C04B2235/5252

Method of manufacturing CMC components using boron carbide
11578774 · 2023-02-14 · ·

A method of manufacturing a ceramic matrix composite component includes pressure casting a fibrous preform with a slurry comprising boron carbide and densifying the fibrous preform using a liquid source of carbon. The method may include forming holes in the fibrous preform before pressure casting the fibrous preform with the slurry. The method may also include sintering the boron carbide after the pressure casting. In various embodiments, the sintering may be performed before the densifying.

OXIDE BASED CERAMIC MATRIX COMPOSITES
20180009718 · 2018-01-11 ·

A method of making a ceramic matrix composites (CMC) having superior properties at high temperatures. The CMC can include a sol gel mixture mixed or blended metal oxide particles. The sol-gel mixture can be an aqueous colloidal suspension of a metal oxide, preferably from about 10 wt % to about 25 wt % of the metal oxide, containing a metal oxide such as alumina (Al.sub.2O.sub.3), silica (SiO.sub.2) or alumina-coated silica. The mixture can be infiltrated into a ceramic fiber, gelled, dried and sintered to form the CMC of the present teachings.

METHOD FOR PREPARING A MATERIAL MADE FROM ALUMINOSILICATE AND METHOD FOR PREPARING A COMPOSITE MATERIAL HAVING AN ALUMINOSILICATE MATRIX

The invention relates to a method for preparing a material based on an aluminosilicate selected from barium aluminosilicate BAS, barium-strontium aluminosilicate BSAS, and strontium aluminosilicate SAS, said aluminosilicate consisting of aluminosilicate with a hexagonal structure, characterised in that it includes a single sintering step in which a mixture of powders of precursors of said aluminosilicate, including an aluminium hydroxide Al(OH).sub.3 powder, are sintered by a hot-sintering technique with a pulsed electric field SPS; whereby a material based on an aluminosilicate, said aluminosilicate consisting of an aluminosilicate with a hexagonal structure is obtained. The material based on an aluminosilicate prepared by said method can be used in a method for preparing a composite material consisting of an aluminosilicate matrix reinforced by reinforcements made of metalloid or metal oxide.

METHOD FOR COATING FIBERS IN A FLUIDIZED BED

A method for coating fibers, includes desizing sized short fibers having an average length less than or equal to 5 mm, the short fibers being made of ceramic material or carbon, sieving the desized short fibers in order to separate them from any agglomerates of sized short fibers still present, introducing the desized and sieved short fibers into a reactor, and coating the short fibers in the reactor by chemical vapor deposition in a fluidized bed.

HIGH TEMPERATURE COMPOSITES AND METHODS FOR PREPARING HIGH TEMPERATURE COMPOSITES

A method for making a high temperature composite, which is a carbon carbon composite, carbon fiber reinforced ceramic matrix composite, ceramic fiber reinforced ceramic matrix composite, or a carbon silica composite, including: a) providing a precursor part including a resin comprising a poly(aryl ether ketone) (PAEK) and at least one reinforcing material, wherein the resin has a degree of crystallinity of 10% or more; b) pyrolyzing the precursor part to a pyrolyzed part; c) infusing a liquid second resin into the pyrolyzed part to make an infused part; and d) pyrolyzing the infused part to make the carbon carbon composite carbon fiber reinforced ceramic matrix composite, ceramic fiber reinforced ceramic matrix composite, or the carbon silica composite, optionally repeating steps c. through d. Also, a carbon carbon composite, carbon fiber reinforced ceramic matrix composite, ceramic fiber reinforced ceramic matrix composite, or carbon silica composite made by the method.

ELECTROSTATIC FILAMENT DISPERSAL FOR CMC APPLICATIONS

A method of preparing a woven fabric material for use in a ceramic matrix composite includes passing a desized woven fabric tape having a first inter-filament spacing through a dispersal module configured to transform the desized woven fabric tape into a dispersed woven fabric tape having a second inter-filament spacing greater than the first inter-filament spacing. The dispersal module includes a first charging element with a charged surface and disposed to apply an electric charge to the desized woven fabric tape. The method further includes applying a polymer binder to the dispersed woven fabric tape to create a stabilized woven fabric tape having the second inter-filament spacing.

Method to produce a ceramic matrix composite with controlled surface characteristics
11697623 · 2023-07-11 · ·

A method to produce a ceramic matrix composite with controlled surface characteristics includes: applying a scrim ply to a surface of a fiber preform, where the fiber preform includes silicon carbide fibers coated with boron nitride; infiltrating the fiber preform and the scrim ply with a slurry, thereby forming an impregnated ply on an impregnated fiber preform; infiltrating the impregnated fiber preform and the impregnated ply with a melt comprising silicon, and then cooling, thereby forming a ceramic matrix composite having a ceramic surface layer thereon, where the ceramic surface layer has a predetermined thickness and is devoid of boron; machining or grit blasting the ceramic surface layer to form an intermediate layer suitable for coating; and depositing an environmental barrier coating on the intermediate layer. Thus, a ceramic matrix composite coated with the environmental barrier coating is formed with the intermediate layer in between.

CVI matrix densification process

Disclosed herein is a chemical vapor infiltration method including flowing ceramic precursors through a preform and depositing a matrix material on the preform at a first gas infiltration pressure, increasing the gas filtration pressure to a second gas infiltration pressure, and lowering the gas infiltration pressure to a third gas infiltration pressure which is intermediate to the first and second gas infiltration pressures.

EMBEDDED WIRE CHEMICAL VAPOR DEPOSITION (EWCVD)

Methods of forming a ceramic matrix, as well as fiber preforms and methods of forming fiber preforms to facilitate formation of a ceramic matrix are provided. The method includes obtaining a fiber preform to facilitate forming the ceramic matrix. The fiber preform includes a fiber layer with a plurality of fibers and a heating element embedded within the fiber preform. The method also includes heating the fiber preform via the heating element embedded within the fiber preform, and depositing matrix material into the fiber preform by embedded wire chemical vapor deposition (EWCVD) of the matrix material during the heating of the fiber preform by the heating element. The chemical vapor deposition of the matrix material within the fiber preform facilitates formation of the ceramic matrix.

SHAPE FORMING OPF PREFORM

A method for manufacturing a C/C part includes fabricating an oxidized PAN fiber preform comprising a stack of sheets of multi-axial, non-crimp, OPF fabric. The method includes positioning the oxidized PAN fiber preform with a female forming tool, the female forming tool comprising a die recess, and forming the oxidized PAN fiber preform into a shaped body. The shaped body is removed from the female forming tool and moved into a graphite fixture for carbonization. The carbonized shaped body may also be densified into the final C/C part. The carbonized shaped body can also be placed in a perforated graphite fixture for densification and removed from the perforated graphite fixture between densification processes for machining and for facilitating further densification.