C10L2290/44

Apparatus and process for producing a deacidified fluid stream

A process for producing a deacidified fluid stream from a fluid stream comprising methanol and at least one acid gas and an apparatus for carrying out the process. The process comprising a) an absorption step in which the fluid stream is contacted with an absorbent in an absorber to obtain an absorbent laden with methanol and acid gases and an least partly deacidified fluid stream; b) a regeneration step in which at least a portion of the laden absorbent obtained from step a) is regenerated in a regenerator to obtain an at least partly regenerated absorbent and a gaseous stream comprising methanol, water and at least one acid gas; c) a recycling step in which at least a substream of the regenerated absorbent from step b) is recycled into the absorption step a); d) a condensation step in which a condensate comprising methanol and water is condensed out of the gaseous stream from step b); e) a distillation step in which at least a portion of the condensate from step d) is guided into a distillation column to obtain a top stream comprising methanol and a bottom stream comprising water; which comprises recycling at least a portion of the bottom stream from step e) into the regenerator.

Method for Purifying Glycol Used as a Hydrate Inhibitor

The invention concerns a purification method comprising: providing a flow comprising a glycol, monovalent ions and multivalent ions; treating this flow with ion exclusion chromatography comprising: injecting the flow into a chromatographic unit comprising an ion exchange stationary phase; injecting an eluent into the chromatographic unit; collecting a fraction at the outlet of the chromatographic unit; the collected fraction being enriched with glycol and depleted of monovalent ions and multivalent ions relative to the flow.

The invention also concerns an installation adapted to implement this method, and its application to the regeneration of an anti-hydrate agent.

Experimental method for coal desulfurization and deashing using permeation and solvating power of a supercritical fluid

An experimental method for coal desulfurization and deashing using permeation and solvating power of a supercritical fluid includes the following steps. The coal sample is ground and loaded into an extraction kettle with a cover. An inlet valve and an outlet valve of the extraction kettle are opened to circulate the supercritical CO.sub.2 fluid in the extraction kettle. The extraction kettle is sealed. By adjusting a temperature and a pressure in the extraction kettle, the supercritical CO.sub.2 fluid is kept at its critical point and permeates the coal sample to dissolve organic sulfur, inorganic sulfur and ash in the coal sample. The extraction kettle is depressurized, and the temperature in the extraction kettle is adjusted to gasify the supercritical CO.sub.2 fluid. The organic sulfur, the inorganic sulfur and part of the ash are separated from the supercritical CO.sub.2 fluid and precipitated at a bottom of the extraction kettle.

METHOD FOR PRODUCING LOW-SULFUR COAL

A method for producing low-sulfur coal having an excellent desulfurization effect. In the production method, coal is brought into contact with a chemical agent that is a mixed solution of hydrogen peroxide and acetic acid to remove sulfur in the coal. It is preferred that the molar ratio of the acetic acid to the hydrogen peroxide ((acetic acid)/(hydrogen peroxide)) is 1.2 to 60.0 inclusive. It is preferred that the acetic acid is mixed with the hydrogen peroxide before the chemical agent is brought into contact with the coal and the chemical agent is brought into contact with the coal after 30 minutes or more has elapsed since the mixing is performed.

Process and apparatus for removal of hydrogen sulphide from a gas
11185818 · 2021-11-30 · ·

A process and apparatus for removing hydrogen sulphide from a gas is disclosed. The process comprises the steps of: providing a gas comprising hydrogen sulphide; supplying oxygen for the process if the gas does not comprise oxygen, or does not comprise sufficient oxygen for converting hydrogen sulphide to elementary sulphur; leading the mixture of gas and, if supplied, oxygen to a tank comprising i) a foam forming liquid, such as a scrubber liquid and ii) a foam layer made from said foam forming liquid on the top of the foam forming liquid where the hydrogen sulphide in the gas is oxidized to elementary sulphur to form a cleaned gas removed from hydrogen sulphide.

Composition for removing sulfur-containing compounds

Provided is a composition for removing a sulfur-containing compound contained in at least one of a liquid and gas, the sulfur-containing compound being at least one selected from the group consisting of hydrogen sulfide and an —SH group-containing compound, the composition containing an aldehyde and an amine whose conjugate acid has a pKa value of 11.3 or higher in water at 25° C.

LOW-SULFUR COAL PRODUCTION METHOD

A low-sulfur coal production method having an excellent desulfurization effect includes bringing coal into contact with a chemical material that is a mixed solution of hydrogen peroxide and acetic anhydride to remove sulfur in the coal. It is preferred that the molar ratio of the acetic anhydride to the hydrogen peroxide is 0.5 to 12.0 inclusive. It is preferred that the acetic anhydride is mixed with the hydrogen peroxide before the chemical material is brought into contact with the coal and the chemical material is brought into contact with the coal after 10 minutes or more has elapsed since the mixing.

Process and equipment assembly for beneficiation of coal discards

According to the invention, there is provided a process for the beneficiation of coal discards by increasing calorific value and carbon content while removing inert mineral matter and sulphur compounds. The process involves the pretreatment of wash water with a non-ionic kinetically energized surface-active agent and the admixture with a fixed mass of raw coal discard to enhance hydrophobicity and carboniferous particle agglomeration. Processing of the resulting suspension though a dedicated series of spiral separators and high frequency, resonance sieves reliably reduces excessive levels of mineral ash and sulphur compounds.

PROCESS AND EQUIPMENT ASSEMBLY FOR BENEFICIATION OF COAL DISCARDS
20210245168 · 2021-08-12 ·

According to the invention, there is provided a process for the beneficiation of coal discards by increasing calorific value and carbon content while removing inert mineral matter and sulphur compounds. The process involves the pretreatment of wash water with a non-ionic kinetically energized surface-active agent and the admixture with a fixed mass of raw coal discard to enhance hydrophobicity and carboniferous particle agglomeration. Processing of the resulting suspension though a dedicated series of spiral separators and high frequency, resonance sieves reliably reduces excessive levels of mineral ash and sulphur compounds.

PROCESS FOR PRODUCING A DEACIDIFIED FLUID STREAM
20210147757 · 2021-05-20 ·

A process for producing a deacidified fluid stream from a fluid stream comprising methanol and at least one acid gas, comprising a) an absorption step in which the fluid stream is contacted with an absorbent in an absorber to obtain an absorbent laden with methanol and acid gases and an least partly deacidified fluid stream; b) a regeneration step in which at least a portion of the laden absorbent obtained from step a) is regenerated in a regenerator to obtain an at least partly regenerated absorbent and a gaseous stream comprising methanol and at least one acid gas; c) a recycling step in which at least a substream of the regenerated absorbent from step b) is recycled into the absorption step a); d) a condensation step in which a condensate comprising methanol is condensed out of the gaseous stream from step b);
wherein the regenerator additionally comprises a rescrubbing section, and the condensate from step d) is recycled into the regenerator partly in the upper region of the rescrubbing zone or above the rescrubbing zone.