C04B35/63448

MONOMER FORMULATIONS AND METHODS FOR 3D PRINTING OF PRECERAMIC POLYMERS

This invention provides resin formulations which may be used for 3D printing and pyrolyzing to produce a ceramic matrix composite. The resin formulations contain a solid-phase filler, to provide high thermal stability and mechanical strength (e.g., fracture toughness) in the final ceramic material. The invention provides direct, free-form 3D printing of a preceramic polymer loaded with a solid-phase filler, followed by converting the preceramic polymer to a 3D-printed ceramic matrix composite with potentially complex 3D shapes or in the form of large parts. Other variations provide active solid-phase functional additives as solid-phase fillers, to perform or enhance at least one chemical, physical, mechanical, or electrical function within the ceramic structure as it is being formed as well as in the final structure. Solid-phase functional additives actively improve the final ceramic structure through one or more changes actively induced by the additives during pyrolysis or other thermal treatment.

Preform for making a component of a braking system
11473637 · 2022-10-18 · ·

A preform for making a component of a braking system having a fibre-reinforced ceramic composite material, obtained by forming and subsequent pyrolysis of a pre-preg is described. Also described is a component of a braking system made wholly or in part from the preform, and a method for making a preform in a fibre-reinforced ceramic composite material.

FLEXIBLE CERAMIC FIBERS AND POLYMER COMPOSITE AND METHOD OF MAKING THE SAME

The present application discloses and claims a method to make a flexible ceramic fibers (Flexiramics™) and polymer composites. The resulting composite has an improved mechanical strength (tensile) when compared with the Flexiramics™ alone. Several different polymers can be used, both thermosets and thermoplastics. Flexiramics™ has unique physical characteristics and the composite materials can be used for numerous industrial and laboratory applications.

CERAMIC SCINTILLATOR FIBER

A method is for the production of a scintillator fiber. In an embodiment, the method includes provisioning a suspension of a binder dissolved in a solvent and a scintillator material; and pressing the suspension into a precipitation bath in which the binder is insoluble.

GREEN CERAMIC BATCH MIXTURES COMPRISING AN INVERSE EMULSION AND METHODS FOR FORMING A CERAMIC BODY
20220055949 · 2022-02-24 ·

Green ceramic batch mixtures include: at least one inorganic batch component, preferably cordierite; at least one binder, preferably polyisoprene, poly(vinyl formal), poly(vinyl methyl ether), polybutadiene carboxy terminated; and an inverse emulsion having a continuous phase, an aqueous dispersed phase, and at least one emulsifier, preferably at least one functionalized silicone compound having at least one functional group chosen from a hydroxyl group, a carboxyl group, hydroxyl-terminated ethylene oxide groups.

Moldable silicon nitride green-body composite and reduced density silicon nitride ceramic process
11365155 · 2022-06-21 · ·

A moldable green-body composite includes milling silicon nitride powder with a solvent and adding a surface modifier to the milled slurry to modify a surface of the silicon nitride particles. A polysiloxane in a solvent and a binder are also added to create a green body slurry. The solvents may be polar or non-polar solvents. A sintering aid, such as yttria-alumina, may be added to the slurry as well. A reduced density silicon nitride ceramic is made from the moldable green-body composite by molding the moldable green-body composite in a mold and curing at a curing temperature to convert the moldable green-body composite to a converted composite. The converted composite can then be sintered to form a reduced density silicon nitride ceramic that has a smooth surface finish and requires no post machining or polishing. The reduced density silicon nitride ceramic may also have very good dielectric properties.

A MOLDING MATERIAL FOR PRODUCING CARBON CLUSTERS AND A METHOD FOR MANUFACTURING THEREOF

A molding material for producing the carbon clusters using biomass as the main raw material, comprising the biomass and a binder as the derived raw material, wherein the molding material is graphitized, the electrical resistivity of the molding material is equal to or less than 100 μΩm, the diffraction pattern of the molding material by powder X-ray diffraction method has one peak between 2θ(θ is the Bragg angle) of 26 to 27°, and the value of ⅓ width divided by the base of the peak is equal to or less than 0.68. The method for producing the molding material for producing the carbon clusters according to any of claims 1 to 6, comprising following steps of: obtaining a molded precursor containing a calcined biomass and a binder; optionally, further baking the precursor; and graphitizing the precursor at a temperature of 2500° C. or higher.

HIGH STRENGTH, TOUGH, COAL AND COAL BY-PRODUCT BASED COMPOSITE CERAMICS
20220144706 · 2022-05-12 ·

A composite material, compositions, processes and methods of using coal and coal by-products composite ceramics is provided for use as a safe, non-toxic material for construction, building and architecture components. The composite material disclosed herein is formed from resin/coal aggregates that contain and prevent the release of harmful impurities that naturally occur in both coal and coal by-products while the advantages of coal-based composites are made available to the building industry. The strength, density and porosity of the composites can be tailored within a wide range to fit the final application by controlling the materials, form factor and processing parameters during fabrication.

Method of making ceramic matrix slurry infused ceramic tows and ceramic matrix composites

Methods of making ceramic matrix prepregs are described. The methods include exposing a coated tow of ceramic fibers to a ceramic matrix slurry comprising a solvent and ceramic precursor. The coating is at least partially removed and the slurry infuses into the ceramic fibers to form prepreg. Steps to form ceramic matrix composites are also described, including forming the prepreg into a green body, and sintering the ceramic precursor.

SPHERICAL MICROPARTICLES FORMED USING EMULSIONS AND APPLICATIONS OF SAID MICROPARTICLES

A composition includes a plurality of microparticles, where the microparticles comprise agglomerates of nanopowder, wherein the nanopowder includes a material selected from the following: a ceramic material, a metal, an alloy, a polymer, or a combination thereof. The microparticles are characterized by having an essentially spherical shape, nanograin features substantially identical to nanograin features of the nanopowder prior to formation into the microparticles, and a nanoscale porosity defined by the nanograin features. The plurality of microparticles have an essentially uniform size relative to one another. Moreover, the composition has flowability having a Hausner Ratio representing tapped density:bulk density less than 1.25.