G01N2030/3061

MONOLITHIC MICROFABRICATED GAS ANALYZER AND ENCLOSURE
20220365043 · 2022-11-17 · ·

An improved gas chromatography system is presented. The system comprises: an enclosure having an inlet and an outlet, such that the ventilation flow is from the inlet to the outlet; a chamber disposed in the enclosure; a monolithic gas analyzer disposed in the chamber and a temperature control unit disposed in physical contact with the chamber. The monolithic gas analyzer operates to separate and detect molecules from a gas; whereas, the temperature control unit is configured to control temperature inside the chamber.

DEVICE FOR TAKING AND ANALYZING A GASEOUS SAMPLE

A device for analyzing a gaseous sample including a first housing including a detection assembly housed in the housing including a preconcentrator, a chromatography column and a detector intended to detect the presence of the separated compounds, a sampling assembly including a cartridge that is removable relative to the first housing, a control and processing unit housed in the housing and configured to execute an analysis operating mode capable of generating a first command for the detection assembly to analyze a first gaseous sample, a second command to determine the exceeding of at least one alert threshold and, if an alert threshold is exceeded, a third command for the sampling assembly to take a second gaseous sample.

ESTABLISHING FLUIDIC CONNECTIONS BETWEEN CHROMATOGRAPHY COMPONENTS

A thermal module for pre-heating liquid flowing into a liquid chromatography column, includes a trough compartment with two ends, one of the two ends having an electrical socket, a first fluidic assembly, a second fluidic assembly, and a clamp assembly. The clamp assembly includes a rail configured to receive the first fluidic assembly. The clamp assembly includes a carriage slidably mounted to the rail and configured to receive the second fluidic assembly. The carriage is operable to establish a first fluid tight seal between the first fluidic assembly and a chromatography column received within the clamp assembly, and to establish a second fluid tight seal between the second fluidic assembly and the chromatography column. The clamp assembly is disposed within the trough compartment, and the first fluidic assembly is plugged into the electrical socket at the one end of the trough compartment.

Establishing fluidic connections between chromatography components

A clamp assembly includes a rail configured to receive a first fluidic assembly, and a carriage slidably mounted to the rail and configured to receive a second fluidic assembly. The carriage is operable to establish a first fluid tight seal between the first fluidic assembly and a chromatography column received within the claim assembly, and to establish a second fluid tight seal between the second fluidic assembly and the chromatography column.

FLOW-FIELD-INDUCTED TEMPERATURE GRADIENT GAS CHORMATOGRAPHY
20170234840 · 2017-08-17 ·

The invention relates to a method, to a device, and to the use of a method for the gas-chromatic separation and determination of volatile substances in a carrier gas by means of a chromatographic separating capillary (1), wherein the separating capillary and/or an enveloping capillary (2) surrounding the separating capillary (1) is electrically conductive and is heated with current in the form of a resistance heater and is cooled by a forced convective flow by means of a fluid in the form of a gradient flow field in such a way that a continuous temperature gradient arises over the length of the separating capillary.

Techniques for accelerating thermal equilibrium in a chromatographic column

Techniques are described for accelerating thermal equilibrium in a chromatographic column. An apparatus comprises a chromatography column, and a plurality of temperature control units in thermal contact with the chromatography column. A method of performing liquid chromatography comprises setting an inlet of a chromatography column to a first temperature using a first temperature control unit in thermal contact with said inlet, setting an outlet of the chromatography column to a second temperature using a second temperature control unit in thermal contact with the outlet, wherein the first temperature is less than the second temperature; and injecting a sample into a liquid stream that flows through the chromatography column after the inlet is set at the first temperature and the outlet is at the second temperature.

Techniques for thermally insulating a liquid chromatographic column

An apparatus for performing liquid chromatography includes a chromatography column, and an insulating member surrounding the chromatography column wherein the insulating member is formed from a vacuum chamber surrounding the chromatography column. Another apparatus for performing liquid chromatography includes a chromatography column, and an insulating member surrounding the chromatography column, wherein the insulating member includes aerogel. Also described is a method of insulating a chromatography column comprising forming a jacket surrounding the chromatography column, and creating a vacuum chamber in an area between the jacket and the chromatography column.

FAST TEMPERATURE RAMP GAS CHROMATOGRAPHY
20210199626 · 2021-07-01 ·

A gas chromatography (GC) column system includes an insulation tubing, a metallic GC column disposed within the insulation tubing and having an outer diameter that is less than or equal to an inner diameter of the insulation tubing, a first electrode in contact with the metallic GC column, and a second electrode in contact with the metallic GC column on an opposite side of the insulation tubing from the first electrode. The metallic GC column may be heated by applying a voltage across the first and second electrodes. The voltage may be controlled in response to a measured temperature of the metallic GC column.

MICRO GAS CHROMATOGRAPHY SYSTEM
20210172913 · 2021-06-10 · ·

A thermal desorption unit includes a tube, an adsorbent material including one material or a combination of several materials disposed inside the tube, holding members disposed inside the tube and configured to hold the adsorbent material in the tube, and a heating wire coiled around the tube and configured to generate heat along the tube. A column module includes a capillary column, a heating wire coiled around the capillary column, a temperature sensor configured to monitor the temperature of the capillary column, and an electrical insulating layer disposed around the capillary column and the heating wire.

Modular mounting system for components of heating chamber

An arrangement for mounting components in a heating chamber for heating a fluid of a fluid separation apparatus, wherein the arrangement comprises a mounting board having at least one mounting recess each configured for accommodating at least one component, and the at least one component each configured to be mountable in and/or on the at least one mounting recess.