Embodiments described herein provide for the flameless premixed combustion of the pyrolysis gases of a milligram-sized sample of solid material in a microscale fire calorimeter (MFC) at high temperatures of combustion and under precisely controlled fuel-to-oxygen ratios. The microscale fire calorimeter (MFC) device and techniques set out herein provide for the generation of fuel gases from solids and the mixing of those fuel gases with oxygen under controlled conditions to obtain precise fuel/oxygen ratios during combustion. Combustion is conducted under flameless, premixed conditions in a rapid test that can generate soot and other products of incomplete combustion, which may then be analyzed to determine their type and nature. This allows for microscale, accurate, and convenient techniques for the generation and determination of the type and nature of combustion species produced over the full range of fire stages from early stage (over-ventilated) fires to late-stage (under-ventilated/high-toxicity) fires.

Embodiments described herein provide for the flameless premixed combustion of the pyrolysis gases of a milligram-sized sample of solid material in a microscale fire calorimeter (MFC) at high temperatures of combustion and under precisely controlled fuel-to-oxygen ratios. The microscale fire calorimeter (MFC) device and techniques set out herein provide for the generation of fuel gases from solids and the mixing of those fuel gases with oxygen under controlled conditions to obtain precise fuel/oxygen ratios during combustion. Combustion is conducted under flameless, premixed conditions in a rapid test that can generate soot and other products of incomplete combustion, which may then be analyzed to determine their type and nature. This allows for microscale, accurate, and convenient techniques for the generation and determination of the type and nature of combustion species produced over the full range of fire stages from early stage (over-ventilated) fires to late-stage (under-ventilated/high-toxicity) fires.

A water quality analyzer includes a combustion tube (2) for burning a liquid sample inside, a sample injector (6; 8) that executes sample injection operation into the combustion tube (2), a pressure sensor (28) that detects pressure inside the combustion tube (2), a temperature sensor (38) that detects a temperature of the combustion tube (2), and a determination part (46) configured to determine whether the combustion tube (2) and/or the sample injector (6; 8) is normal or abnormal based on an output of the pressure sensor (28) and an output of the temperature sensor (38) immediately after the sample injection operation by the sample injector (6; 8) is executed.

A water quality analyzer includes a combustion tube (2) for burning a liquid sample inside, a sample injector (6; 8) that executes sample injection operation into the combustion tube (2), a pressure sensor (28) that detects pressure inside the combustion tube (2), a temperature sensor (38) that detects a temperature of the combustion tube (2), and a determination part (46) configured to determine whether the combustion tube (2) and/or the sample injector (6; 8) is normal or abnormal based on an output of the pressure sensor (28) and an output of the temperature sensor (38) immediately after the sample injection operation by the sample injector (6; 8) is executed.

Embodiments described herein provide for the flameless premixed combustion of the pyrolysis gases of a milligram-sized sample of solid material in a microscale fire calorimeter (MFC) at high temperatures of combustion and under precisely controlled fuel-to-oxygen ratios. The microscale fire calorimeter (MFC) device and techniques set out herein provide for the generation of fuel gases from solids and the mixing of those fuel gases with oxygen under controlled conditions to obtain precise fuel/oxygen ratios during combustion. Combustion is conducted under flameless, premixed conditions in a rapid test that can generate soot and other products of incomplete combustion, which may then be analyzed to determine their type and nature. This allows for microscale, accurate, and convenient techniques for the generation and determination of the type and nature of combustion species produced over the full range of fire stages from early stage (over-ventilated) fires to late-stage (under-ventilated/high-toxicity) fires.

Embodiments described herein provide for the flameless premixed combustion of the pyrolysis gases of a milligram-sized sample of solid material in a microscale fire calorimeter (MFC) at high temperatures of combustion and under precisely controlled fuel-to-oxygen ratios. The microscale fire calorimeter (MFC) device and techniques set out herein provide for the generation of fuel gases from solids and the mixing of those fuel gases with oxygen under controlled conditions to obtain precise fuel/oxygen ratios during combustion. Combustion is conducted under flameless, premixed conditions in a rapid test that can generate soot and other products of incomplete combustion, which may then be analyzed to determine their type and nature. This allows for microscale, accurate, and convenient techniques for the generation and determination of the type and nature of combustion species produced over the full range of fire stages from early stage (over-ventilated) fires to late-stage (under-ventilated/high-toxicity) fires.

A combustion tube comprises a generally cylindrical body with an outwardly extending tube stop spaced from one end of the combustion tube for engaging a combustion tube mounting assembly and fixing the tube in a precise position. Near the opposite end of the tube is an enlarged opening for receiving an upper seal assembly of a combustion furnace with the outer annular shoulder of the upper end of the tube having a rolled edge to facilitate the insertion of the tube through the seal in the upper seal assembly of the furnace. The combustion tube is made of quartz glass to withstand the temperatures encountered in the furnace. The combustion tube is specifically designed and adapted to be precisely positioned in an induction furnace with an easy tube removal system for the furnace.

A combustion tube comprises a generally cylindrical body with an outwardly extending tube stop spaced from one end of the combustion tube for engaging a combustion tube mounting assembly and fixing the tube in a precise position. Near the opposite end of the tube is an enlarged opening for receiving an upper seal assembly of a combustion furnace with the outer annular shoulder of the upper end of the tube having a rolled edge to facilitate the insertion of the tube through the seal in the upper seal assembly of the furnace. The combustion tube is made of quartz glass to withstand the temperatures encountered in the furnace. The combustion tube is specifically designed and adapted to be precisely positioned in an induction furnace with an easy tube removal system for the furnace.

A water quality analyzer includes a combustion tube (2) for burning a liquid sample inside, a sample injector (6; 8) that executes sample injection operation into the combustion tube (2), a pressure sensor (28) that detects pressure inside the combustion tube (2), a temperature sensor (38) that detects a temperature of the combustion tube (2), and a determination part (46) configured to determine whether the combustion tube (2) and/or the sample injector (6; 8) is normal or abnormal based on an output of the pressure sensor (28) and an output of the temperature sensor (38) immediately after the sample injection operation by the sample injector (6; 8) is executed.

A water quality analyzer includes a combustion tube (2) for burning a liquid sample inside, a sample injector (6; 8) that executes sample injection operation into the combustion tube (2), a pressure sensor (28) that detects pressure inside the combustion tube (2), a temperature sensor (38) that detects a temperature of the combustion tube (2), and a determination part (46) configured to determine whether the combustion tube (2) and/or the sample injector (6; 8) is normal or abnormal based on an output of the pressure sensor (28) and an output of the temperature sensor (38) immediately after the sample injection operation by the sample injector (6; 8) is executed.