C07C49/16

Production method for hexachloroacetone

The present invention relates to a production method of hexachloroacetone, including performing a reaction between at least one kind of compound (A) selected from the group consisting of acetone and chloroacetones having a chlorine atom number of from 1 to 5, and a chlorine molecule (B) in a solvent in the presence of an activated carbon, to obtain the hexachloroacetone.

Production method for hexachloroacetone

The present invention relates to a production method of hexachloroacetone, including performing a reaction between at least one kind of compound (A) selected from the group consisting of acetone and chloroacetones having a chlorine atom number of from 1 to 5, and a chlorine molecule (B) in a solvent in the presence of an activated carbon, to obtain the hexachloroacetone.

PROCESS AND INTERMEDIATE FOR THE MANUFACTURE OF DIFLUOROACETYL CHLORIDE
20200407304 · 2020-12-31 ·

The present invention concerns a process and intermediates for the manufacture of difluoro acetyl chloride. The invention further concerns a process for the manufacture of an agrochemically or pharmaceutically active compound, which comprises the process and intermediate for the manufacture of difluoro acetyl chloride for the manufacture of difluoro acetyl chloride or its intermediate.

PROCESS AND INTERMEDIATE FOR THE MANUFACTURE OF DIFLUOROACETYL CHLORIDE
20200407304 · 2020-12-31 ·

The present invention concerns a process and intermediates for the manufacture of difluoro acetyl chloride. The invention further concerns a process for the manufacture of an agrochemically or pharmaceutically active compound, which comprises the process and intermediate for the manufacture of difluoro acetyl chloride for the manufacture of difluoro acetyl chloride or its intermediate.

Practical method for manufacturing 3,3-difluoro-2-hydroxypropionic acid

Disclosed is a practical method for production of 3,3-difluoro-2-hydroxypropionic acid, which is important as pharmaceutical and agrichemical intermediates. The method includes forming a 4,4-difluoro-2,2-dichloro-3-oxobutanoic acid ester by reaction of a 4,4-difluoro-3-oxobutanoic acid ester with chlorine (Cl.sub.2), forming 3,3-difluoro-1,1-dichloro-2-propanone by reaction of the chlorination product with an acid, and then, reacting the degradation product with a basic aqueous solution.

Practical method for manufacturing 3,3-difluoro-2-hydroxypropionic acid

Disclosed is a practical method for production of 3,3-difluoro-2-hydroxypropionic acid, which is important as pharmaceutical and agrichemical intermediates. The method includes forming a 4,4-difluoro-2,2-dichloro-3-oxobutanoic acid ester by reaction of a 4,4-difluoro-3-oxobutanoic acid ester with chlorine (Cl.sub.2), forming 3,3-difluoro-1,1-dichloro-2-propanone by reaction of the chlorination product with an acid, and then, reacting the degradation product with a basic aqueous solution.

Practical method for manufacturing 3,3-difluoro-2-hydroxypropionic acid

Disclosed is a practical method for production of 3,3-difluoro-2-hydroxypropionic acid, which is important as pharmaceutical and agrichemical intermediates. The method includes forming a 4,4-difluoro-2,2-dichloro-3-oxobutanoic acid ester by reaction of a 4,4-difluoro-3-oxobutanoic acid ester with chlorine (Cl.sub.2), forming 3,3-difluoro-1,1-dichloro-2-propanone by reaction of the chlorination product with an acid, and then, reacting the degradation product with a basic aqueous solution.

PREPARATION METHOD, INTERMEDIATE COMPOUNDS, AND SYNTHESIS METHOD FOR A CLASS OF ANTHRACENE-DERIVED TOXINS IN ORGANIC CHEMISTRY

This invention relates to the field of organic synthesis technology, specifically an intermediate compound for the preparation of a class of anthracene ring toxins derivatives. Starting from relatively inexpensive and readily available anthracene drugs or their derivatives (IV), an intermediate compound (III) has been cleverly designed, which, through a single-step reaction, can be converted into the corresponding pyran, oxazole, and thiazole-like compounds (V); this effectively addresses the issues of restricted raw materials and high costs, as these commercially available raw materials are inexpensive and abundantly supplied in the market, reducing the raw material costs for producing compound (V) and ensuring a stable supply of raw materials for large-scale production.

PREPARATION METHOD, INTERMEDIATE COMPOUNDS, AND SYNTHESIS METHOD FOR A CLASS OF ANTHRACENE-DERIVED TOXINS IN ORGANIC CHEMISTRY

This invention relates to the field of organic synthesis technology, specifically an intermediate compound for the preparation of a class of anthracene ring toxins derivatives. Starting from relatively inexpensive and readily available anthracene drugs or their derivatives (IV), an intermediate compound (III) has been cleverly designed, which, through a single-step reaction, can be converted into the corresponding pyran, oxazole, and thiazole-like compounds (V); this effectively addresses the issues of restricted raw materials and high costs, as these commercially available raw materials are inexpensive and abundantly supplied in the market, reducing the raw material costs for producing compound (V) and ensuring a stable supply of raw materials for large-scale production.

Practical Method for Manufacturing 3,3-Difluoro-2-Hydroxypropionic Acid
20180037533 · 2018-02-08 ·

Disclosed is a practical method for production of 3,3-difluoro-2-hydroxypropionic acid, which is important as pharmaceutical and agrichemical intermediates. The method includes forming a 4,4-difluoro-2,2-dichloro-3-oxobutanoic acid ester by reaction of a 4,4-difluoro-3-oxobutanoic acid ester with chlorine (Cl.sub.2), forming 3,3-difluoro-1,1-dichloro-2-propanone by reaction of the chlorination product with an acid, and then, reacting the degradation product with a basic aqueous solution.