C22B3/382

METHOD OF RECOVERING CATHODE ACTIVE MATERIAL PRECURSOR
20230049078 · 2023-02-16 ·

A method of recovering a cathode active material precursor according to an embodiment of the present invention includes preparing a cathode active material mixture including a lithium composite oxide, separating lithium from the cathode active material mixture to form a preliminary transition metal precursor, acid-treating the preliminary transition metal precursor to form a complex transition metal salt solution, and adding an acidic extractant to the complex transition metal salt solution and then adding a basic compound to recover a transition metal precursor, and thus the extraction rate of transition metals can be improved.

METHOD FOR EXTRACTING LITHIUM BY MEANS OF EXTRACTION-BACK EXTRACTION SEPARATION AND PURIFICATION
20220372592 · 2022-11-24 ·

The present disclosure relates to a method for lithium recovery by extraction-stripping separation and purification, including: (1) performing an extraction on a lithium-containing solution using an extraction system including a composite extractant at a pH in a range of 10-13 and separating to obtain a lithium-loaded organic phase; (2) subjecting the lithium-loaded organic phase obtained in step (1) to a gas-liquid-liquid three-phase stripping to obtain a lithium-loaded stripping solution; and (3) subjecting the stripping solution obtained in step (2) to a thermal treatment and separating to obtain a lithium product and a separated mother liquor.

Process for separating and recycling a spent alkaline battery

A variety of systems, methods and compositions are disclosed, including, in one method for recycling a spent alkaline battery comprising: dissolving insoluble metal ions in aqueous solution thereby producing pregnant leach solution; extracting zinc sulfate from aqueous solution thereby producing zinc sulfate product and raffinate solution comprising manganese sulfate and potassium sulfate; separating manganese hydroxide from raffinate solution thereby producing manganese sulfate product and aqueous potassium sulfate solution; crystallizing aqueous potassium sulfate solution to produce solid potassium sulfate product. A system for recycling spent alkaline battery comprising: first liquid-solid extraction unit capable of dissolving insoluble metal ions in aqueous solution thereby producing pregnant leach solution; liquid-liquid extraction unit capable of extracting zinc from pregnant leach solution; second liquid-solid extraction unit capable of precipitating manganese hydroxide from raffinate produced by liquid-liquid extraction unit; and third liquid-solid extraction unit capable of crystallizing aqueous potassium sulfate solution produced by second liquid-solid extraction unit.

Continuous solvent extraction process for generation of high grade rare earth oxides from leachates generated from coal sources

A continuous solvent extract process is provided for concentrating rare earth elements from leachates generated from coal sources. The process involves solvent extraction which utilizes an organic extractant mixed into an organic solvent.

PROCESSING OF TITANIFEROUS ORES AND MINERALS
20230312364 · 2023-10-05 ·

The present invention relates to metallurgical processes, and more particularly to a process for producing titaniferous feedstock and fines, a process for agglomerating titaniferous fines, and a process for producing titaniferous metals and titaniferous alloys. Recovery of rare-earth, vanadium and scandium from titanium iron bearing resources is also disclosed. Selective leaching for Scandium recovery from all magnetite type resources such as ilmenite, ferro titanic resources, nickel laterites, magnetite iron resources etc.

SELECTIVE RECOVERY METHOD OF VANADIUM AND CESIUM FROM WASTE SULFURIC ACID VANADIUM CATALYST, AND HIGH-QUALITY VANADIUM AQUEOUS SOLUTION AND CESIUM ALUM PRODUCED THEREBY

Provided are a selective recovery method of vanadium and cesium from a waste sulfuric acid vanadium catalyst by a hydrometallurgical method including water leaching, solid-liquid separation, vanadium solvent extraction, vanadium selective stripping, and cesium alum production, and a high-quality vanadium aqueous solution and cesium alum produced thereby.

Selective recovery method of vanadium and cesium from waste sulfuric acid vanadium catalyst, and high-quality vanadium aqueous solution and cesium alum produced thereby

Provided are a selective recovery method of vanadium and cesium from a waste sulfuric acid vanadium catalyst by a hydrometallurgical method including water leaching, solid-liquid separation, vanadium solvent extraction, vanadium selective stripping, and cesium alum production, and a high-quality vanadium aqueous solution and cesium alum produced thereby.

METHOD FOR PRODUCING BERYLLIUM SOLUTION, METHOD FOR PRODUCING BERYLLIUM, METHOD FOR PRODUCING BERYLLIUM HYDROXIDE, METHOD FOR PRODUCING BERYLLIUM OXIDE, AND BERYLLIUM OXIDE

This invention has an object to provide a method for producing a beryllium solution by dissolving beryllium oxide, the method being novel and having high energy efficiency. A production method (M10) for producing a beryllium solution includes a main heating step (S13) of dielectrically heating an acidic solution containing beryllium oxide to generate a beryllium solution.

PROCESS FOR SEPARATING AND RECYCLING A SPENT ALKALINE BATTERY
20210135250 · 2021-05-06 ·

A variety of systems, methods and compositions are disclosed, including, in one method for recycling a spent alkaline battery comprising: dissolving insoluble metal ions in aqueous solution thereby producing pregnant leach solution; extracting zinc sulfate from aqueous solution thereby producing zinc sulfate product and raffinate solution comprising manganese sulfate and potassium sulfate; separating manganese hydroxide from raffinate solution thereby producing manganese sulfate product and aqueous potassium sulfate solution; crystallizing aqueous potassium sulfate solution to produce solid potassium sulfate product. A system for recycling spent alkaline battery comprising: first liquid-solid extraction unit capable of dissolving insoluble metal ions in aqueous solution thereby producing pregnant leach solution; liquid-liquid extraction unit capable of extracting zinc from pregnant leach solution; second liquid-solid extraction unit capable of precipitating manganese hydroxide from raffinate produced by liquid-liquid extraction unit; and third liquid-solid extraction unit capable of crystallizing aqueous potassium sulfate solution produced by second liquid-solid extraction unit.

CONTINUOUS SOLVENT EXTRACTION PROCESS FOR GENERATION OF HIGH GRADE RARE EARTH OXIDES FROM LEACHATES GENERATED FROM COAL SOURCES
20200048737 · 2020-02-13 ·

A continuous solvent extract process is provided for concentrating rare earth elements from leachates generated from coal sources. The process involves solvent extraction which utilizes an organic extractant mixed into an organic solvent.