C07C29/78

Resveratrol-piperazine co-crystals

The present document is directed to co-crystals of resveratrol and/or curcumin with piperazine and their use in medicine and/or as food and feed supplements.

Resveratrol-piperazine co-crystals

The present document is directed to co-crystals of resveratrol and/or curcumin with piperazine and their use in medicine and/or as food and feed supplements.

Procedure for crystallization of (22E)-(24R)-2-methylene-22-dehydro-1α,24-25-trihydroxy-19-nor-vitamin D.SUB.3

Disclosed are methods of purifying the compound (22E)-(24R)-2-methylene-22-dehydro-1α,24,25-trihydroxy-19-nor-vitamin D.sub.3 to obtain the compound in crystalline form. The methods typically include the steps of dissolving (22E)-(24R)-2-methylene-22-dehydro-1α,24,25-trihydroxy-19-nor-vitamin D.sub.3 in a solvent comprising ethyl acetate and hexane to form a solution, allowing crystals of (22E)-(24R)-2-methylene-22-dehydro-1α,24,25-trihydroxy-19-nor-vitamin D.sub.3 to form and precipitate from the solution, and recovering the crystals of (22E)-(24R)-2-methylene-22-dehydro-1α,24,25-trihydroxy-19-nor-vitamin D.sub.3 from the solution.

Procedure for crystallization of (22E)-(24R)-2-methylene-22-dehydro-1α,24-25-trihydroxy-19-nor-vitamin D.SUB.3

Disclosed are methods of purifying the compound (22E)-(24R)-2-methylene-22-dehydro-1α,24,25-trihydroxy-19-nor-vitamin D.sub.3 to obtain the compound in crystalline form. The methods typically include the steps of dissolving (22E)-(24R)-2-methylene-22-dehydro-1α,24,25-trihydroxy-19-nor-vitamin D.sub.3 in a solvent comprising ethyl acetate and hexane to form a solution, allowing crystals of (22E)-(24R)-2-methylene-22-dehydro-1α,24,25-trihydroxy-19-nor-vitamin D.sub.3 to form and precipitate from the solution, and recovering the crystals of (22E)-(24R)-2-methylene-22-dehydro-1α,24,25-trihydroxy-19-nor-vitamin D.sub.3 from the solution.

Method for the preparation of methanol
11697628 · 2023-07-11 · ·

A method for the preparation of methanol by conversion of a mixture of fresh methanol synthesis gas and unconverted methanol synthesis separated from produced methanol in a low pressure separator and recycled and admixed to the fresh synthesis gas upstream the suction side of a make-up gas compressor.

Method for the preparation of methanol
11697628 · 2023-07-11 · ·

A method for the preparation of methanol by conversion of a mixture of fresh methanol synthesis gas and unconverted methanol synthesis separated from produced methanol in a low pressure separator and recycled and admixed to the fresh synthesis gas upstream the suction side of a make-up gas compressor.

METHOD FOR THE PREPARATION OF METHANOL
20220388934 · 2022-12-08 ·

A method for the preparation of methanol by conversion of a mixture of fresh methanol synthesis gas and unconverted methanol synthesis separated from produced methanol in a low pressure separator and recycled and admixed to the fresh synthesis gas upstream the suction side of a make-up gas compressor.

METHOD FOR THE PREPARATION OF METHANOL
20220388934 · 2022-12-08 ·

A method for the preparation of methanol by conversion of a mixture of fresh methanol synthesis gas and unconverted methanol synthesis separated from produced methanol in a low pressure separator and recycled and admixed to the fresh synthesis gas upstream the suction side of a make-up gas compressor.

DIHYDROXYLATION OF OLEFINS USING OSMATE (VI) SALTS
20220388931 · 2022-12-08 ·

A highly efficient synthesis of cis-diol compounds through cis-dihydroxylation of olefins using osmate (VI) salt as catalysts is disclosed, which has found important application in efficient large-scale preparation of, among others, α,α-cedranediol from α-cedrene.

DIHYDROXYLATION OF OLEFINS USING OSMATE (VI) SALTS
20220388931 · 2022-12-08 ·

A highly efficient synthesis of cis-diol compounds through cis-dihydroxylation of olefins using osmate (VI) salt as catalysts is disclosed, which has found important application in efficient large-scale preparation of, among others, α,α-cedranediol from α-cedrene.