C07C45/61

2,4-DIETHYLOCTA-2,6-DIENAL AND ITS USE AS AROMA CHEMICAL

The present invention relates to 2,4-diethylocta-2,6-dienal and a method of preparing same, to the use of 2,4-diethylocta-2,6-dienal as aroma chemical; to the use of 2,4-diethylocta-2,6-dienal for preparing an aroma chemical composition or for modifying the aroma character of an aroma chemical composition; to an aroma chemical composition containing 2,4-diethylocta-2,6-dienal; and to a method of preparing an aromatized composition or for modifying the aroma character of an aromatized composition.

2,4-DIETHYLOCTA-2,6-DIENAL AND ITS USE AS AROMA CHEMICAL

The present invention relates to 2,4-diethylocta-2,6-dienal and a method of preparing same, to the use of 2,4-diethylocta-2,6-dienal as aroma chemical; to the use of 2,4-diethylocta-2,6-dienal for preparing an aroma chemical composition or for modifying the aroma character of an aroma chemical composition; to an aroma chemical composition containing 2,4-diethylocta-2,6-dienal; and to a method of preparing an aromatized composition or for modifying the aroma character of an aromatized composition.

VISIBLE-LIGHT MEDIATED ORGANOPHOTOREDOX CATALYTIC DEUTERATION OF AROMATIC AND ALIPHATIC ALDEHYDES
20230016922 · 2023-01-19 ·

Described are methods for preparing a deuterated aldehyde using with a photocatalyst and a hydrogen atom transfer agent in a H.sub.2O free solvent comprising D.sub.2O and an organic solvent under an inert gas. The methods may be used to convert a wide variety of aldehydes (e.g., aryl, alkyl, or alkenyl aldehydes) to C-1 deuterated aldehydes under mild reaction conditions.

VISIBLE-LIGHT MEDIATED ORGANOPHOTOREDOX CATALYTIC DEUTERATION OF AROMATIC AND ALIPHATIC ALDEHYDES
20230016922 · 2023-01-19 ·

Described are methods for preparing a deuterated aldehyde using with a photocatalyst and a hydrogen atom transfer agent in a H.sub.2O free solvent comprising D.sub.2O and an organic solvent under an inert gas. The methods may be used to convert a wide variety of aldehydes (e.g., aryl, alkyl, or alkenyl aldehydes) to C-1 deuterated aldehydes under mild reaction conditions.

Continuous production of methyl pentenone using cation exchange resin in a fixed bed reactor

Provided herein is a method for producing methyl pentenone (MPO) in high yield in a continuous mode in a fixed bed reactor having a plurality of sidewall injecting ports by reacting excess methyl ethyl ketone (MEK) with acetaldehyde in presence of a cation exchange resin catalyst, wherein the acetaldehyde is injected from the plurality of sidewall injecting ports of the reactor. The method is also effective in reducing the complete consumption of the catalyst during the course of the reaction.

Continuous production of methyl pentenone using cation exchange resin in a fixed bed reactor

Provided herein is a method for producing methyl pentenone (MPO) in high yield in a continuous mode in a fixed bed reactor having a plurality of sidewall injecting ports by reacting excess methyl ethyl ketone (MEK) with acetaldehyde in presence of a cation exchange resin catalyst, wherein the acetaldehyde is injected from the plurality of sidewall injecting ports of the reactor. The method is also effective in reducing the complete consumption of the catalyst during the course of the reaction.

REDUCED ACYLATED GRAPHENE OXIDE AND METHOD FOR PREPARING THE SAME

Provided are reduced acylated graphene oxide as an electrode active material and a method for preparing the same. By the method for preparing reduced acylated graphene oxide according to the present invention, a negative electrode active material for a lithium secondary battery having stable activity and a high battery capacity may be prepared with a simple and low-cost process. In addition, the active material prepared by the preparation method has low resistance, a high battery capacity, and improved rate-limiting characteristics while having stable cycle characteristics.

REDUCED ACYLATED GRAPHENE OXIDE AND METHOD FOR PREPARING THE SAME

Provided are reduced acylated graphene oxide as an electrode active material and a method for preparing the same. By the method for preparing reduced acylated graphene oxide according to the present invention, a negative electrode active material for a lithium secondary battery having stable activity and a high battery capacity may be prepared with a simple and low-cost process. In addition, the active material prepared by the preparation method has low resistance, a high battery capacity, and improved rate-limiting characteristics while having stable cycle characteristics.

Anticancer compounds and process for the preparation thereof

The invention disclosed herein relates to novel Peribysin E analogs of general formula-I. Further the invention provides simple, economical and short synthesis of Peribysin E and its analogs of Formula I, in good yield and purity leading to the identification of more potent cell adhesion inhibitors. ##STR00001##

Anticancer compounds and process for the preparation thereof

The invention disclosed herein relates to novel Peribysin E analogs of general formula-I. Further the invention provides simple, economical and short synthesis of Peribysin E and its analogs of Formula I, in good yield and purity leading to the identification of more potent cell adhesion inhibitors. ##STR00001##