According to some embodiments method for making an optical fiber preform comprises the steps of: (i) placing a plurality of rods with an outer surface having a coefficient of friction 0.02≦COF≦0.3 into an inner cavity of an apparatus; (ii) placing particulate glass material in the inner cavity between the rods and an inner wall of the mold cavity; and (iii) applying pressure against the particulate glass material to press the particulate glass material against the plurality of rods.

A supercontinuum source, comprises a pump source and a supercontinuum generator configured for receiving electromagnetic radiation derived from the pump source and for generating supercontinuum radiation, the supercontinuum generator comprising a nonlinear microstructured optical fibre having a core region comprising silica. The core region includes a dopant selected to reduce light-induced non-bridging oxygen hole centre loss in the nonlinear microstructured optical fibre.

A new type of all-silica optical fiber is described; a Structured Silica Clad Silica (SSCS) optical fiber, whose cladding is structured to provide mode mixing within the core; and/or to have an average effective refractive index. Its cross-section is essentially symmetrical, it can be used, among other objects, to provide flatter, more speckle-free outputs from fiber lasers, or other limited mode photonic sources. Building the new fiber structure around a rare earth doped laser core provides a better fiber laser/amplifier for cladding pumping. The structured silica cladding contains paired layers, in which a down doped silica layer is followed by a layer of pure, or lesser down-doped, or even up-dope silica, and die number of paired layers is, typically, from 5 to about 25, and, generally, within the paired layers the ratio of thickness of the higher RI layer of silicate the down-doped silica is very broad, lying between about 0.0625 to about 16, depending on the intended use of the SSCS fibers. In some versions, the main core material can be up-doped silica with pure silica or down-doped silica as the primary second component.

The production and new type of preforms are presented which yield, upon drawing, new, class of optical fibers, improved, speckle-free output optical fibers. Useful fibers, providing speckle-free, smooth output with flat top transmission of light from gaussian or few mode sources are produced from preforms introduced herein. The unique production of these improved preforms is also presented. The preforms, and thus the fibers produced in varying core dimensions from about 100 μm to above 1000 μm, are based on a structured silica section of mode mixing area adjacent to the inner core, or in the case of non-circular core, within the core. Plasma Vapor Deposition process is modified to achieve the structured sections in a well-controlled manner. The structured sections are composed of a number of pairs of layers, where a thin down-doped layer is alternated with a much thicker core material layer. The ratio of the thickness of the core layer to the thickness of the down-doped layer is about 3 to 25. The number of paired layers is typically between about 8 to 30-layer pairs. The effective NA of the structured section is dependent on the particulars of the structured silica section and of the individual down-doped layer. Both circular inner core examples and non-circular core examples are possible and are discussed, herein.

One exemplary embodiment of this disclosure relates to a transfer molding assembly. The assembly includes a die having a molding cavity interconnected with a reservoir. The assembly further includes a heater operable to heat the die, and a load plate configured to move under its own weight to transfer material from the reservoir into the molding cavity.

A method for adjusting an etchability of a first borosilicate glass by heating the first borosilicate glass; combining the first borosilicate glass with a second borosilicate glass to form a composite; and etching the composite with an etchant. A material having a protrusive phase and a recessive phase, where the protrusive phase protrudes from the recessive phase to form a plurality of nanoscale surface features, and where the protrusive phase and the recessive phase have the same composition.

Annealing treatments for modified titania-silica glasses and the glasses produced by the annealing treatments. The annealing treatments include an isothermal hold that facilitates equalization of non-uniformities in fictive temperature caused by non-uniformities in modifier concentration in the glasses. The annealing treatments may also include heating the glass to a higher temperature following the isothermal hold and holding the glass at that temperature for several hours. Glasses produced by the annealing treatments exhibit high spatial uniformity of CTE, CTE slope, and fictive temperature, including in the presence of a spatially non-uniform concentration of modifier.

The present disclosure relates to a method for forming a glass, ceramic or composite material. The method may involve initially forming a plurality of tubes and then performing a coating operation to coat the plurality of tubes with materials containing metal or metalloid elements, including inorganic compounds, organometallic compounds, or coordination complexes to form coated tubes. The method may further include performing at least one of a thermal operation or a thermochemical operation on the coated tubes to form a solid glass, ceramic, or composite structure with dimensions representing at least one of a rod or fiber.

Methods for forming a sintered patch on a silicon-based substrate are disclosed. The methods include applying a patch slurry on the silicon-based substrate, drying the patch slurry on the silicon-based substrate to form a dried patch material, and sintering the dried patch material in an oxidizing atmosphere to form a sintered patch on the silicon-based substrate. The patch slurry includes a patch material containing silicates in a fluid carrier.

An example of an optical fiber includes an attenuating cladding disposed around a first waveguide (e.g., a core) and a waveguide (e.g., a waveguide cladding) disposed around the attenuating cladding. An attenuating cladding may be a doped layer that may be doped with, for example, a dopant comprising metal. A first waveguide and a second waveguide may each transmit light for a distinct sample characterization technique. An example of an optical fiber includes a core, a first intermediate cladding disposed around the core, an attenuating cladding disposed around the first intermediate cladding, an attenuating cladding disposed around the first intermediate cladding, a second intermediate cladding disposed around the attenuating cladding, a waveguide cladding disposed around the second intermediate cladding, and outer cladding disposed around the waveguide cladding, and an outer coating around the outer cladding. An optical fiber may be formed using a rod-in-tube process.