Patent classifications
C03B2201/40
Continuous sol-gel process for producing silicate-containing glasses or glass ceramics
A continuous sol-gel process for producing silicate-containing glasses and glass ceramics is proposed, comprising the following steps: (a) continuously feeding a silicon tetraalkoxide, a silicon alkoxide with at least one non-alcoholic functional group and an alcohol into a first reactor (R1), and at least partially hydrolyzing by the addition of a mineral acid to obtain a first product stream (A); (b) continuously providing a second product stream (B) in a second reactor (R2) by feeding a metal alkoxide component or continuously mixing an alcohol and a metal alkoxide component; (c) continuously mixing product streams (A) and (B) in a third reactor (R3) for producing a presol to obtain a third product stream (C); (d) continuously adding water or a diluted acid to the product stream (C) to obtain a sol (gelation); (e) continuously filling the emerging sol into molds to obtain an aquagel; (f) drying the aquagels to obtain xerogels; (g) sintering the xerogels to obtain silicate-containing glasses and glass ceramics.
CONTINUOUS SOL-GEL PROCESS FOR PRODUCING SILICATE-CONTAINING GLASSES OR GLASS CERAMICS
A continuous sol-gel process for producing silicate-containing glasses and glass ceramics is proposed, comprising the following steps: (a) continuously feeding a silicon tetraalkoxide, a silicon alkoxide with at least one non-alcoholic functional group and an alcohol into a first reactor (R1), and at least partially hydrolyzing by the addition of a mineral acid to obtain a first product stream (A); (b) continuously providing a second product stream (B) in a second reactor (R2) by feeding a metal alkoxide component or continuously mixing an alcohol and a metal alkoxide component; (c) continuously mixing product streams (A) and (B) in a third reactor (R3) for producing a presol to obtain a third product stream (C); (d) continuously adding water or a diluted acid to the product stream (C) to obtain a sol (gelation); (e) continuously filling the emerging sol into molds to obtain an aquagel; (f) drying the aquagels to obtain xerogels; (g) sintering the xerogels to obtain silicate-containing glasses and glass ceramics.
METHODS OF FERRULE RESHAPING FOR CORRECTING CORE-TO-FERRULE CONCENTRICITY ERRORS, AND OPTICAL FIBER CABLE ASSEMBLIES RELATED TO SUCH METHODS
Methods of reshaping ferrules (20) used in optical fiber cables assemblies (170) are disclosed. The reshaping methods reduce a core-to-ferrule concentricity error (E), which improves coupling efficiency and optical transmission. The methods include measuring a distance (δ) and angular direction (θ) from a true center (30) of the ferrule to the core (46), wherein the true center (30) is based on an outer surface (26) of the ferrule. The methods also include reshaping at least a portion (26P) of the ferrule (20) to define a new true center (30′) of the ferrule (20) and reduce the distance (δ). A variety of reshaping techniques are also disclosed.
Optical fibers and preforms with one step fluorine trench and overclad and methods for making the same
A method is provided that includes: forming a low-index trench region with a first density; forming an inner barrier layer comprising silica around the trench region at a second density greater than the first density; depositing silica-based soot around the first barrier layer to form an overclad region at a third density less than the second density; inserting a core cane into a trench-overclad structure; forming an outer barrier layer comprising silica in an outer portion of the overclad region at a fourth density greater than the third density; flowing a down dopant-containing gas through the trench-overclad structure to dope the trench region with the down dopant, and wherein the barrier layers mitigate diffusion of the down-dopant into the overclad region; and consolidating the trench-overclad and the core cane.
DOPED FUSED SILICA COMPONENT FOR USE IN A PLASMA-ASSISTED MANUFACTURING PROCESS AND METHOD FOR PRODUCING THE COMPONENT
Doped quartz glass components for use in a plasma-assisted manufacturing process contain at least one dopant which is capable of reacting with fluorine to form a fluoride compound, and the fluoride compound has a boiling point higher than that of SiF.sub.4. The doped quartz glass component has high dry-etch resistance and low particle formation, and has uniform etch removal when used in a plasma-assisted manufacturing process. The doped quartz glass has a microhomogeneity defined by (a) a surface roughness with an R.sub.a value of less than 20 nm after the surface has been subjected to a dry-etching procedure as specified in the description, or (b) a dopant distribution with a lateral concentration profile in which maxima of the dopant concentration are at an average distance apart of less than 30 μm.
