second slurry of -calcium sulphate hemihydrate crystals suspended in an aqueous phase based-on phosphoric acid, wherein the content of free SO.sub.3 is less than 10% by weight, and a separation between said aqueous phase and a filter cake based on particularly pure -calcium sulphate hemihydrate.
Method for producing calcium sulphate hemihydrate with unique properties
The present invention relates to a new method for producing a calcium sulphate hemihydrate with unique properties for use for therapeutic applications in the cosmetic or pharmaceutical industry. Calcium sulphate hemihydrate is a biocompatible and biodegradable inorganic substance and thus suitable as a carrier in pharmaceutical compositions, e.g. a controlled release composition, containing at least one pharmaceutically active ingredient.