C01B39/445

Process for preparing a zeolitic material having a framework type FER

The present invention relates to a process for preparing a zeolitic material having a framework type FER and having a framework structure comprising silicon, aluminum, and oxygen, said process comprising (i) preparing an aqueous synthesis mixture comprising water; a zeolitic material having a framework type other than FER and having a framework structure comprising silicon, aluminum, and oxygen; a source of silicon other than the zeolitic material having a framework type other than FER; an organic structure directing agent comprising piperidine; a source of an alkali metal; and a source of a base; (ii) subjecting the aqueous synthesis mixture prepared according to (i) to hydrothermal synthesis conditions comprising heating the synthesis mixture to a temperature in the range of from 140 to 190° C. and keeping the synthesis mixture at a temperature in this range under autogenous pressure, obtaining a mother liquor comprising a solid material which comprises the zeolitic material having a framework type FER.

CATALYST FOR GASOLINE SYNTHESIS FROM DIMETHYL ETHER, METHOD FOR PREPARING THE SAME, AND METHOD FOR PREPARING GASOLINE USING THE SAME

Disclosed is a method for preparing a catalyst for a gasoline reaction of dimethyl ether that includes reacting a silica source, an aluminum source, and a structural derivative to synthesize a zeolite sol, mixing an alcohol with an organic template to form an emulsion phase, and adding a zeolite sol to the emulsion phase to perform a reaction.

SYNTHESIS OF FINNED ZEOLITE CRYSTALS

A secondary growth procedure described herein is used to prepare finned zeolites. The finned zeolites possess properties that are distinctly unique compared to crystals of similar size lacking fins. The procedure is amenable to a wide range of zeolite crystal structures.

Small crystal ferrierite and method of making the same

There is disclosed a highly crystalline, small crystal, ferrierite zeolite prepared from a gel containing a source of silica, alumina, alkali metal and a combination of two templating agents. The resulting material includes ferrierite crystals having a particle size of about or less than about 200 nm. The desired crystal size can be achieved by using a specific composition of the gel. The purity of the material and the crystal size was determined by using X-ray powder diffraction and scanning electron microscopy. The material has excellent surface area and micropore volume as determined by nitrogen adsorption.

PROCESS FOR THE PREPARATION OF ZEOLITES ENCAPSULATING TRANSITION METAL NANOPARTICLES FROM LAYERED SILICATE PRECURSORS
20210370277 · 2021-12-02 · ·

The present invention relates to a process for the production of a transition metal containing zeolite comprising expanding a layered silicate with a swelling agent and introducing the transition metal into the interlayer expanded silicate prior to calcination thereof for obtaining the transition metal containing zeolite. The present invention further relates to a zeolite containing transition metal nanoparticles as obtainable or obtained according to the inventive process, as well as to a zeolite containing nanoparticles per se. Finally the present invention relates to the use of a zeolite containing transition metal nanoparticles as obtainable or obtained according to the inventive process, as well as to the use of a zeolite containing nanoparticles per se.

Synthesis of zeolites having the ferrierite structure
11180376 · 2021-11-23 · ·

A zeolite having the ferrierite framework structure is produced using one or more of n-propylamine, n-butylamine, isobutylamine, and n-amylamine as a structure directing agent.

ZSM-35 MOLECULAR SIEVE AND PRODUCTION METHOD THEREFOR, ISOMERIZATION CATALYST AND PRODUCTION METHOD THEREFOR, AND ISOMERIZATION METHOD
20230286817 · 2023-09-14 ·

The present disclosure provides a ZSM-35 molecular sieve and a preparation method therefor, an isomerization catalyst and a preparation method therefor, and an isomerization method. The preparation method for a ZSM-35 molecular sieve comprises: mixing a silicon source, an aluminum source, an alkali, a template agent and water, then adding a polyacrylamide thereto, and performing crystallization on same twice to obtain a ZSM-35 molecular sieve. The present disclosure further provides an isomerization catalyst prepared from the ZSM-35 molecular sieve and a preparation method therefor, and an isomerization method.

Catalyst for gasoline synthesis from dimethyl ether, method for preparing the same, and method for preparing gasoline using the same

Disclosed is a method for preparing a catalyst for a gasoline reaction of dimethyl ether that includes reacting a silica source, an aluminum source, and a structural derivative to synthesize a zeolite sol, mixing an alcohol with an organic template to form an emulsion phase, and adding a zeolite sol to the emulsion phase to perform a reaction.

PROCESS FOR PREPARING A ZEOLITIC MATERIAL HAVING A FRAMEWORK TYPE FER

The present invention relates to a process for preparing a zeolitic material having a framework type FER and having a framework structure comprising silicon, aluminum, and oxygen, said process comprising (i) preparing an aqueous synthesis mixture comprising water; a zeolitic material having a framework type other than FER and having a framework structure comprising silicon, aluminum, and oxygen; a source of silicon other than the zeolitic material having a framework type other than FER; an organic structure directing agent comprising piperidine; a source of an alkali metal; and a source of a base; (ii) subjecting the aqueous synthesis mixture prepared according to (i) to hydrothermal synthesis conditions comprising heating the synthesis mixture to a temperature in the range of from 140 to 190° C. and keeping the synthesis mixture at a temperature in this range under autogenous pressure, obtaining a mother liquor comprising a solid material which comprises the zeolitic material having a framework type FER.

Carbonylation catalyst and process
10583426 · 2020-03-10 · ·

A catalyst and process for the production of methyl acetate by contacting dimethyl ether and carbon monoxide in the presence of a catalyst which is a zeolite of micropore volume of 0.01 ml/g or less.