Continuous sol-gel process for producing silicate-containing glasses or glass ceramics
A continuous sol-gel process for producing silicate-containing glasses and glass ceramics is proposed, comprising the following steps: (a) continuously feeding a silicon tetraalkoxide, a silicon alkoxide with at least one non-alcoholic functional group and an alcohol into a first reactor (R1), and at least partially hydrolyzing by the addition of a mineral acid to obtain a first product stream (A); (b) continuously providing a second product stream (B) in a second reactor (R2) by feeding a metal alkoxide component or continuously mixing an alcohol and a metal alkoxide component; (c) continuously mixing product streams (A) and (B) in a third reactor (R3) for producing a presol to obtain a third product stream (C); (d) continuously adding water or a diluted acid to the product stream (C) to obtain a sol (gelation); (e) continuously filling the emerging sol into molds to obtain an aquagel; (f) drying the aquagels to obtain xerogels; (g) sintering the xerogels to obtain silicate-containing glasses and glass ceramics.
GLASS AND METHOD FOR MANUFACTURING THE SAME
A glass includes a first glass portion and a second glass portion. The first glass portion has a higher ion packing density than the second glass portion (has a composition that forms a glass in which, out of plastic deformation characteristics, plastic flow is dominant). The second glass has a lower ion packing density than the first glass portion (has a composition that forms a glass in which, out of the plastic deformation characteristics, densification is dominant).
METHOD FOR PRODUCING AN OPTICAL FIBRE FOR A DISTRIBUTED MEASUREMENT OF TEMPERATURE OR DEFORMATION IN A HARSH ENVIRONMENT USING THE RAYLEIGH BACKSCATTERED SIGNAL
An optical fibre, for use in the field of distributed measurement of temperature or deformation by optical reflectometry in the frequency domain using the Rayleigh backscattered signal in the fibre, includes a core doped with nanoparticles for example formed from gold particles covered with zirconium oxide, and can be subjected to high temperatures during the measurement. A method for producing the optical fibre includes a step of heat treatment during which the optical fibre is subjected, for a duration of at least one hour, to a heat treatment temperature higher than a maximum temperature to which it will be subjected during a measurement.
Ultraviolet-shielding glass sheet and vehicle window pane using the glass sheet
The present invention provides a glass sheet having a good property of blocking transmission of ultraviolet light, having a low to moderate visible transmittance, being relatively thin, being capable of substantially blocking transmission of solar ultraviolet light, and also having a good solar shielding property. The glass sheet of the present invention has a thickness of 1 to 5 mm, a Tuv 380 of 1.5% or less, a Tuv 400 of 2.5% or less, a visible transmittance (YA) of 5 to 40%, and a solar transmittance (TG) of 5 to 45%, and is formed from a glass composition, wherein the glass composition includes: 1.0 to 5.0 wt % T-Fe.sub.2O.sub.3; 1.0 to 5.0 wt % TiO.sub.2; and 50 to 600 wt. ppm CoO as coloring components in addition to predetermined base composition, a FeO ratio is 5 to 40%, and the sum of T-Fe.sub.2O.sub.3 multiplied by 2 and TiO.sub.2 is 7.0% or more.
GLASS STRAND, GLASS ROVING, AND METHOD FOR MANUFACTURING SAME
Provided is a glass strand that, when mixed with mortar, is less likely to decrease the fluidity of the mortar and can 5 effectively increase the mechanical strength of a cementitious material. A glass strand includes: a plurality of glass filaments containing 12% by mass or more ZrO.sub.2 and 10% by mass or more R.sub.2O (where R represents at least one selected from Li, Na, and K); and a coating covering surfaces of the glass filaments, 10 wherein the coating contains polyvinyl acetate resin and polyether-based urethane resin, and wherein a content of the polyether-based urethane resin in the coating is, in solid content ratio, not less than 10% by mass and not more than 90% by mass.