C01B21/44

METHOD OF CLEANING AN APPARATUS USED IN THE CONCENTRATION OF A MINERAL ACID
20230016848 · 2023-01-19 ·

The present invention relates to a method for preparing an apparatus (or a plant comprising a plurality of apparatuses), for example a heat exchanger, a vaporizer or a distillation column, for use in a process (in particular a continuously operated process) for concentrating a mineral acid by evaporation of water, wherein the apparatus or the plant comprises (at least) a device which is resistant to the mineral acid and the device is flushed with an aqueous alkali metal hydroxide solution having a concentration by mass of alkali metal hydroxide in the range from 1% to 30% at a temperature in the range from 40° C. to 90° C. for a time of from 2 hours to 7 days.

METHOD OF CLEANING AN APPARATUS USED IN THE CONCENTRATION OF A MINERAL ACID
20230016848 · 2023-01-19 ·

The present invention relates to a method for preparing an apparatus (or a plant comprising a plurality of apparatuses), for example a heat exchanger, a vaporizer or a distillation column, for use in a process (in particular a continuously operated process) for concentrating a mineral acid by evaporation of water, wherein the apparatus or the plant comprises (at least) a device which is resistant to the mineral acid and the device is flushed with an aqueous alkali metal hydroxide solution having a concentration by mass of alkali metal hydroxide in the range from 1% to 30% at a temperature in the range from 40° C. to 90° C. for a time of from 2 hours to 7 days.

ABSORPTION TOWER FOR A NITRIC ACID PLANT METHOD FOR PRODUCING NITRIC ACID

An absorption tower for production of nitric acid by the Ostwald process may include sieve trays that are arranged on top of one another and each spaced apart from one another, a water inlet in an upper region of the absorption tower, an inlet for gaseous nitrogen oxides in a lower region of the absorption tower, and a column bottom that is disposed in the lower region of the absorption tower beneath a lowermost sieve tray and is divided by a dividing wall into a first, radially inner region and at least a second, radially outer region. Nitric acid that trickles down from the lowermost sieve tray with a higher concentration can be collected in a middle region. The less-concentrated nitric acid that then effluxes from sieve trays higher up can then be collected separately in a region farther outward.

Method of cleaning an apparatus used in the concentration of a mineral acid
12441614 · 2025-10-14 · ·

The present invention relates to a method for preparing an apparatus (or a plant comprising a plurality of apparatuses), for example a heat exchanger, a vaporizer or a distillation column, for use in a process (in particular a continuously operated process) for concentrating a mineral acid by evaporation of water, wherein the apparatus or the plant comprises (at least) a device which is resistant to the mineral acid and the device is flushed with an aqueous alkali metal hydroxide solution having a concentration by mass of alkali metal hydroxide in the range from 1% to 30% at a temperature in the range from 40 C. to 90 C. for a time of from 2 hours to 7 days.

Method of cleaning an apparatus used in the concentration of a mineral acid
12441614 · 2025-10-14 · ·

The present invention relates to a method for preparing an apparatus (or a plant comprising a plurality of apparatuses), for example a heat exchanger, a vaporizer or a distillation column, for use in a process (in particular a continuously operated process) for concentrating a mineral acid by evaporation of water, wherein the apparatus or the plant comprises (at least) a device which is resistant to the mineral acid and the device is flushed with an aqueous alkali metal hydroxide solution having a concentration by mass of alkali metal hydroxide in the range from 1% to 30% at a temperature in the range from 40 C. to 90 C. for a time of from 2 hours to 7 days.