A method for the preparation of a composite article containing aerogel particles and ceramic fibers, as well as to a composite article obtained by this method, are described.

A method for the preparation of a composite article containing aerogel particles and ceramic fibers, as well as to a composite article obtained by this method, are described.

Provided are a heat transfer suppression sheet having an excellent heat transfer prevention effect and excellent retainability of inorganic particles and shape retainability at a high temperature, and a battery pack in which the heat transfer suppression sheet is interposed between battery cells. The heat transfer suppression sheet (10) includes inorganic particles (20), first inorganic fibers (30), and second inorganic fibers (31). The first inorganic fibers (30) are amorphous fibers. The second inorganic fibers (31) contain at least one kind selected from amorphous fibers having a glass transition point higher than that of the first inorganic fibers (30) and crystalline fibers.

Provided are a heat transfer suppression sheet having an excellent heat transfer prevention effect and excellent retainability of inorganic particles and shape retainability at a high temperature, and a battery pack in which the heat transfer suppression sheet is interposed between battery cells. The heat transfer suppression sheet (10) includes inorganic particles (20), first inorganic fibers (30), and second inorganic fibers (31). The first inorganic fibers (30) are amorphous fibers. The second inorganic fibers (31) contain at least one kind selected from amorphous fibers having a glass transition point higher than that of the first inorganic fibers (30) and crystalline fibers.

In a porous body, a surface layer thickness Ts takes a relatively small value satisfying P≧0.54 Ts (formula (1)), the surface layer thickness Ts being derived by a microstructure analysis using the porous-body data that is prepared through three-dimensional scanning of a region including a surface (inflow plane 61) of the porous body. Here, P denotes a porosity [%] of the porous body, and 0%<P<100% and 0 μm<Ts are assumed. The surface layer thickness Ts is derived as a distance in a thickness direction (X direction) between a surface-layer region start plane 92 in which a straight-pore opening ratio becomes 98% or less for the first time and a surface-layer region end plane 93 in which the straight-pore opening ratio becomes 1% or less for the first time.

In a porous body, a surface layer thickness Ts takes a relatively small value satisfying P≧0.54 Ts (formula (1)), the surface layer thickness Ts being derived by a microstructure analysis using the porous-body data that is prepared through three-dimensional scanning of a region including a surface (inflow plane 61) of the porous body. Here, P denotes a porosity [%] of the porous body, and 0%<P<100% and 0 μm<Ts are assumed. The surface layer thickness Ts is derived as a distance in a thickness direction (X direction) between a surface-layer region start plane 92 in which a straight-pore opening ratio becomes 98% or less for the first time and a surface-layer region end plane 93 in which the straight-pore opening ratio becomes 1% or less for the first time.

The honeycomb structure includes a pillar-shaped honeycomb structure body, and a circumferential coating layer disposed to surround a circumference of the honeycomb structure body, and cells which are formed at an outermost circumference of the honeycomb structure body and in which peripheries of the cells are defined by the partition walls without any lacks are defined as outermost circumference complete cells, and in a cross section of the honeycomb structure body which is perpendicular to an extending direction of the cells a minimum distance T (mm) among distances from the outermost circumference complete cells to the surface of the circumferential coating layer and a porosity P (%) of the circumferential coating layer satisfy relations of Equation (1) and Equation (2) as follows:

1.5≧T≧16×(100−P).sup.−1.4; and  Equation (1):

20≦P≦75.  Equation (2):

The honeycomb structure includes a pillar-shaped honeycomb structure body, and a circumferential coating layer disposed to surround a circumference of the honeycomb structure body, and cells which are formed at an outermost circumference of the honeycomb structure body and in which peripheries of the cells are defined by the partition walls without any lacks are defined as outermost circumference complete cells, and in a cross section of the honeycomb structure body which is perpendicular to an extending direction of the cells a minimum distance T (mm) among distances from the outermost circumference complete cells to the surface of the circumferential coating layer and a porosity P (%) of the circumferential coating layer satisfy relations of Equation (1) and Equation (2) as follows:

1.5≧T≧16×(100−P).sup.−1.4; and  Equation (1):

20≦P≦75.  Equation (2):

The present disclosure provides a preparation method of an aluminum silicate fiber-reinforced aerogel felt, including the following steps: mixing orthosilicate, ethanol, and water evenly, adding an NH.sub.4F solution and ammonia water successively, and stirring evenly to obtain a silica sol; winding an aluminum silicate fiber felt into a roll and mounting on a rotatable central shaft of a impregnation reaction kettle; where a plurality of injection holes are equidistantly provided on a surface of the reaction kettle; the central shaft of the reaction kettle drives the aluminum silicate fiber felt to rotate and slowly inject the silica sol into the surface of the fiber felt through the injection holes to conduct the impregnation; allowing the fiber felt-gel composite to stand to conduct aging; placing the aged fiber felt-gel composite in absolute ethanol to conduct solvent replacement to remove moisture; and drying to obtain the aluminum silicate fiber-reinforced aerogel felt.

Provided is a structure having both fire resistance and heat insulation properties and capable of retaining its shape without being collapsed or deformed even when exposed to a flame. The present invention provides a fire-resistant heat-insulation composition comprising 70 to 250 parts by mass of gypsum based on 100 parts by mass of calcium aluminate having a CaO content of 34% or more, and 0.1 to 20 parts by mass of a fibrous inorganic clay mineral having a crystallization water ratio of 5% or more, based on 100 parts by mass of the total of the calcium aluminate and the gypsum.